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in publisher: "Dow Corning Corp., Carrollton, KY United States"  
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Methyl chloride via oxyhydrochlorination of methane

Description: Work to develop a highly selective methyl chloride synthesis catalyst continued, but no stable catalyst with >80% selectivity at 20% methane exists yet. Effort was made on finalizing the pre- engineering scope definition of the Process Demonstration Unit. Natural gas purification, reactor, reactor effluent and MeCl purification, and anhydrous HCl recovery are discussed.
Date: March 4, 1993
Creator: Naasz, B.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane

Description: Purpose of this contract is to develop a process for converting light alkane gases to methyl chloride via oxyhydrochlorination using highly selective, stable catalysts (Cu) in either fixed-bed or fluid-bed reactors. Catalyst development and micro-packed bed screening studies are underway. Engineering support for pre-design on the miniplant is struggling with the unit operations problem associated with separation of products from unreacted methane.
Date: February 10, 1992
Creator: Naasz, B.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 5, October--December 1992

Description: Objective is to develop a process for converting light alkane gases to methyl chloride via oxyhydrochlorination using highly selective, stable catalysts (CuO based) in fixed-bed reactors designed to remove the large amount of heat generated, so as to control the reaction temperature. The proposed PFD for this unit was described to management, and the PDU PFD is currently being expanded into a P&ID with a subcontractor.
Date: June 1, 1993
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 6, January--March 1993

Description: The purpose of this contract is to develop a process for converting light alkane gases to methyl chloride via oxyhydrochlorination using highly selective, stable catalysts in fixed-bed reactors designed to remove the large amount of heat generated, so as to control the reaction temperature. Further, the objective is to obtain the engineering data base necessary for developing a commercially feasible process and to evaluate the economics of the process. This document reports significant progress… more
Date: November 1, 1993
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 7, April--June 1993

Description: The purpose of this contract is to develop a process for converting light alkane gases to methyl chloride via oxyhydrochlorination using highly selective, stable catalysts in fixed-bed reactors designed to remove the large amount of heat generated, so as to control the reaction temperature. Further, the objective is to obtain the engineering data base necessary for developing a commercially feasible process and to evaluate the economics of the process. Several key technology areas were evaluate… more
Date: January 1, 1994
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Final quarterly technical report, July 1, 1992--September 30, 1992

Description: Work to develop a highly selective methyl chloride synthesis catalyst continued, but no stable catalyst with >80% selectivity at 20% methane exists yet. Effort was made on finalizing the pre- engineering scope definition of the Process Demonstration Unit. Natural gas purification, reactor, reactor effluent and MeCl purification, and anhydrous HCl recovery are discussed.
Date: March 4, 1993
Creator: Naasz, B.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Final quarterly technical report, October 1, 1991--December 31, 1991

Description: Purpose of this contract is to develop a process for converting light alkane gases to methyl chloride via oxyhydrochlorination using highly selective, stable catalysts (Cu) in either fixed-bed or fluid-bed reactors. Catalyst development and micro-packed bed screening studies are underway. Engineering support for pre-design on the miniplant is struggling with the unit operations problem associated with separation of products from unreacted methane.
Date: February 10, 1992
Creator: Naasz, B.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 11, April--June 1994

Description: The purpose of this contract is to develop a process for converting light alkane gases to methyl chloride via oxyhydrochlorination using highly selective, stable catalysts in fixed-bed reactors designed to remove the large amount of heat generated, so as to control the reaction temperature. Further, the objective is to obtain the engineering data base necessary for developing a commercially feasible process and to evaluate the economics of the process. Significant progress was made in catalyst … more
Date: November 1, 1994
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 10, January 1944--March 1994

Description: In work related to the design and construction of the Process Development Unit (PDU) this quarter involved further detail design and a real start to the construction activities. Status updates are given below for each discipline in the Task 2.0 and 3.0 headings. This work is progressing well. with the caveat of several small slips in the scheduling. On the catalyst development front this quarter was extremely productive. Many catalyst screening experiments were completed and they showed that co… more
Date: August 1, 1994
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 12, July--September 1994

Description: Significant progress was made in six different technical areas during this quarter. These key highlights are: (1) Mixed LnCl{sub 3} solutions were successfully tested as substitutes for LaCl{sub 3} in preparing OHC catalysts. This will dramatically lower the price of the catalyst. (2) Six catalyst samples were received from UCI. Each was made via either incipient wetness or compounded extrudate techniques. Four of the catalysts have been screened. All seem adequate. (3) Contact has opened with … more
Date: November 1, 1994
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane: A building block for chemicals and fuels from natural gas. Quarterly technical progress report No. 01, September 30, 1996--December 31, 1996

Description: The objectives of this cooperative agreement are to develop the oxyhydrochlorination (OHC) process for the conversion of methane to methyl chloride. In the first Phase of the project, Dow Corning has developed a stable selective catalyst and demonstrated the technology on a laboratory and a pilot plant scale. Specific tasks to achieve these objectives have been developed as follows: TASK 1 Fundamental Technical and Economic Evaluation TASK 2 Catalyst Selection Optimization and Characterization … more
Date: January 16, 1997
Creator: Wineland, J.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 16, July 1995--September 1995

Description: Continuous progress is being made toward the contract objectives in our attempt to produce {open_quotes}Methyl Chloride via Oxyhydrochlorination of Methane.{close_quotes} Specifically, gains have been achieved in Task 1.0 Catalyst Development and Separation Unit Operation Development and Task 4.0 PDU Startup. Catalyst development continued forward to examine the copper, lanthanum, and lithium loadings as well as support surface area in four factor, two level, fully crossed design experiments ca… more
Date: March 1, 1996
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 17, October 1995--December 1995

Description: Continuous progress is being made toward the contract objectives in our attempt to produce {open_quotes}Methyl Chloride via Oxyhydrochlorination of Methane.{close_quotes} Specifically, gains have been achieved in Task 1.0 Catalyst Development and Separation Unit Operation Development and Task 5.0 Evaluation of Packed Bed Technology. Task 4.0 PDU Startup has been completed. A recent patent by Asahi Glass Company (JP 06340560) claims significant improvement in the OHC process through the use of a… more
Date: March 1, 1996
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 9, October 1993--December 1993

Description: The purpose of this contract is to develop a process for converting light alkane gases to methyl chloride via oxyhydrochlorination using highly selective, stable catalysts in fixed-bed reactors designed to remove the large amount of heat generated, so as to control the reaction temperature. Further, the objective is to obtain the engineering data base necessary for developing a commercially feasible process and to evaluate the economics of the process. The key technical progress this quarter wa… more
Date: February 1, 1994
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane. Quarterly technical progress report No. 13, October--December 1994

Description: The purpose of this contract is to develop a process for converting light alkane gases to methyl chloride via oxyhydrochlorination using highly selective, stable catalysts in fixed-bed reactors designed to remove the large amount of heat generated, so as to control the reaction temperature. Further, the objective is to obtain the engineering data base necessary for developing a commercially feasible process and to evaluate t economics of the process. Significant progress was made in six differe… more
Date: February 1, 1995
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
open access

Methyl chloride via oxyhydrochlorination of methane: A building block for chemicals and fuels from natural gas. Environmental assessment

Description: DOE`s natural gas mission, in partnership with its stakeholders, is to undertake and promote activities to maximize the Nation`s ability to supply, transport, and use natural gas to encourage economic growth, enhance energy interests security, and improve the environment. In implementing this mission, DOE has been involved in promoting domestic natural gas as a clean, abundant, and reliable source of energy. In particular, DOE is interested in technologies capable of converting natural gas to o… more
Date: September 1, 1996
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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