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Summary Technical Report for the Period July 1, 1956 to September 1, 1956

Description: The activities of the Technical Division, including the HNO/sub 3/ recovery process, a study of UO/sub 3/ factors as related to the production of metal-grade UF/sub 4/, a thermobalance investigation of starch as a reducing agent for UO/sub 3/, reduction of UF/sub 4/ to uranium by a thermite type reaction, melting and casting of Nb-U alloy, uranium recovery from scrap materials, preparation of uranium shot, cal cium reduction of ThO/sub 2/ production of thorium ingots, "wet chemical" and spectro… more
Date: October 15, 1956
Creator: Simmons, J. W.
Partner: UNT Libraries Government Documents Department
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THE DETERMINATION OF NIOBIUM IN URANIUM-NIOBIUM ALLOYS

Description: Niobium is determined as the peroxy complex in concentrated sulfuric acid by photometric measurement at 360 m mu . Uranium interference is cancelled by using a solution of the sample for reference in the photometric measurement. The method covers the determination of niobium in uranium --niobium alloys made from pure melting stock. Molybdenum interferes and must be removed if present. Zirconium does not interfere. The calibration curve covers a concentration range from 0.2 to 5.0 mg. (auth)
Date: April 24, 1956
Creator: Bryson, T. C.; Goward, G. W. & Hartmann, M. D.
Partner: UNT Libraries Government Documents Department
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