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Chemical Development Section C Progress Report for October-November 1960

Description: Studies are being made on the recovery of thorium (and uranium) from granitic rock, since this source represents a very large potential thorium reserve for the nuclear power industry. In preliminary leaching studies on 16 granite samples (containing 8-95 ppm thorium and 1.5-16 ppm uranium), maximum recoveries of thorium and uranium ranged 30-85% and 15-65% respectively, and sulfuric acid consumption was high (30-120 lbs H2SO4 per ton of granite). A relatively high acidity was needed to obtain r… more
Date: March 3, 1961
Creator: Brown, K. B.
Partner: UNT Libraries Government Documents Department
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Erosion Experiments of Powder Compacted Uranium Dioxide Under Dynamic Steam Flow (Preliminary Report)

Description: Experiments were carried out to determine the erosion, oxidation and dimensional characteristics of purposely defected fuel elements containing unsintered UO2 powder prepared by the swaging technique. The experiments were conducted in an out-of-reactor loop under superheat conditions of pressure, temperature, flow velocity and steam chemical composition.
Date: March 21, 1961
Creator: Spalaris, C. N.; Comprelli, F. A. & Siegler, M.
Partner: UNT Libraries Government Documents Department
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VARI-II

Description: Writing the VARI-II Program was motivated by the need for a method of analyzing the results for the Absorber Burn-Up Experiment in progress at the Vallecitos Atomic Laboratory.
Date: March 10, 1961
Creator: Russell, J. L. (John L.), Jr.
Partner: UNT Libraries Government Documents Department
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VARI Solution of Simultaneous, First-Order, Ordinary, Differential Equations

Description: VARI solves on the IBM-650 a system of simultaneous, first-order, ordinary, differential equations. The program was written so that a large number of calculations could be done in a reasonable length of time. The program permits the consideration of the production of the isotope by absorption and/or decay of one or more of any of the other isotopes in the chain.
Date: March 15, 1960
Creator: Kerr, B. A.
Partner: UNT Libraries Government Documents Department
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0-2 kv Flash Tube Supplies

Description: In order to perform the various experiments with a bubble chamber, a high intensity flash tube is used. This report briefly describes the power supplies designed and constructed to power these lamps.
Date: March 15, 1962
Creator: Miller, D. M.
Partner: UNT Libraries Government Documents Department
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6 kv Capacitor Charging Supply

Description: The power supplies designed and constructed to power high intensity flash tubes used in bubble chamber experiments are briefly described and are accompanied by a schematic diagram of the layout. (D.C.W.)
Date: March 15, 1962
Creator: Miller, D. M.
Partner: UNT Libraries Government Documents Department
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Volatilization of Cesium During Calcination and Hydrolysis of Cs2ZnFe(CN)6 Precipitates

Description: The feasibility of removing and recovering cesium-137 from various HAPO process solutions by precipitation of Cs2ZnFe(CN)6 has been demonstrated previously. Pilot plant studies of calcination and steam hydrolysis of non-radioactive Cs2ZnFe(CN)6 precipitates by members of the Process Equipment Development Operation are currently in progress. In support of these pilot plant studies, experiments were performed to determine the extent, if any, to which cesium volatilizes during calcination and hydr… more
Date: March 23, 1960
Creator: Bouse, Donald G. & Schulz, Wallace W.
Partner: UNT Libraries Government Documents Department
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A Mathematical and Statistical Approach to the Design and Analysis of a Reactor Containment Vessel Pressure Test

Description: This report discusses the mathematical and statistical questions concerned with the estimation of a leak rate from data collected during a reactor containment vessel pressure test such as that performed on the PRTR vessel in May, 1959. A mathematical method is suggested in Section 3 for the construction of a total number of gas molecules in the containment vessel time series using vessel absolute pressure and temperature readings at several positions within the vessel. A formula for the precisi… more
Date: March 23, 1960
Creator: Nicholson, W. L.
Partner: UNT Libraries Government Documents Department
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Density and Hydrogen Content of Uranium Oxide Cakes and Slurries

Description: The work described was undertaken to provide data for nuclear safety studies concerning NPF reprocessing equipment. The original objective was to determine the uranium density and water (hydrogen) content of UO2-H2O mixtures ranging from compact centrifuge cakes to dilute slurries. The scope was later expanded to include mixtures of UO2 with hydrocarbon oil and mixtures of UO3-H2O.
Date: March 22, 1960
Creator: Amos, L. C.
Partner: UNT Libraries Government Documents Department
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The Pilot Plant Operation of a Vertical Tube, Recirculating Dissolver for the Dissolution of Uranium Dioxide in Nitric Acid

Description: The need for criticality control in the proposed reprocessing of slightly enriched non-production fuels at Hanford has led to the development of a geometrically "safe", vertical tube, recirculating dissolver. A study of the nitric acid dissolution of uranium dioxide in a pilot plant dissolver of this type is reported here. The study was pointed toward the comparison of uranium dioxide dissolution rates in a batch and a recirculating dissolver and the definition of hydraulic problems associated … more
Date: March 21, 1960
Creator: Smith, P. W.
Partner: UNT Libraries Government Documents Department
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Problems of a Small Leak Between the Flow Monitor and Heated Section of a PRTR Process Tube

Description: The result of a leak in a PRTR process tube between the flow monitor and the heated section would be to increase the flow through the monitor, but to decrease the flow through the heated section. The concern for the case of small leaks is whether the increase in flow through the flow monitor is sufficient to cause a high flow tip and a reactor scram for the condition where the flow through the heated section is reduced to the point to cause excessive fuel element temperatures.
Date: March 15, 1960
Creator: Hesson, G. M.
Partner: UNT Libraries Government Documents Department
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Development of a Welding Process for Spire-Can Fuel Elements

Description: The components for the present aluminum clad, Al-Si bonded, internally and externally cooled (I & E), uranium fuel elements are composed of impact extruded cans and spire caps as shown in Figure 1. This type of component requires two impact extrusions; however, in December, 1957, J. E. Ruffin proposed another design of component in which there was only one impact extrusion. For this component, Figure 2, the spire was impact extruded as a part of the can.
Date: March 11, 1960
Creator: Hanson, G. R.
Partner: UNT Libraries Government Documents Department
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Reamed Rear Face Parker Fitting

Description: A study and tests of the feasibility and best method of reaming rear face Parker fittings has been made. Flow increase of 8 percent, based on maintaining the same front header pressure, can be obtained at B, D, and F reactors by reaming the rear Parker fittings to .610 inch and using existing rear face hardware. Tests indicate mechanical strength will not be significantly reduced, high frequency vibration will not be increased, and that methods of reaming are available.
Date: March 17, 1960
Creator: McCarthy, P. B.
Partner: UNT Libraries Government Documents Department
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Unique Fabrication Processes Applied to Fuel Cladding Materials

Description: The fabrication processes applied to nuclear fuels are subject to severe limitations because of the conditions imposed by the reactor environment. The combined problems of neutrons fluxes, high heat fluxes, corrosion by the coolant , and embrittlement by hydriding or similar reactions may be minimized through establishing rigorous materials and fabrication specifications for fuel and cladding.
Date: March 15, 1960
Creator: Bush, S. H.
Partner: UNT Libraries Government Documents Department
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The Preparation of Plutonium Powder by a Hydriding Process--Initial Studies

Description: Powder metallurgy is rapidly gaining importance as a means of fabricating nuclear fuel elements and other reactor components. It provides a convenient method for forming metals, unusual combinations of metals, and metal-ceramic combinations. The unique features of this technique which make it desirable for nuclear engineering purposes are the following:
Date: March 10, 1960
Creator: Stiffler, G. L. & Curtis, M. H.
Partner: UNT Libraries Government Documents Department
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Critical Pressure Ratio for a Nozzle with Two-Phase Fog Flow

Description: In many cases of analysis of two-phase flow in systems, considerable computation or program time could be saved if the critical pressures ratio were known. If a reservoir or plenum pressure is fixed, the usual computational procedure involves the assumption of several critical pressures and the generation of several momentum terms to find the applicable critical pressure ratio and thereby the critical flow. The formulation of an equation of state make it possible to compute critical pressure ra… more
Date: March 8, 1960
Creator: Love, W. J.
Partner: UNT Libraries Government Documents Department
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Glove Box Integrity Study

Description: The amount of dry air or inert gas supplied to a "one pass" glove box ventilation system is proportional to the glove box inleakage. Most glove boxes in the 234r5 Building are equipped with sundry attachments, each contributing to the inleakage. No individual leak rate date is available for these auxiliary components in the "as installed" condition. Nor is the effect of time upon the leak rates known. Knowledge of these values, or at least an indication of the order of magnitude of the leakage … more
Date: March 8, 1960
Creator: Ciccarelli, R. A.
Partner: UNT Libraries Government Documents Department
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The Blast Cleaning Process as an Aid to Visual Weld Inspection

Description: Late in 1958 it became apparent that some fuel elements were failing in the Hanford reactors as a result of water entering through the weld. The mode of entry appeared to be first through a void in the weld, then through a non-wet area or a train of voids in the braze, and finally to the uranium core. Defective closures of a similar nature were also typical of many fuel elements which have failed in the autoclaving operation as shown in Figure 1.
Date: March 9, 1960
Creator: Hanson, G. R.
Partner: UNT Libraries Government Documents Department
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Multi-Purpose Dissolver Information Manual

Description: The multi-purpose dissolver was designed to provide: 1. A critically safe vessel for dissolving uranium metal of enrichments up to one percent U-235. 2. A vessel which can be charged with fuel elements up to 10 feet long. 3. An off-gas arrangement which will eliminate return of ammonia to the dissolver during the Zirflex decladding process. 4. A vessel in which small charges can be dissolved without using extra chemicals. 5. A by-pass routing around the silver reactor during cladding removal.
Date: March 4, 1960
Creator: Simonds, H. P.
Partner: UNT Libraries Government Documents Department
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100-N Decontamination Facility Design Guide.

Description: Space has been reserved near the southeast corner of the 100-N Area for the 122-N Decontamination Facility. Previous correspondence between Burns and Roe, Inc and General Electric bae discussed various facilities which might be needed in the building. The concepts of the decontamination processes are under active development by research groups at Hanford. At present, there are several workable processes known; each one has one or more fairly serious drawbacks.
Date: March 8, 1960
Creator: Bainard, W. D.
Partner: UNT Libraries Government Documents Department
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A Study of the Wear and Galling of Various Fuel Element Support Materials on Autoclaved Zircaloy-2 Interim Report No. 2

Description: This is the second of two reports describing the phases of a study of the wear and galling of autoclaved Zircaloy-2 by various fuel element support materials. The first report (1) showed that increasing contact area between the autoclaved Zircaloy-2 support and the autoclaved Zircaloy-2 process tube will not significantly improve the fuel support performance, and that a large flat contact area between the fuel supports and the process tube would be impractical to endeavor to achieve and maintai… more
Date: March 1, 1960
Creator: Weber, J. W.
Partner: UNT Libraries Government Documents Department
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Preliminary Evaluation of Chlorine for Use as a Gas Cooled Reactor Safeguard*

Description: A coolant line rupture during operation of a high temperature gas cooled graphite moderated reactor would present a serious hazard. The reactor would immediately depressurize and a great deal of air would be introduced into the coolant stream. As the air passed over the graphite moderator a runaway oxidation reaction would probably ensue unless an adequate safety system were available. This investigation was designed to evaluate chlorine as a reactor safeguard to be used to control a runaway re… more
Date: March 8, 1960
Creator: Dahl, R. E.
Partner: UNT Libraries Government Documents Department
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PCTR Measurements of the EGCR Lattice Parameters

Description: Measurements of k∞, f, p, and ∈ have been performed in the PCTR in support of the EGCR Program. The values listed below were obtained for the 21.875-inch cell used in the PCTR measurements. They are for a nonabsorbing (helium or vacuum) atmosphere.
Date: March 30, 1960
Creator: Nichols, P. F.; Engesser, F. C. & Oakes, T. J.
Partner: UNT Libraries Government Documents Department
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A Note Concerning the "100% Value" in Iron Absorption Studies by Whole Body Counting

Description: The evaluation of iron absorption using a single crystal whole-body counter is complicated by the inherent difficulty of determining a correct "100% value". Shortly after ingestion, tracer radioiron can be found in the stomach, upper small intestine, portal circulation and liver. Fourteen to twenty days later, the time at which absorption is measured most effectively, the radioiron will be distributed between the red cell mass, liver, spleen, bone marrow and other storage areas. With this mixed… more
Date: March 26, 1963
Creator: Schiffer, L.; Price, D. C.; Cuttner, J.; Cohn, S. H. & Cronkite, E. P.
Partner: UNT Libraries Government Documents Department
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