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Critical Dimensions of Untamped Conical Vessels

Description: Abstract: "The need often arises for determining the critical chemical concentration of uranium solution in the conical bottom of a plant reactor or storage vessel, or the dimension if the concentration is known. This report describes the mathematical analysis of Poisson's equation for a spherical sector, which approximates a right circular cone. The ratio of the critical dimension of an equivalent sphere to the height of the sector for various sector angles is derived from a comparison of firs… more
Date: August 25, 1947
Creator: Murray, Raymond
Item Type: Refine your search to only Report
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Fractionation of Fission Products and Heavy Elements by Volatilization Methods

Description: Technical report describing the attempt to separate the long lived fission product oxides by volatilization methods. A fractionization crucible was used. The fractionations give a fair idea of the relative volatilities of the longer lived fission products and also of the degrees of separation of the plutonium oxide or oxides from the fission products.
Date: August 27, 1946
Creator: Erway, N. D. & Simpson, O. C.
Item Type: Refine your search to only Report
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The Charge on Uranium(VI) in Acid Solution

Description: Abstract. The distribution coefficient of U(VI) between perchloric acid solutions and benzene solutions of TTA has been measured as a function of the acidity. It was possible to interpret the data in terms of the charge on the U(VI) species present in the aqueous phase. The experiments indicate that U(VI) exists as an ion charge +2 at acidities from 0.1M to 2.5M. In the interpretations of the distribution data, it was necessary to know the acidity coefficient of the uranyl chelate in the ben… more
Date: August 15, 1946
Creator: King, Edward L.
Item Type: Refine your search to only Report
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The Dissolution of Thorium Metal and Thorium Dioxide in HNO3 - HF and HNO3- ( NH4 ) 2 SiF6 Mixtures

Description: Abstract. A satisfactory method has been found for dissolving thorium metal and thorium oxide in heat-treated 25-12 stainless steel vessels without excessive corrosion of the vessels. The dissolution medium consists of strong HNO3 containing a small amount of fluoride or fluo-silicate. the fluoride required has no harmful effects on a subsequent solvent-extraction step for a separation of uranium isotopes from the dissolved thorium.
Date: August 2, 1946
Creator: Schuler, Frederick W.; Steahly, Frank L. & Stoughton, Raymond W.
Item Type: Refine your search to only Report
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The Effect of Geometry and Voltage Variations on the Operations of the Phillips Ion Gage

Description: Abstract: "The study of ten P.I.G. geometries with copper electrodes and d.c. voltage indicates that from a pressure of 0.1 to about 3.0 microns, depending upon the gage, there is a consistent change in the air pressure-current characteristics of a P.I.G. as the geometry and voltage are changed. At higher pressures discontinuities appear in the gage current and prohibit its use as a pressure gage. In all useful geometries, the greater the applied voltage above 1000 volts, the shorter the useful… more
Date: August 22, 1945
Creator: McKinney, C. R.; Eggen, Donald T.; Bishop, A.; Arnold, W. A. & Starr, C.
Item Type: Refine your search to only Report
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Crystal Structures of Some Uranium Compounds : a Summary from the Ames Laboratory

Description: Introduction. Some forty different uranium compounds have now been given diffraction study at Ames. Reports of these investigations are scattered in the Project literature; many have been reported in a sentence or two as a note along with chemical or metallographic reports. To make the results of this crystal structure work more available this summary of the Ames work has been compiled. (A similar summary has already been published from the Chicago laboratory.)
Date: August 15, 1945
Creator: Rundle, R. E.; Baenziger, N. C. & Wilson, A. S.
Item Type: Refine your search to only Report
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Vacuum Probe, Standard Leaks, and Needle Valve for Use with the Helium Leak Detector

Description: The following report is split into four parts describing the usage of a vacuum probe for leak hunting with the Helium Leak Detector, the two types of Standard Leaks that were designed to measure the sensitivity of the detector, the development of a needle valve adjusted for controlling the flow of a standard mixture of helium and air into the leak detector for a sensitivity check by the single leak method, and a worm and gear adjustment developed to facilitate throttling of the Helium Leak Dete… more
Date: August 1945
Creator: Samuel, A. J.
Item Type: Refine your search to only Report
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Preparation of Carrier Free Zr-Cb Tracer, Problem Assignment No. 263-X61C, Progress Report

Description: Technical report abstract. A rapid procedure for the preparation of very pure carrier-free Zr and Nb tracer involves the chloroform extraction of the cupferrides of Zr and Nb activities from process solutions. Zr and Nb form very stable chloroform soluble cupferrides in acid solutions (CK-993) and are separated from other fission elements almost quantitatively to yield pure mixture of Zr and Nb activity. A minimum of operations is required and the method is easily adaptable to remote control.
Date: August 28, 1944
Creator: Marinsky, Jacob A. (Jacob Akiba), 1918-2005 & Ballou, Nathan Elmer, 1919-
Item Type: Refine your search to only Report
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Warping Instability in Long Rods

Description: Abstract. If a pile rod gets bowed within its cooling tube it becomes warmer on the side which approaches the tube wall, and thermal expansion tends to warp it in the same direction as the original displacement. This was discussed roughly in N-601, and it was there concluded that the mechanism was not important for an isolated short slug. In connection with current development of continuous jacket (cartridge) assemblies, it seems desirable to look at this question again. In this case it is poss… more
Date: August 17, 1944
Creator: Young, Gale Jay
Item Type: Refine your search to only Report
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Further End Cap Temperature Calculations

Description: Abstract. Recently (CP-1989) it has been shown that the neutron density, and thus the heat production, at the end of a slug with an A1 cap may be appreciably higher than that at the middle of the slag. A re-examination of earlier temperature calculations is made in light of this effect.
Date: August 16, 1944
Creator: Karush, William; Monk, A. T. & Wilkins, J. Ernest, Jr., 1923-2011
Item Type: Refine your search to only Report
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Electrolytic Production of Uranium from Solutions of its Tribromide in Fused Salts

Description: Abstract. the electrodeposition of uranium metal, in the form of tree-like deposits, from molten strontium halide baths is described. Under the best conditions studied, approximately 40% recovery is attained. Freedom from side-reactions of the reduced uranium with anode products and/or refractory materials, and high cathode current densities appear to be essential to the success of the process. the refining of uranium under similar conditions appears to occur quite readily, with approximatel… more
Date: August 15, 1944
Creator: Webster, Richard A.
Item Type: Refine your search to only Report
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The Distribution of Thermal Neutrons in a Slug with Thick End Caps

Description: The distribution of thermal neutrons in a W slug having a one centimeter aluminum end cap has been calculated on the basis of simple diffusion theory. It is found that the average neutron density, and therefore the power output, at the end of the slug is about 34% higher than the density far from the end cap. This result agrees well with the recent Argonne pile experiments (CP-1729).
Date: August 3, 1944
Creator: Wilkins, J. Ernest, Jr., 1923-2011
Item Type: Refine your search to only Report
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Temperature and Heat Flow in a Graphite Electrode

Description: In making various experimental heat studies a power producing metal slug is simulated by a slug with a graphite rod electrode of 3/8" diameter inserted lengthwise through it. There is a helium filled annular space between the graphite and the inner surface of the slug cylinder. Radiant heat passes from the electrode to the metal; with proper adjustment of the electrode current the slug in the steady state will therefor "produce" the same amount of energy from its exterior surface as it would un… more
Date: August 3, 1944
Creator: Schlegel, R.
Item Type: Refine your search to only Report
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Distribution Coefficient of Dâ‚‚O Between Triethylamine and Water

Description: Summary: "Water containing 1.8% D2O was distributed between the two liquid phases formed with triethylamine at 20 and 35 C. The triethylamine was removed from each phase by aseotropic distillation with benzene before analyzing the water by determining its density with a quartz float. The ratios of the concentrations of the D2O in the water layer to that in the amino layer were 1.007 and 1.004 at 20 and 35, respectfully. The differences from unity are about the same as the errors of analysis."
Date: August 31, 1943
Creator: Carlson, H. C.
Item Type: Refine your search to only Report
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Polarographic Determination of Uranium in Dust Samples

Description: Abstract: "Samples of dust are collected from the atmosphere with a Mine Safety Appliance Co. electrostatic precipitator and analyzed for uranium by means of a dropping mercury electrode apparatus. Two to three micrograms of uranium can be detected in a cell solution volume of 1 ml. Iron, nickel and chromium present in shop dusts do not interfere. Copper may interfere if present in excess but may be removed by a sulfide precipitation. Directions for preparation of cell solution and operation of… more
Date: August 30, 1943
Creator: Smith, Stanton B.
Item Type: Refine your search to only Report
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The Extraction Method of Purification of Uranyl Nitrate

Description: Technical report. Three extractions of a diethyl ether solution of uranyl nitrate with small portions of water are effective in removing rare earths, as is shown by radio-gadolinium and radio-europium tracer experiments. A study of representative ethers, alcohols, ketones, and esters showed that diethyl ether and a mixture of 85% ethyl methyl ketone with 15% xylene are the best solvents for the extraction.
Date: August 28, 1942
Creator: Myers, L. S., Jr.; Anderson, K. C.; Wexler, Sol & Boyd, G. E.
Item Type: Refine your search to only Report
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