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Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Month Ending May 15, 1943

Description: Technical report that information has bee obtained on the effect of beta and gamma radiation on the electrical resistance of insulating materials The results are summarized. The recovery to original resistance values has been measured. In general, the initial rate is rapid for the first few hours; the rate then decreases sharply. Certain samples show evidence of complete recovery. Effects on mechanical properties of several plastics has also been studied. Data on gas evolution from severa… more
Date: May 15, 1943
Creator: Franck, J.
Partner: UNT Libraries Government Documents Department
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The Extraction of Uranium into Hexone as Uranyl Thiocyanate from Thorium Nitrate Solutions

Description: Technical report with six sections describing the process: (1) The reaction of HN)3 with HSCN; (2) The distribution of nitric acid between hexone and water; (3) The distribution of HSCN between hexone and water; (4) The solubility of thorium sulfate in various extraction solutions; (5) The distribution of protoactinium and fission elements between hexone and aqueous thiocyanate solutions; and (6) Separation of uranium from thorium by extraction into hexone as UO2(SCH)a.
Date: May 18, 1945
Creator: Reas, William H.
Partner: UNT Libraries Government Documents Department
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Preparation of U233

Description: Technical report. The object of the research is to determine the procedure and equipment for the preparation of U233 on a semi-works scale. The general proposed procedure is that thorium carbonate in aluminum cans will be irradiated with pile neutrons. The Pa233 resulting from neutron absorption the Th232 and the decay of Th233 will be extraction from 99% of the thorium and the natural U in thorium by MnO2 precipitations. The Pa233 will then be allowed to decay to U233 which in turn will be… more
Date: May 16, 1944
Creator: Apple, R. S.
Partner: UNT Libraries Government Documents Department
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Analysis for Oxide in Thorium Metal

Description: Abstract. to estimate the oxygen picked up by thorium in casting a rapid method of running the acid insoluble content was developed. the quickest procedure consists of reacting with mixed acids, fuming with perchloric and filtration to separate the "free" thorium from the "combined". The precipitate is ignited and weighed as thorium dioxide.
Date: May 12, 1945
Creator: Ayers, A. S.
Partner: UNT Libraries Government Documents Department
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Analysis of Heavy Water by Equilibration

Description: Technical report discussing that the deuterium concentration of heavy water can be determined by equilibrating the water with deuterium gas in the presence of a catalyst with subsequent analysis of the equilibrated gas on the mas spectrometer. The apparatus for equilibration analyses maybe be considered in three parts: 1) apparatus for introducing the ingredients into the reaction chambers; 2) the reaction chambers; 3) the mass spectrometer for analysis of the equilibrated gas. The isotopic co… more
Date: May 15, 1945
Creator: Fischer, R. B.; Potter, R. A. & Voskuyl, R. J.
Partner: UNT Libraries Government Documents Department
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The Preparation of High-Purity Beryllium Oxide

Description: Abstract. A method for the preparation of beryllium oxide of high purity is presented. Beryllium basic acetate (BeO-3Be(C2H3O2)2) is prepared from the metal or a convenient salt, a chloroform solution of this material extracted with redistilled water, the dried basic acetate distilled in a quartz apparatus, and this purified material converted to the oxide by fuming down with sulfuric acid and igniting at 1000 degrees C. Impurities detectable spectrographically were reduced to a very low leve… more
Date: May 27, 1946
Creator: Tomkins, F. S.; Cressman, G. W. & Tolmach, L. J.
Partner: UNT Libraries Government Documents Department
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Metallurgical Laboratory, Chemical Research - Heavy Water, Report for the Month Ending May 1, 1944

Description: Technical report with short reports on (1) Heavy water analysis and standardization, and Specific gravity of pure D2O; (2) Homogenous exponential experiment; (3) Recombination of pile gases; (4) Slurry pumping studies; and (5) Electron microscope laboratory.
Date: May 16, 1944
Creator: Hogness, T. R. (Thorfin Rusten), 1894-; Hiskey, C. F. & Eidinoff, Maxwell Leigh, 1915-
Partner: UNT Libraries Government Documents Department
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