Tank 41H Saltstone Regulatory Analyses Page: 28 of 42
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WSRC-TR-2004-00051
Revision 0Date: 01/30/04
D H E C
LABORATORY:
PROMOIL PRILC1 P905PLR
So-h Ca-rhnaDeparmentofHeaIh METHOD NAME:
andEn onmenta1Control SUBJECT:BWXS - NELS
SW-846-6010B, SW-846-9056, SW-846-7470A, and Alpha Counting
QA- Blk, Laboratory Control Sample (LCS), Matrix Spike (MS), Matrix Spike Duplicate (MSD)Reference: Industrial Inorganic TCLP/R.61-58.5
Instrument: BWXT - Miscellaneous
Analyte Concentrations, mg / I Recovery Percent Flags
Analytes RDL MDL Blank LCS LCSD MS MSD Other LCS LCSD MS MSD Ave MS/MSD REC Limits % RPD RPD Limits -
Antimony 0.006 0.028 <0.025 1.00 - 1.00 1.00 - 99.1 - 86.3 86.5 86.4 75-125 1.7 10% -
Arsenic 0.01 0.012 <0.011 1.00 - 1.00 1.00 - 99.2 - 86.8 86.5 86.6 75-125 0.3 10% -
Barium 2 0.0012 0.025 1.00 - 1.00 1.00 - 97.6 - 76.2 75.5 75.8 75-125 0.8 10% -
Beryllium 0.004 0.00017 0.0002(B) 1.00 - 1.00 1.00 - 100.0 - 83.1 82.2 82.7 75-125 1.1 10% -
Cadmium 0.0050 0.0016 0.0016(B) 1.00 - 1.00 1.00 - 99.5 - 79.9 79.3 79.6 75-125 0.8 10% -
Chloride 250 25 <250 2000 - 2000 - - 93 - 92 - 92 75-125 0(A) 10% -
Chromium 0.1 0.0032 0.004(B) 1.00 - 1.00 1.00 - 99.7 - 78.6 78.1 78.3 75-125 0.6 10% -
Copper 1.3 0.0059 0.020(B) 1.00 - 1.00 1.00 - 99.5 - 83.7 82.7 83 75-125 1.1 10% -
Cyanide 0
C a ie 0.2 - - - - - - - - - - - - - - --
(as free c anide ___ ___ ___
Fluoride 4 12 509 2000 - 2000 - - 88 - 86 - 86 75-125 1.2(A) 10% -
Iron 0.3 0.0051 0.045(B) 1.00 - 1.00 1.00 - 105.0 - 69.0 67.7 68 75-125 1.7 10% N
Lead 0.015 0.028 <0.025 1.00 - 1.00 1.00 - 100.0 - 76.8 78.5 78 75-125 2.2 10% -
Manganese 0.05 0.0012 0.006(B) 1.00 - 1.00 1.00 - 97.3 - 76.4 75.9 76.1 75-125 0.6 10% -
Mercury 0.002 0.00014 0.012(B) 0.00471 - 0.0050 0.0050 - 107.6 - 106.9 105.9 106 75-125 0.9 10% -
Nitrate
as10 9 <56 452.00 - 452.00 92 75 - 75 75-125 1.3(A) 10% -
Nitroen 10 16 <76 610.00 - 610.00 - - 94 - 98 - 98 75-125 8.9(A) 10% -
Nitrate/Nitrite 10 16 <132 1062.00 - 1062.00 - - 93 - 77 - 77 75-125 1.4(A) 10% -
(Total) ___
Selenium 0.05 0.028 <0.025 1.00 - 1.00 1.00 - 98.5 - 90.4 88.5 89 75-125 1.8 10% -
Silver 0.1 0.0054 0.0052(B) 1.00 - 1.00 1.00 - 98.3 - 80.9 80.5 80.7 75-125 0.5 10% -
Sulfate 250 41 <250 2000 - 2000 - - 93.0 - 90 - 90 75-125 7.0(A) 10% -
Thallium 0.002 - - - - - - - - - - - - - - - -
Aluminum 36 0.03 0.097(B) 1.00 - 1.00 1.00 - 96.9 - 31.7 30.1 30.9 75-125 1.7 10% N
Boron 3.3 0.018 0.12(B) 1.00 - 1.00 1.00 - 103.0 - 92.9 89.0 91 75-125 3.1 10% -
Cobalt 2.2 0.0026 <0.0023 1.00 - 1.00 1.00 - 101.0 - 79.2 79.1 79.2 75-125 0.2 10% -
Lithium 0.73 0.011 <0.0097 1.00 - 1.00 1.00 - 105.0 - 113.9 114.7 114.4 75-125 0.4 10% -
Molybdenum 0.18 0.023 <0.021 1.00 - 1.00 1.00 - 103.0 - 96.7 93.6 95 75-125 2.3 10% -
Nickel 0.73 0.0069 <0.0062 1.00 - 1.00 1.00 - 102.0 - 79.4 79.7 79.6 75-125 0.3 10% -
Strontium, stable 22 0.0013 0.014 1.00 - 1.00 1.00 - 97.6 - 97.9 97.0 97.5 75-125 0.5 10% -
Uranium 7.3 0.000001 3.E-08 4.70E-07 - - - - 126 - - - - - 13 - -
(A) These RPD were determined from duplicate analyses of the same sample.23
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FERRARA, D. Tank 41H Saltstone Regulatory Analyses, report, April 15, 2004; South Carolina. (https://digital.library.unt.edu/ark:/67531/metadc780578/m1/28/: accessed July 17, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.