Heteronuclear probes of coal structure and reactivity. Quarterly report, July--September 1993
Description:
The most exciting finding in this quarter is the quantitative removal of sulfur from Illinois No. 6 coal using PBu{sub 3}. In previous quarterly reports we described the removal of 92% sulfur by refluxing a suspension of Illinois No. 6 in PBu{sub 3} for two days. The secret for quantitative removal (98.7%, run 1 in Table I) is to place the coal sample under vacuum, then adding the PBu{sub 3} while the sample is still under vacuum and finally raising the pressure of the system to atmospheric wit…
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Date:
October 31, 1993
Creator:
Verkade, J. G. & Hall, G.
Partner:
UNT Libraries Government Documents Department