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A Study of Thorium Peroxide Sulfate

Description: Abstract. Thorium peroxide was precipitated from thorium nitrate solutions containing varying amounts of sulfate ion and of hydrogen ion. The washed solids were analyzed both wet and dry. Analyses were made for thorium, peroxide oxygen, sulfate, nitrate, and water contents. X-ray powder photographs of the dried samples by W.H. Zachariasen showed the presence of only two phases. When precipitated from high sulfuric acid, the solid phase was isomorphous with Th(OO)SO4.3H20. More weakly acid … more
Date: October 1, 1945
Creator: Hamaker, John W.
Partner: UNT Libraries Government Documents Department
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Recovery of D2O and UO2F2 by Distillation

Description: Technical report describing the purification and separation by distillation of UO2F2 from D2O. In the experiment which is discussed 2,129.6 lbs of UO2F2 were dissolved in 6,605 lbs of D2O. The average isotopic purity of the D2O decreased during the distillation from 99.77% to 99.73%. The dissolved impurities were less than those present originally in the heavy water.
Date: October 10, 1945
Creator: Fischer, R. & Wattenberg, Albert, 1917-
Partner: UNT Libraries Government Documents Department
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Precipitation of Thorium Oxalate from Nitric Acid Solutions

Description: Introduction. It has been known for a long time that thorium is precipitated by oxalic acid in acid solutions, but a survey of the literature showed no study of the limits of the acidity and oxalic acid excess which yield quantitative results. V. I. Spitzin reports on the solubility of thorium oxalate in varying concentrations of several acids, but the effect of an excess oxalic acid is not included. Since solutions are sometimes presented for analysis that contain more than the recommended … more
Date: October 5, 1945
Creator: Ayers, A. S.
Partner: UNT Libraries Government Documents Department
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Analysis of Uranium-Manganese Alloys

Description: Introduction. the conventional procedures of analysis for uranium and manganese can be employed in the analysis of alloys of these metals. The alloys are reacted with perchloric acid and hydrogen peroxide, fumed to remove any chloride ions, diluted to volume and aliquots analyzed by redoximetry.
Date: October 5, 1945
Creator: Ayers, A. S.
Partner: UNT Libraries Government Documents Department
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Range of U235 Fission Fragments in Photographic Emulsion

Description: From abstract: "A fine-grain emulsion has been found which is sensitive only to the densely ionizing fission fragments. This emulsion was soaked in uranyl acetate and exposed to slow neutrons. The ranges in the emulsion of about four-hundred fission fragments were measured. The resulting distribution shows a sharp maximum at 23 microns of emulsion. No ternary fissions or large-angle scattering of fragments were observed."
Date: October 17, 1945
Creator: Richards, H. T.
Partner: UNT Libraries Government Documents Department
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Procedure for improving temperature distribution via rods and columns -- B Pile

Description: Since the development of relationships between rod changes and temperature shifts, the temperature distribution of the B Pile has been improved as much as possible by shifting the rods. Certain unbalances have been found which can only be removed by improvement of the poison pattern. At present the maximum imperfection in the B Pile is 5% diagonal quadrupole unbalance. An estimate of the poison pattern needed to correct these imperfections is given herein. This poison pattern has been calculate… more
Date: October 5, 1945
Creator: Menegus, R. L.
Partner: UNT Libraries Government Documents Department
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Consolidation and shaping of boron ; summary of previous work

Description: From abstract: "The deposit on the rods is in the form of a brittle uneven tube which is cracked off and subsequently pulverized to a 200-mesh powder. This report is chiefly concerned with methods of consolidating this powder and shaping it into forms required, though it also discusses to some extent other methods of shaping boron or born-rich materials."
Date: October 8, 1945
Creator: Kamm, Robert L.
Partner: UNT Libraries Government Documents Department
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The Production of Ceramic Ware by Slip-Casting

Description: This report discusses the production of ceramic ware through the process of slip-casting. The report separately describes the processes of creating zirconia ware, beryllia ware, alundum ware, thoria ware, and specially shaped ceramic ware.
Date: October 20, 1945
Creator: Calderwood, Wayne
Partner: UNT Libraries Government Documents Department
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Preparation and Stability of Cobalt Trifluoride

Description: Report discussing the preparation, stability, and recommended storage of cobalt trifluoride. "Cobalt trifluoride prepared by the action of fluorine upon anhydrous cobalt dichloride remains stable when kept in sealed glass tubes but on exposure to air it absorbs water and its use in the conversion of T3O8 to TF6 cannot be relied upon..."
Date: October 15, 1945
Creator: Whitney, J.; Smith, Fred & Miller, A. J.
Partner: UNT Libraries Government Documents Department
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Equations Used for Calculation of Data by the Feedback Method

Description: The following report studies a method of assay where an unknown sample is determined by comparison with a standard sample of known isotopic ratio. The purpose is to acquaint the technical personnel with the fundamentals of the feedback method of assaying samples of TF6.
Date: October 26, 1945
Creator: Happ, G. P. & Cameron, A. E.
Partner: UNT Libraries Government Documents Department
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July 16th nuclear explosion: Permanent earth displacement

Description: A measurement was made of the permanent earth movement in the neighborhood of the tower caused by the nuclear explosion at Trinity. The crater was apparently formed by a compression phenomenon and was noted to be much shallower than craters formed by ordinary high explosives. Scaling up existing information on the radius of craters, the TNT equivalence of the nuclear bomb is given as 10,000 tons to within 50 percent. Observations were made on the damage in the crater region and suggestions are … more
Date: October 3, 1945
Creator: Reines, F.
Partner: UNT Libraries Government Documents Department
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Correlation of exhaust-valve temperatures with engine operating conditions and valve design

Description: Report presenting a theory regarding engine-cooling variables from a previous report, which was used as a basis for the development of a semi-empirical equation to correlate exhaust-valve temperature with engine conditions. Results regarding the determination of constants, influences of operating variables on mean effective gas temperatures, thermal-resistance factor, and accuracy of correlating equation are provided.
Date: October 1945
Creator: Zipkin, M. A. & Sanders, J. C.
Partner: UNT Libraries Government Documents Department
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