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Accurate Nuclear Fuel Burnup Analyses; Eighth Quarterly Progress Report, (September - November 1963)

Description: The objective of the Accurate Nuclear Fuel Burnup Analyses program is to develop more accurate methods for burnup analysis for general use than the current method of analysis of Ca-137 or Sr-90. The program will require from three to five years of effort.
Date: December 1, 1963
Creator: Rider, B. F.; Ruiz, C. P.; Luke, P. S., Jr.; Peterson, J. P., Jr. & Smith, F. R.
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Plutonium Trichloride: Preparation by Reaction with Phosgene or Carbon Tetrachloride and Bomb Reduction to Metal

Description: Thirty gram patches of plutonium dioxide can be readily chlorinated by reaction with phosgene or carbon tetrachloride at temperatures of 350 and 450 C respectively. Plutonium trichloride prepared by either method can be reduced to the metal in a hermetically sealed bomb by reaction with calcium. On a twenty gram scale yields of approximately 97 per cent are obtained when a calcium-iodine booster is employed. It has been demonstrated that a method for reduction of plutonium trichloride to the… more
Date: December 3, 1953
Creator: Tolley, W. B.
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Two-Phase Pressure Losses Quarterly Progress Report: Seventh Quarter, August 12, 1963 - November 11, 1963

Description: Technical report describing that the pressure drop along an annular channel with dimensions D(1) = 0.375 inch; D(2) = 0.875 inch, L = 70 inches. Flow was vertical and upward, and only the internal surface was heated. Subcooled conditions existed at the inlet, with two-phase conditions at the exit. Groups of three radial spacer pins on 18-inch centers along the channel, held the inner surface concentric with the outer surface. The single phase loss coefficient for each spacer group is K(8) = 0.2… more
Date: December 2, 1963
Creator: Janssen, E. (Engineer) & Kervinen, J. A.
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Wet Fluoride Studies: Calcium Plutonium (IV) Fluoride

Description: Laboratory studies have shown that the double salt, CaF2-PuF4, can be precipitated by rapid addition of hydro-fluoric acid to solutions containing 25 to 75 g Pu/1, caleium equimolar to plutonium, and 1 to 10 M HNO3. The precipitate, which is subsequently washed with water and dried to 300 degrees C in dehumidified, deoxygenated argon, can be reduced thermally by calcium to give high yields of plutonium metal.
Date: December 22, 1953
Creator: Branin, P. B.
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