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Hanford Neptunium Oxalate-Oxide Process Experience

Description: In recent months, relatively large quantities of neptunium-237 have been recovered from Hanford irradiated uranium. The over-all recovery process consisted of 1) isolation from Purex plant solutions by solvent extraction, to yield an impure neptunium nitrate solution contaminated principally with uranium, plutonium, and fission products (2) purification by anion exchange 3) precipitation of neptunium (IV) oxalate; and 4) calcination of the oxalate to yield neptunium (IV) oxide, NpO2. This paper… more
Date: July 1, 1959
Creator: Pollock, C. W. & Schneider, R. A.
Partner: UNT Libraries Government Documents Department
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PRTR Single Tube Prototype Mockup (STPM) Operational Characteristics

Description: The Single Tube Prototype Mockup (STPM) was constructed to be used as a tool to evaluate the mechanical problems involved in operating and maintaining many components of the Plutonium Recycle Test Reactor (PRTR). This report has been written to acquaint interested HAPO components with the capability of the STPM and for use as an aid in scheduling tests and/or to properly evaluate testing results obtained from the mockup.
Date: July 2, 1959
Creator: Scott, P. A.
Partner: UNT Libraries Government Documents Department
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Quarterly Report of Non-Production Reactor Fuels Reprocessing Budget Activity 3790

Description: This report summarizes the research and development work carried out during March, April and May, 1959, for Budget Activity 2790 - Separations Development for Non-Production Reactors, The effort on Activity 2790 will enable Hanford to begin reprocessing in January, 1962, the fuel elements from power reactors which employ depleted or slightly enriched uranium fuels.
Date: July 2, 1959
Creator: Cooper, V. R.
Partner: UNT Libraries Government Documents Department
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PRTR Hazard Analysis For Various Mechanical Failures

Description: The hazards associated with several possible mechanical failures were analyzed for the PRTR. The consequences of these failures were evaluated for inclusion in the Final Hazards Summary Report.
Date: July 6, 1959
Creator: Muraoka, J.
Partner: UNT Libraries Government Documents Department
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Heat Transfer Testing

Description: Several tests are being performed and others being planned to investigate the role of heat transfer in corrosion processes. These tests are measuring both corrosion rates of metals (Zr-2 and X-8001 aluminum) under heat transfer, and the temperature rise associated with the buildup of the corrosion product. A brief description of these tests is given in this report.
Date: July 7, 1959
Creator: Doman, D. R.; Hokenson, J.F. & Lobsinger, R. J.
Partner: UNT Libraries Government Documents Department
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Neutron Age Calculations. (Homogeneous Systems)

Description: In an earlier study on criticality conditions for homogenous mixtures, 2/cm^2 was used as the neutron age for all mixtures of water and uranium. At the higher H/U ratios (low uranium concentration), the calculated critical parameters were in good agreement were in good agreement with experimental data. At the low H/U ratios (high uranium concentrations) the calculated critical parameters were smaller than the experimental ones (more conservative from a nuclear safety point view). These results … more
Date: July 10, 1959
Creator: Ketzlach, N.
Partner: UNT Libraries Government Documents Department
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The Operation and Maintenance of an Alpha Energy Analyzing System

Description: The measurement of a alpha-particle energy has been used by many radiochemical laboratories for the identification and analysis of alpha-active radio nuclides. The use of the total-ionization method for alpha-active radio-nuclides. The use of the total-ionization method for alpha energy in ionization chamber in which the alpha particle loses all its energy in ionization of the chamber gas. Collection of the electrons thus formed generates a voltage pulse across the chamber capacity which is pro… more
Date: July 10, 1959
Creator: Brauer, F. P. & Connally, R. E.
Partner: UNT Libraries Government Documents Department
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Division of Reactor Development Programs Monthly Reports-June 1959

Description: Basic Studies. Sinterability experiments in the system UO2-PuO2 have continued, and data are available at one hour hold times across the UO2-PuO2 composition limits. Sintered densities appear to be markedly dependent on pressed densities with densification occurring very rapidly at higher pressing pressures. The following table illustrates the effect of one hour at temperature on final density for pure plutonium dioxide pressed to both 40 and 60 percent of theoretical density.
Date: July 15, 1959
Creator: Lewis, M.
Partner: UNT Libraries Government Documents Department
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Recovery of Plutonium and Neptunium from Purex IWW by Anion Exchange

Description: The recovery of plutonium and neptunium by anion exchange has been well demonstrated on a laboratory scale. (1, 2,3,4) The specific adsorbed by the resin is the tetravalent hexanitrate complex of either element. With plutonium (IV) and neptunium(V) in IWW, the plutonium is adsorbed but the neptunium is not. If nitrite is used as the reductant in strong (preferably 8 M or over) nitric acid, both plutonium and neptunium are obtained in the tetravalent state, and both are adsorbed on the resin. Wi… more
Date: July 16, 1959
Creator: Van Tuyl, H. H.
Partner: UNT Libraries Government Documents Department
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An Aqua Recia Flowsheet for Uranium Dissolution

Description: Relatively long time cycles are required for the standard nitric acid dissolution of enriched uranium using safe batch size techniques for criticality control. Upwards of forty eight hours are required for the total dissolution of solid of I and E enriched slugs in nitric acid. The dissolution capacity may be increased by: (1) using a dissolver critically safe by virtue of its geometry or, (2)increasing the rate of uranium dissolution. Dilute agua regia -- a mixture of hydrochloric and nitric a… more
Date: July 21, 1959
Creator: Shefcik, J. J.
Partner: UNT Libraries Government Documents Department
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A Remote Phase Separation Bulb for Highly Radioactive Sample Analyses

Description: Extraction systems involving chelating agents are widely used in radiochemical separations on a control basis due to the economy in time and equipment. In the case of waste streams, the element of interest is, by definition, at a very low concentration in the presence of gross fission product activities. The resultant large sample size necessary for a reliable analytical results creates a marked radiation hazard to laboratory personnel.
Date: July 21, 1959
Creator: Campbell, M. H.
Partner: UNT Libraries Government Documents Department
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Stack Effluent Monitor Operation and Maintenance

Description: The Stack Effluent Radioisotope Monitor is an instrument which continuously measures and records the amounts of each of several different radioactive isotopes in the stack effluent of the Redox Facility. An informal report, HW-56151, describing the theory of operation and the circuits was prepared and is available to Hanford personnel from the technical files. The formal report, HW-56151 Rev, containing essentially the same information, is available from the Office of Technical Services, Depar… more
Date: July 21, 1959
Creator: Harvey, R. A.
Partner: UNT Libraries Government Documents Department
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A Microspark Apparatus for the Study of Inclusions in Metals

Description: A study of metallurgical problems resulting from variation in grain boundaries, bonding layers, and inclusions in metals and alloys has become increasingly important over the past several years. To keep pace with and aid in these studies, several new techniques have been developed in emission and X-ray spectroscopy. In X-ray, areas as smalls as one square micron can be studied by making them targets for a focused electron beam and observing the X-rays emitted (5,2). Such an instrument would be … more
Date: July 22, 1959
Creator: Smith, F. M.
Partner: UNT Libraries Government Documents Department
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DC Bridge NPR Horizontal Rod Counting

Description: This report is a summary of work done for system development on the NPR ball safety backup for the horizontal rods. This phase of the system development is limited to discussion of the horizontal rod counting circuitry utilizing a direct current bridge network.
Date: July 24, 1959
Creator: {{{name}}}
Partner: UNT Libraries Government Documents Department
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Preliminary Chemical Flowsheets for the Decladding and Dissolution of Non-Production Fuels

Description: This document presents preliminary chemical flowsheets for cladding and core dissolution of zircaloy-clad uranium dioxide and stainless steel-clad uranium-molybdenum non-production fuels. These preliminary flowsheets together with existing process flowsheets should be adequate for process development in the currently forecast non-production fuels dissolution facility.
Date: July 24, 1959
Creator: Harmon, M. K.
Partner: UNT Libraries Government Documents Department
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Suggested Major Equipment for NPR Water Quality Control Labs

Description: Two water quality control labs are being provided for the the NPR. One, a "cold" lab, is located in the183 Building adjacent to the control room. Its primary purpose is to provide facilities for quality control of the output of the filter plant and the demineralizer plant. The other, a "hot" lab, is located in the 190 Building. Its primary purpose is to provide facilities for the quality control of the primary and secondary coolants, and the moderator coolant.
Date: July 30, 1959
Creator: Bainard, W. D.
Partner: UNT Libraries Government Documents Department
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Fabrication of the PRTR Zircaloy-2 High Pressure Process Tubes

Description: Development of a fabrication process and the manufacture of 95 PRTR process tubes demonstrates that the commercial fabrication of high quality Zircaloy-2 pressure tubing is feasible.
Date: July 31, 1959
Creator: Knecht, R. L.
Partner: UNT Libraries Government Documents Department
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PRTR Total Energy Distribution Calculations

Description: Since the calculation of the PRTR energy distribution was first carried out by J. R. Triplett, the design has become sufficiently fixed to allow a refinement of his values. The present analysis, also, includes a calculation of the fraction of energy which is released in the shroud and process tubers that flows to the primary coolant to the top and bottom shield coolant is taken into consideration. Nuclear data used in the original calculations still appears satisfactory and is, therefore, util… more
Date: July 31, 1959
Creator: Peterson, R. E.
Partner: UNT Libraries Government Documents Department
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