A Rapid Method for Determination of Water in TO₃

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Description

Summary: A set of conditions is described for a ten minute determination of water in TO₃ by ignition and absorption of the evolved water in magnesium perchlorate. Complete conversion to T₃O₃ is obtained under these conditions, so that total loss on ignition and total T (plus non-volatile impurity) content may also be obtained. It has been found unnecessary to employ Cu foil to prevent interference by nitrates, which may be present with a nitrate/water ratio as high as 5, and in an amount that does not exceed 100 mg.

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12 p.

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Barash, Bernard B.; Lee, Franklin B. & Curtiss, Edgar O. February 16, 1945.

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  • Main Title: A Rapid Method for Determination of Water in TO₃
  • Series Title: Atomic Energy Commission Reports
  • Added Title: Atomic Energy Commission Report AECD-3898

Description

Summary: A set of conditions is described for a ten minute determination of water in TO₃ by ignition and absorption of the evolved water in magnesium perchlorate. Complete conversion to T₃O₃ is obtained under these conditions, so that total loss on ignition and total T (plus non-volatile impurity) content may also be obtained. It has been found unnecessary to employ Cu foil to prevent interference by nitrates, which may be present with a nitrate/water ratio as high as 5, and in an amount that does not exceed 100 mg.

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12 p.

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Digitized from microopaque cards (1).

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  • OCLC: 911538127
  • SuDoc Number: Y 3.AT 7:22/AECD-3898
  • Report No.: AECD-3898
  • Archival Resource Key: ark:/67531/metadc172972

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Technical Report Archive and Image Library

The Technical Report Archive & Image Library (TRAIL) identifies, acquires, catalogs, digitizes and provides unrestricted access to U.S. government agency technical reports. The mission of TRAIL is to ensure preservation, discoverability, and persistent open access to government technical publications regardless of form or format.

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Imaged from microcard, these technical reports describe research performed for U.S. government agencies from the 1930s to the 1960s. The reports were provided by the Technical Report Archive and Image Library (TRAIL).

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  • February 16, 1945

Added to The UNT Digital Library

  • Feb. 12, 2018, 7:42 a.m.

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  • April 23, 2019, 7:34 p.m.

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Barash, Bernard B.; Lee, Franklin B. & Curtiss, Edgar O. A Rapid Method for Determination of Water in TO₃, report, February 16, 1945; [Oak Ridge, Tennessee]. (https://digital.library.unt.edu/ark:/67531/metadc172972/: accessed June 6, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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