Description: Five batches of unplasticized AFNOL, each approximately one pound, were synthesized using 4,4-dinitropimelic acid as the starting material. Two 10 g batches were completed prior to the pound batches to assure the usability of the acid chloride. Characterization of each of the larger batches was by differential thermal analysis (DTA), infrared spectrophotometry (IR), and cure tests. Some characterization was also done on the commercial chemicals used in the synthesis.
Date: December 31, 1972
Creator: Quinlin, W.T.
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