A pilot-plant scale process for animation of sym-trichlorotrinitrobenzene (TCTNB) in the presence of water to produce sym-triaminotrinitrobenzene (TATB) has been developed. With this process the chlorine content from trapped impurities is reduced from the typical 0.5 to 1.0 percent range fown to about 0.1 percent. This reduction in chlorine is accompanied by a decrease in size of the median particle by 5 to 10 ..mu..m.
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A pilot-plant scale process for animation of sym-trichlorotrinitrobenzene (TCTNB) in the presence of water to produce sym-triaminotrinitrobenzene (TATB) has been developed. With this process the chlorine content from trapped impurities is reduced from the typical 0.5 to 1.0 percent range fown to about 0.1 percent. This reduction in chlorine is accompanied by a decrease in size of the median particle by 5 to 10 ..mu..m.
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