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Analytical Chemistry of the Polyphosphates

Description: Additional data were obtained on the separation of linear polymers from cyclic polymers by precipitation with barium chloride. An unexpected peak was observed in the anion-exchange chromatography of a sodium poly-phosphate of n-bar average degree of polymerization) = 6, and the compound represented by this peak was isolated. An end-group titration of this compound by microtechnique proved unequivocally that it is a cyclic phosphate. Although the identification (number of phosphorus atoms per mo… more
Date: October 17, 1961
Creator: Rieman, W., III & Rothbart, H. L.
Partner: UNT Libraries Government Documents Department
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CLOSE-CAPTURE ABSORPTION SYSTEM FOR REMOTE RADIOISOTOPE CHEMISTRY

Description: Molecular sieves are used as the basic adsorber in a close-capture air recirculation system designed primarily for remote operation with master-siave equipment. A compact evaporator-dissolver unit provides a vessel for dissolution of an Al slug containing the radioactive material and provides an evaporator head under which volume reduction may be carried out within a specially prepared centrifuge cone. One movable condenser serves both operations. Resistance films of Pt provide heat for the cen… more
Date: August 17, 1961
Creator: Spencer, Neil C.; Parsons, Thomas C. & Howe, Patrick W.
Partner: UNT Libraries Government Documents Department
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Close-Capture Adsorption System For Remote Radioisotope Chemistry

Description: Molecular sieves are synthetic zeolites which, when dehydrated, contain a network of empty pores and cavities that constitute almost 50% of the total volume of the crystals. They have the unique property of adsorbing within these cavities only those molecules that are small enough to pass through the pores of the crystals, Molecular sieves have a very strong affinity for water and other polar molecules. It is this selective property plus their stability and reasonable cost that make them of int… more
Date: August 17, 1961
Creator: Spencer, Neil C.; Parsons, Thomas C. & Howe, Patrick W.
Partner: UNT Libraries Government Documents Department
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Comparison of Radiation-Induced Graft Copolymerization Untilizing Electron Accelerators and Isotope Sources as Radiation Initiators

Description: "A brief examination of the post irradiation grafting of machine irradiated polyethylene film with acrylic acid monomer was made. Evidence of postgrafting was detected in samples that had been irradiated to a total dose of 10 Mrads at a dose rate of 0.01 Mrad/sec. and then exposed to a 25% purified acrylic acid solution in benzene for periods of 1 to 4 days."
Date: October 17, 1961
Partner: UNT Libraries Government Documents Department
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"Crud" Scrubbing with a Purex-Type Zebra Cartridge

Description: Entrained solids have in the past been one of the major factors limiting solvent extraction fission product decontamination. These solids are known to be surface active, to absorb fission products, and to form interfacial films or "cruds". A major step in eliminating these cruds was taken when the Purex columns were modified to operate with the interfaces at the waste ends of the columns rather than the product ends. This type of operation tended to flush the solids out with the waste rather th… more
Date: October 17, 1961
Creator: Richardson, G. L
Partner: UNT Libraries Government Documents Department
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Current-Switching Circuitry

Description: This paper discusses a group of high-speed switching circuits using the basic current-switching mode of operation. The first part of the paper presents a dynamic analysis of the basic current-switching mode and the second part is the dynamic and steady-state analysis of a current-switching flip-flop.
Date: July 17, 1961
Creator: Salvador, Jack Gilbert & Pederson, D. O.
Partner: UNT Libraries Government Documents Department
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THE CYCLOTRON RESONANCE INSTABILITY WITH NEGATIVE MASS IONS

Description: Both the effect of resonant coupling of ion cyclotron motion to electron plasma oscillations, as previously discussed by Harris, and the effect of a negative radial gradient in a magnetic mirror field, the so-called "negative mass'' effect, were combined in an approximate calculation for the threshold for electrostatic instability in DCX. The two mechanisms for instability were found to act more or less independently. (auth)
Date: October 17, 1961
Creator: Fowler, T.K. & Harris, E.G.
Partner: UNT Libraries Government Documents Department
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Decay-Energy Systematics Of The Heavy Elements

Description: Figures 1 and 2 summarize total decay energies for the four radioactive series. The alpha-decay energy obtained by measuring the energy of the alpha particle leading to the ground state includes the energy of the recoil nucleus. The curve shown in figure 3 defines in broad outline the conditions and regions of alpha instability. A great deal more is to be learned from a more detailed examination of the region where alpha radioactivity is prominent. Of great value to the experimentalist is that … more
Date: January 17, 1961
Creator: Perlman, Isadore & Asaro, Frank
Partner: UNT Libraries Government Documents Department
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The Design and Operation of Purex Process Pulse Columns

Description: Information on the development of pulse columns for the Purex Process is presented in order to indicate qualitutively the performance attainable with improved cartridge designs, and to show some of the factors involved in scaling up pilot plant results to full plant scale. The pulse columns were designed to produce separated uranium and plutonium products decontaminated by at least a factor of 10>s7/sup /om fission products, with average uranium and plutonium losses of less than 0.2% per column… more
Date: February 17, 1961
Creator: Richardson, G. L.
Partner: UNT Libraries Government Documents Department
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Development of High-Temperature Strain Gages

Description: From Introduction: "An improved high-temperature gage was needed, and in an attempt to fill this need an investigation was initiated in February 1954 in the Enameled Metals Laboratory at the National Bureau of Standards. The present Monograph constitutes a final summary on this program."
Date: March 17, 1961
Creator: Pitts, J. W. & Moore, D. G.
Partner: UNT Libraries Government Documents Department

[Egg Scrambled Over Skillet by Slingshot John Milligan]

Description: Photograph of Slingshot John Milligan scrambling an egg dropped over a skillet. In the image a lady on the left is holding a skillet under an egg that Milligan has shot through with a slingshot while it was in mid-air. John Milligan, a machinist in Detroit, Michigan who was also the “country’s greatest slingshot expert. “He won local fame by shooting the marks out of playing cards, hitting objects in mid air and bagging game in the field.” Joe took John national with his photos documenting his … more
Date: January 17, 1961
Creator: Clark, Joe
Partner: UNT Libraries Special Collections

[Egg Scrambled Over Skillet by Slingshot John Milligan (1)]

Description: Photograph of John Milligan shooting an egg that was being dropped over a skillet. In the image a waitress on the left is holding a skillet under an egg that Milligan has shot through with a slingshot while it was in mid-air. John Milligan, a machinist in Detroit, Michigan who was also the “country’s greatest slingshot expert. “He won local fame by shooting the marks out of playing cards, hitting objects in mid air and bagging game in the field.” Joe took John national with his photos documenti… more
Date: January 17, 1961
Creator: Clark, Joe
Partner: UNT Libraries Special Collections

[Egg Scrambled Over Skillet by Slingshot John Milligan (2)]

Description: Photograph of John Milligan shooting an egg that was being dropped over a skillet. In the image a waitress on the left is holding a skillet under an egg that Milligan has shot through with a slingshot while it was in mid-air. John Milligan, a machinist in Detroit, Michigan who was also the “country’s greatest slingshot expert. “He won local fame by shooting the marks out of playing cards, hitting objects in mid air and bagging game in the field.” Joe took John national with his photos documenti… more
Date: January 17, 1961
Creator: Clark, Joe
Partner: UNT Libraries Special Collections
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Evaluation of Some Integrals Arising in the Theory of Ionized Gases

Description: In some recent theories of the equation of state of classical ionized systems, the free energy depends on integrals of the form {integral}{sub 0}{sup {infinity}}[e{sup -{beta}V{sub s}}-1+{beta}V{sub s}-{beta}{sup 2}V{sub s}{sup 2}/2]r{sup 2}dr, where V{sub s} is a "screened" potential obtained from the real potential by summing certain infinite series of diagrams. This integral has been tabulated for V{sub s} appropriate to a potential {+-}(e{sup 2}/ r)(1 - e{sup -{gamma}r}). The equation of st… more
Date: May 17, 1961
Creator: Trulio, J. G. & Brush, S. G.
Partner: UNT Libraries Government Documents Department
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Fabricating Liquid-Hydrogen Targets From Mylar

Description: The increasing popularity of liquid-hydrogen targets in physics research has emphasized the need for containers with maximum beam transparency (i.e., thin walls and low Z) and suitable strength at cryogenic temperatures. Fabrication of a Mylar container satisfying these requirements is described here.
Date: August 17, 1961
Creator: Mehr, David L.
Partner: UNT Libraries Government Documents Department
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Fractional heat generation rates in Hanford reactors after shutdown

Description: The knowledge of the fraction of decay-heat which is absorbed in fuel elements after a reactor is shutdown is important for many reasons. For example, allowable, reduced flow-rates after shutdown are very sensitive to the manner in which the decay-heat is distributed. Also, the temperature-rise in a discharged, uncooled fuel element is dependent on the total heat generated in the slug. Apart from any heat consideration, the escape of rays from a discharged fuel element is also of importance in … more
Date: May 17, 1961
Creator: Nilson, R. & Meichle, R. H.
Partner: UNT Libraries Government Documents Department
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Heavy-Ion Elastic Scattering

Description: The elastic scattering of C/sup 12/ ions from Ar, Fe, Ni, Ag/sup 107/ In, and Ta was measured as a function of angle, at a laboratory-system energy of 124.5 Mev with the Berkeley heavy-ion linear accelerator. The experimental equipment and techniques are discussed. The angular distributions show the same general behavior as previous heavy-ion elastic scattering experiments. The experimental data were analyzed with the semiclassical Blair model as modified by McIntyre. Very good agreement with e… more
Date: April 17, 1961
Creator: Alster, Jonas
Partner: UNT Libraries Government Documents Department
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Interim Report on Corrosion by Zirconium-Base Fluorides

Description: Report issued by the Oak Ridge National Laboratory discussing studies conducted on corrosion by fluorides. Equipment, procedures, results, and analysis is presented. This report includes tables, illustrations, and photographs.
Date: January 17, 1961
Creator: Adamson, G. M.; Crouse, R. S. & Manly, W. D.
Partner: UNT Libraries Government Documents Department
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Internal Conversion Coefficients of the 2+-0+, E2 Transitions in Even-Even Sm152[over]90 and Gd152[over]88

Description: From abstract: "To investigate the deviation of the internal conversion coefficients of E2 transitions from theoretical computations and their dependence on nuclear deformation, the total internal conversion coefficient of the 121.8-kev 2+-0+ transition in ellipsoidal Sm152[over]90 was measured to be 1.135 ± 0.010 with a high accuracy coincidence-sum method. The K-shell to total internal conversion ratio was determined to be 0.588 ± 0.003 with a [beta] spectrometer...The experiment revealed no … more
Date: July 17, 1961
Creator: Lu, D. C. & Schupp, G.
Partner: UNT Libraries Government Documents Department
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Irradiation Processing Department monthly report, October 1961

Description: This document details activities of the irradiation processing department during the month of October, 1961. A general summary is included at the start of the report, after which the report is divided into the following sections: Research and Engineering Operations; Production and Reactor Operations; Facilities Engineering Operation; Employee Relations Operation; and Financial Operation.
Date: November 17, 1961
Partner: UNT Libraries Government Documents Department

[Joe Clark and Ron Unternahrer Toss Up a Target Egg for Slingshot Milligan]

Description: Photograph of Joe Clark and Ron Unternahrer tossing up a target egg for Slingshot Milligan to shoot. In the image both men are wearing towels around their necks from the splattered egg matter. The two men are practicing the height of the egg being tossed in the air for the photograph they are making where Milligan shoots the egg with a Milligan Special slingshot. Narrative by Junebug Clark: This is truly a behind the scenes or a how it was done photo. At 25 paces that egg is a pretty small movi… more
Date: January 17, 1961
Creator: Clark, Joe
Partner: UNT Libraries Special Collections
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