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Radiochemical analysis of the first plateout probe from the Fort St. Vrain high-temperature gas-cooled reactor

Description: This report presents the analysis of radioactive elements on the first plateout probe from the Fort St. Vrain high-temperature gas-cooled reactor. The plateout probe is a device which samples the primary coolant for condensible fission products. Circuit inventories of individual radionuclides are estimated from the probe analysis. The analysis shows that the radioactive contamination in the primary circuit is remarkable low, with activation product concentrations much greater than that of fissi… more
Date: June 1, 1982
Creator: Burnette, R. D.
Partner: UNT Libraries Government Documents Department
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Orientation study of the Lake Sunapee area, New Hampshire. National Uranium Resource Evaluation Program

Description: An orientation study was conducted in the area of Lake Sunapee, New Hampshire, in preparation for a hydrogeochemical and stream sediment reconnaissance in glacial terrain. The study was carried out by the Savannah River Laboratory as part of the National Uranium Resource Evaluation (NURE). Ground water, lake water, stream water, lake sediment, and stream sediment samples were collected at 188 sites. The concentrations of uranium and other elements were determined by neutron activation analysis.… more
Date: August 1, 1982
Creator: Karfunkel, B. S. & Sargent, K. A.
Partner: UNT Libraries Government Documents Department
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Sediment and radionuclide transport in rivers. Phase 3. Field sampling program for Cattaraugus and Buttermilk Creeks, New York

Description: A field sampling program was conducted on Cattaraugus and Buttermilk Creeks, New York during April 1979 to investigate the transport of radionuclides in surface waters as part of a continuing program to provide data for application and verification of Pacific Northwest Laboratory's (PNL) sediment and radionuclide transport model, SERATRA. Bed sediment, suspended sediment and water samples were collected during unsteady flow conditions over a 45 mile reach of stream channel. Radiological an… more
Date: August 1, 1982
Creator: Ecker, R. M.; Walters, W. H. & Onishi, Y.
Partner: UNT Libraries Government Documents Department
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Tested method to minimize plutonium assay discrepancies between laboratories

Description: Plutonium assay differences are frequently observed between laboratories exchanging plutonium dioxide powders. These differences are commonly the result of chemical changes and/or nonhomogeneities in sampled materials. The irregularities are often caused by moisture absorption during sampling, packaging, shipment, and storage of the materials. A method is proposed which eliminates the effects of chemical change in samples, particularly moisture absorption, and minimizes sampling error. A nondes… more
Date: January 29, 1982
Creator: Seiler, R. J.; Goss, R. L.; Rodenburg, W. W. & Rogers, D. R.
Partner: UNT Libraries Government Documents Department
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Standards for holdup measurement

Description: Holdup measurement, needed for material balance, depend intensively on standards and on interpretation of the calibration procedure. More than other measurements, the calibration procedure using the standard becomes part of the standard. Standards practical for field use and calibration techniques have been developed. While accuracy in holdup measurements is comparatively poor, avoidance of bias is a necessary goal.
Date: January 1, 1982
Creator: Zucker, M.S.
Partner: UNT Libraries Government Documents Department
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Data report: Illinois, Indiana, Kentucky, Tennessee, and Ohio. National Uranium Resource Evaluation Program. Hydrogeochemical and stream sediment reconnaissance

Description: This report presents the results of ground water, stream water, and stream sediment reconnaissance in Illinois, Indiana, Kentucky, Tennessee, and Ohio. The following sample types were collected in each state: Illinois - 716 stream sediment, 1046 ground water, 337 stream water; Indiana - 126 stream sediment, 443 ground water, 111 stream water; Kentucky - 4901 stream sediment, 6408 ground water, 3966 stream water; Tennessee - 3309 stream sediment, 3574 ground water, 1584 stream water; Ohio - 1214… more
Date: February 1, 1982
Creator: Sargent, K. A.; Cook, J. R. & Fay, W. M.
Partner: UNT Libraries Government Documents Department
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Quantification of surface contamination: principles and applications

Description: The applications discussed in this paper underscore the usefulness and versatility of molecular luminescence spectroscopy as an efficient surface detection technique. The technique can be used not only as a qualitative characterization method, but also as a quantitative analytical tool to detect trace contaminants on surfaces. Recent advances in instrumentation and methodology have expanded the applicability of surface luminescence into many new problem areas. Trace organics are emphasized here. more
Date: January 1, 1982
Creator: Vo-Dinh, T.
Partner: UNT Libraries Government Documents Department
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Determination of light elements in amalgam restorations. [Dental amalgam]

Description: Rutherford backscattering has been used to measure the major elemental compositions in the near-surface regions of freshly prepared and used samples of dental amalgam. A depletion from bulk stoichiometry of the major elements, which indicates an accumulation of lighter elements on the surface of the materials, has been observed. Increases in the F, Na, Cl, P, O, C, and N concentrations between freshly prepared samples and used samples were measured by observation of gamma rays produced by proto… more
Date: January 1, 1982
Creator: Hanson, A. L.; Jones, K. W.; Kraner, H. W.; Osborne, J. W. & Nelson, G. V.
Partner: UNT Libraries Government Documents Department
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Radiological and Environmental Research Division, Center for Human Radiobiology. Annual report, July 1980-June 1981. [Lead abstract]

Description: Separate abstracts were prepared for the 22 papers of this annual report of the Center for Human Radiobiology. Abstracts were not written for 2 appendices which contain data on the exposure and radium-induced malignancies of 2259 persons whose radium content has been determined at least once. (KRM)
Date: March 1, 1982
Partner: UNT Libraries Government Documents Department
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TRU waste-assay instrumentation and application in nuclear-facility decommissioning

Description: The Los Alamos TRU waste assay program is developing measurement techniques for TRU and other radioactive waste materials generated by the nuclear industry, including decommissioning programs. Systems are now being fielded for test and evaluation purposes at DOE TRU waste generators. The transfer of this technology to other facilities and the commercial instrumentation sector is well in progress. 6 figures.
Date: January 1, 1982
Creator: Umbarger, C.J.
Partner: UNT Libraries Government Documents Department
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Sediment and radionuclide transport in rivers. Phase 2. Field sampling program for Cattaraugus and Buttermilk Creeks, New York

Description: As part of a study on sediment and radionuclide transport in rivers, Pacific Northwest Laboratory (PNL) is investigating the effect of sediment on the transport of radionuclides in Cattaraugus and Buttermilk Creeks, New York. A source of radioactivity in these creeks is the Western New York Nuclear Service Center which consists of a low-level waste disposal site and a nuclear fuel reprocessing plant. Other sources of radioactivity include fallout from worldwide weapons testing and natural backg… more
Date: April 1, 1982
Creator: Walters, W. H.; Ecker, R. M. & Onishi, Y.
Partner: UNT Libraries Government Documents Department
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DOE research and development report. Progress report, October 1980-September 1981

Description: The DOE New Brunswick Laboratory (NBL) is the US Government's Nuclear Materials Standards and Measurement Laboratory. NBL is assigned the mission to provide and maintain, as an essential part of federal statutory responsibilities related to national and international safeguards of nuclear materials for USA defense and energy programs, an ongoing capability for: the development, preparation, certification, and distribution of reference materials for the calibration and standardization of nu… more
Date: March 1, 1982
Creator: Bingham, Carleton D.
Partner: UNT Libraries Government Documents Department
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Physical and chemical characterization of synthetic calcined sludge

Description: Calcined synthetic sludge was chemically characterized in support of engineering studies to design a processing plant to solidify highly radioactive waste at the Savannah River Plant. An analytical technique is described which provides quantitative data by mass spectrometric analysis of gases evolved during thermogravimetric analysis without measurements of gas flow rates or mass spectrometer sensitivities. Scanning electron microprobe analysis, Mossbauer spectroscopy, and several other common … more
Date: March 1, 1982
Creator: Slates, R.V.; Mosley, W.C. Jr.; Tiffany, B. & Stone, J.A.
Partner: UNT Libraries Government Documents Department
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Advances in measurement of alpha-contaminated wastes

Description: A comprehensive program is in progress at the Los Alamos National Laboratory for the development of sensitive, practical, nondestructive assay techniques for the quantification of low-level transuranics in bulk solid wastes. The program encompasses a broad range of techniques, including sophisticated active and passive gamma-ray spectroscopy, passive neutron detection systems, pulsed portable neutron generator interrogation systems, and electron accelerator-based techniques. The techniques can … more
Date: January 1, 1982
Creator: Close, D. A.; Crane, T. W.; Caldwell, J. T.; Kunz, W. E.; Shunk, E. R.; Pratt, J. C. et al.
Partner: UNT Libraries Government Documents Department
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Calculation of parameters for inspection planning and evaluation: mixed-oxide fuel fabrication facilities

Description: As part of Task C.35 (Calculation of Parameters for Inspection Planning and Evaluation) of the US Program of Technical Assistance to IAEA Safeguards, Pacific Northwest Laboratory has performed some quantitative analyses of IAEA inspection activities for mixed-oxide fuel fabrication facilities. There were four distinct efforts involved in this task. These were as follows: show the effect on a material balance verification of using two variables measurement methods in some strata; perform additio… more
Date: August 1, 1982
Creator: Reardon, P.T. & Mullen, M.F.
Partner: UNT Libraries Government Documents Department
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Nondestructive verification and assay systems for spent fuels. Technical appendixes

Description: Six technical appendixes are presented that provide important supporting technical information for the study of the application of nondestructive measurements to spent-fuel storage. Each appendix addresses a particular technical subject in a reasonably self-contained fashion. Appendix A is a comparison of spent-fuel data predicted by reactor operators with measured data from reprocessors. This comparison indicates a rather high level of uncertainty in previous burnup calculations. Appendix B de… more
Date: April 1, 1982
Creator: Cobb, D. D.; Phillips, J. R. & Baker, M. P.
Partner: UNT Libraries Government Documents Department
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Analysis data on samples from the TMI-2 reactor-coolant system and reactor-coolant bleed tank

Description: Two liquid samples from the Three Mile Island Unit 2 (TMI-2) Reactor Coolant System (RCS) and three liquid samples from the three Reactor Coolant Bleed Tanks (RCBT) were taken during the time period March 29, 1979 to August 14, 1980. The samples were analyzed for radionuclide concentrations by two independent laboratories, Exxon Nuclear Idaho Co., Inc. (ENICO) and EG and G Idaho, Inc. at the Idaho National Engineering Laboratory (INEL). The RCS sample taken on March 29, 1979 was also analyzed b… more
Date: May 1, 1982
Creator: Nitschke, R.L.
Partner: UNT Libraries Government Documents Department
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Spectrophotometric determination of plutonium with chlorophosphonazo III in n-pentanol

Description: Microgram amounts of plutonium are measured spectrophotometrically as the plutonium-chlorophosphonazo III complex after extraction into n-pentanol from 1.5 M HCl. The relative standard deviation is 1.5% for the range of 2.5 to 17.5 ..mu..g. The tolerance is excellent for many metals and nonmetals present in nuclear fuel-cycle materials. A preceding anion-exchange-column separation increases tolerance for certain metals and nonmetals.
Date: March 1, 1982
Creator: Saponara, N.M. & Marsh, S.F.
Partner: UNT Libraries Government Documents Department
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Fast-neutron coincidence-counter manual

Description: The fast neutron counter (FNC) described in this report is a computer-based assay system employing fast-pulse counting instrumentation. It is installed below a glove box in the metal electrorefining area of the Los Alamos National Laboratory Plutonium Processing Facility. The instrument was designed to assay plutonium salts and residues from this process and to verify the mass of electrorefined metal. Los Alamos National Laboratory Groups Q-1, Q-3, and CMB-11 carried out a joint test and evalua… more
Date: March 1, 1982
Creator: Ensslin, N.; Atwell, T. L.; Lee, D. M.; Erkkila, B.; Marshall, R. S.; Morgan, A. et al.
Partner: UNT Libraries Government Documents Department
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Hydrogeochemical and stream-sediment reconnaissance, orientation study, Ouachita Mountain area, Arkansas. National Uranium Resource Evaluation Program

Description: A hydrogeochemical ground water orientation study was conducted in the multi-mineralized area of the Ouachita Mountains, Arkansas in order to evaluate the usefulness of ground water as a sampling medium for uranium exploration in similar areas. Ninety-three springs and nine wells were sampled in Clark, Garland, Hot Springs, Howard, Montgomery, Pike, Polk, and Sevier Counties. Manganese, barite, celestite, cinnabar, stibnite, copper, lead, and zinc are present. The following parameters were dete… more
Date: August 1, 1982
Creator: Steele, K. F.
Partner: UNT Libraries Government Documents Department
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Environmental monitoring at the Lawrence Livermore National Laboratory. 1981 annual report

Description: This report gives methods and results of the 1981 radiation monitoring program at LLL for both radioactive and non-radioactive contamination from gaseous and liquid effluents. Off-site monitoring includes various radionuclides but especially tritium in the ecosystems. (PSB)
Date: March 11, 1982
Creator: Auyong, M.; Griggs, K.S. & Buddemeier, R.W.
Partner: UNT Libraries Government Documents Department
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Simple home-made sensors for potentiometric titrations. [Nitroform CH(NO/sub 2/)/sub 3/]

Description: A sensor for potentiometric titrations was prepared by coating a spectroscopic graphite rod with a solution of poly(vinyl chloride) and dioctyphthalate in tetrahydrofuran. The reference electrode was an Ag/AgCl single-junction electrode. The sensor was used in precipitation, acid-base, compleximetric, and redox titrations. Preparation of the coated-graphite sensor is simple and rapid. Moreover, it is quite inexpensive. A limitation is its applicability in aqueous media only, because organic sol… more
Date: April 1, 1982
Creator: Selig, W.
Partner: UNT Libraries Government Documents Department
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Initial emission assessment of hazardous-waste-incineration facilities

Description: Health and Safety Research Division, sponsored by EPA, conducted a study to quantify emission factors from stacks, spills, fugitives, storage, and treatment for a typical hazardous waste incinerator facility. Engineering participated in preparing flowsheets and providing calculations for fugitive emissions. Typical block-flow diagrams were developed two types of hazardous waste incinerators (rotary kiln and liquid-injector) and for three capacities (small: 1 MM Btu/hr, median: 10 MM Btu/hr, and… more
Date: January 1, 1982
Creator: Harrington, E. S.; Holton, G. A. & O'Donnell, F. R.
Partner: UNT Libraries Government Documents Department
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Gamma-ray measurements for simultaneous calorimetric assay

Description: Gamma-ray measurements obtained in the course of developing a simultaneous calorimetric assay system are described. Gamma-ray measurements of the isotopic composition of six, well-characterized plutonium oxide samples were obtained while the samples were in the calorimeter. These samples represent a range of plutonium masses from 19 to 231 g and two isotopic compositions. The values of effective specific power determined from the gamma-ray measurements agree with the values determined from dest… more
Date: March 2, 1982
Creator: Rakel, D.A.
Partner: UNT Libraries Government Documents Department
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