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Chemical Technology Division Unit Operations Section Monthly Progress Report, September 1961

Description: Nine samples of ThO/sub 2/ -UO/sub 2/ prepared as part of the solgel process development studies showed no consistent effects from small variations in several process parameters. The reaction of methane and copper oxide was studied. Engineering studies of the continuous dissolution of simulated U-Zr-Sn fuels in 6.5 M NH4F, 0.6-1.0 M NH/sub 4/NO/sub 3/, 0.1 M H/sub 2/O/sub 2/ were continued in modified 6-in.-dia. equipment. A total of 1642 kg of U from NaK bonded SRE Core I fuel rods wad dejacke… more
Date: April 1, 1962
Creator: Whatley, M. E.; Haas, P. A.; Horton, R. W.; Ryon, A. D.; Suddath, J. C. & Watson, C. D.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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HRT CORROSION SAMPLES--ADDITIONAL DATA ON SPECIMENS REMOVED PRIOR TO RUN NO. 20

Description: Results of the examinations of corrosion specimens exposed in the HRT are presented. Specimens examined include core screen samples, core specimen array No. 1, blanket specimen array No. 2, core solution line specimen arrays No. 103 and 103A, and blanket solution line specimen array No. 203. These data include corrosion rates, computed from specimen weight-changes, and results of chemical analyses of scales removed from the specimens or specimen holders. A summary is included of the HRT operati… more
Date: February 1, 1961
Creator: Baker, J.E.; Silverman, M.D.; Jenks, G.H. & Olsen, A.R.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Startup and Initial Testing of SM-1 Core II With Special Components

Description: The loading operation for SM-1 Core II is described. Results of startup physics measurements (Test A-300 (Series) and fission product iodine monitoring in the primary coolant are given. The SM-1 Core II initial loading progressed satisfactorily, fulfilling the predictions of the zero power experiment performed at the Alco Criticality Facility. The initial cold clean five rod bank position was 6.53 in.; the initial hot, no xenon, five rod bank position was 9.62 in.; the initial hot, equilibrium … more
Date: February 28, 1962
Creator: Moote, F. G. & Schrader, E. W.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Magnetic Properties of Insulators. Quarterly Report No. 2 Covering Period May 15, 1961 to August 15, 1961

Description: The electron paramagnetic resonance (EPR) of color centers in additively colored KCl crystals is measured to observe the effects of optical bleaching at room temperature. Earlier measurements on the F-center are confirmed and the susceptibility is measured at 78 and 300 deg K over five decades of power, including the very low power region. The width and the saturation properties of the individual multiplets are studied in detail and the technique of making E PR measurements on inhomogeneously b… more
Date: August 30, 1961
Creator: Markham, J. J.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Murgatroyd-an Ibm 7090 Program for the Analysis of the Kinetics of the Msre

Description: The IBM 7090 program Murgatroyd is a revised and extended version of the IBM 704 program PET-I, which solves (by a fifth-order Runge-Kutta procedure) the coupled firstorder differential equations for power, delayed neutron concentration, and temperature in a one-region reactor as a function of time, given an input reactivity variation represented by a series of linear ramps. The basic extensions were those which were necessary to include the effects of the separate heat capacities and temperatu… more
Date: April 1, 1962
Creator: Nestor, C. W. Jr.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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DEVELOPMENT OF A PROCESS FOR SODIUM BONDING OF EBR-II FUEL AND BLANKET ELEMENTS

Description: Procedures for assembling EBR-II fuel elements with annular sodium bonds between the uranium rods and the stainless steel claddings are outlined. The results of several meltdown and uranium-settling experiments are given. Bonding experiments were performed: furnace bonding, submerged canning, ultrasonic bonding, centrifuging, pressure pulsing, and vibratory bonding. Vibratory bonding was chosen for the production of the first EBR-II core. (D.L.C.)
Date: July 1, 1961
Creator: Sowa, E.S. & Kimont, E.L.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Chemical Technology Division, Unit Operations Section Monthly Progress Report, February 1962

Description: In the operation of 6-in.-dia. foam-liquid columns, increase in either the liquid flow or foam flow caused increased channeling with increased HTU. Flooding values for the Immi mixer-settler were obtalned using the amine extraction final cycle Pu flowsheet. Two tests of the addltlon of uranyl nitrate to a thoria sol were made, one of which gave a good product and the other a product which disintegrated during calcination. Material balances for 22 waste calcination runs are summarized. (auth)
Date: August 23, 1962
Creator: Whatley, M. E.; Haas, P. A.; Horton, R. W.; Ryon, A. D.; Suddath, J. C. & Watson, C. D.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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PILOT PLANT SHUTDOWN AND Pu-Al PROCESSING

Description: The large aqueous pilot plant facilities at ORNL were cleaned and are being put in standby condition. Experience was gained during the year as anion exchange was used to recover more than one kg of plutonium left in the exploded evaporator system. This experience is being applied to a new recovery program just beginning in cell 1 of Building 4507. (auth)
Date: September 25, 1961
Creator: Bresee, J.C.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Supporting Analysis for Thermal Suitability of Fuel Elements for SM-1A Core I Loading

Description: A recommended SM-1A Core I loading chart was derived from available, metallurgically acceptable elements at the SM-1A and SM-1 sites. The derivation was based on local thermal and hydraulic considerations of minimum elementto- element coolant channel clearances. These clearances were determined from field inspection measurements of outer fuel plate spacing, as modified by analytical calculations of plate ripple growth during exposure to reactor operating thermal stresses. (auth)
Date: January 10, 1962
Creator: Brondel, J. O.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Chemical Technology Division, Unit Operations Section Monthly Progress Report, June 1961

Description: An interfacial viseometer was built for use in an interfacial phenomena study. Installation of a 6-in.-ID foam separation column system was completed. The dispersiondrying-sintering characteristics of six low-nitrate batches of thoria sol material were studied. The average effective porosity of the CuO pellets used for reactor helium purification was determined to be 0.0545 for H/ sub 2/ transport and 0.0526 for CO transport. In continuous Zirflex dissolution studies, no H/sub 2/O/sub 2/ decomp… more
Date: January 23, 1962
Creator: Whatley, M. E.; Haas, P. A.; Horton, R. W.; Ryon, A. D.; Suddath, J. C. & Watson, C. D.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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STAINLESS STEEL WASTES. III. LABORATORY STUDIES OF THE RATE OF REMOVAL OF STAINLESS STEEL IONS BY MERCURY CATHODE ELECTROLYSIS

Description: ABS> The removal rates of iron, nickel, and chromium from synthetic stainless steel waste solutions during electrolysis over a mercury cathode were studied. The loading capacity of the mercury for the stainless steel metals was estimated on the basis of laboratory experiments to be about two% by weight. The laboratory data indicated that, at an electrode potential of --1.80 voits vs S.C.E., 85 ampere-hours per liter of waste removed essentially all of the stainless steel ions from a sulfuric ac… more
Date: February 12, 1962
Creator: Anderson, D. R. & Rhodes, D. W.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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BRAZING OF CERAMICS. Progress Report

Description: Brazing alloys such as 48 Ti-48 Zr-4 Be (wt%) and 49 Ti-49 Cu-2 Be (wt%) have been found to readily flow on oxide and graphite ceramics. Two demonstrati on fuel element assemblies were fabricated to illustrate the usefulness of these procedures for nuclear applications. One of these assemblies contained graphite tubes and end caps which were brazed to a molybdenum hanger. The second demonstration fuel element was composed of a compartmented aluminum oxide plate to which aluminum oxide cover pla… more
Date: November 1, 1962
Creator: Fox, C.W.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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The Effects of Irradiation on Some Binary Alloys of Thorium-Plutonium and Zirconium-Plutonium

Description: A specimen of cast thorium-5 wt% plutonium and one of thorium-10 wt% plutonium were irradiated to total atom burnups of 1.9 and 2.6%, respectively, at maximum fuel temperatures of approximately 450 deg C. Both alloys displayed excellent dimensional stability with volume increases of 0.8 and 1.2% per atom per cent burnup, respectively. Three cold-rolled specimens of zirconium-5 wt% plutonium and one cold-rolled specimen of zirconium-7 wt% plutonium were also irradiated. The zirconium- plutonium … more
Date: July 1, 1962
Creator: Horak, J. A.; Kittel, J. H. & Rhude, H. V.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Recording Equipment for Internal Friction Measurements

Description: An apparatus was developed for recording internal friction data in such a manner as to circumvent many of the laborious and time-consuming observations and calculations usually associated with these measurements. An optical lever is used and the passage of the beam across the scale is detected by photoconductive cells. The cells are strategically located so that, when their signals are fed through a multichannel switching circuit to the pens of an operation recorder, a plot of the logarithm of … more
Date: October 31, 1961
Creator: Stephenson, R. L. & McCoy, H. E. Jr.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Organic Nuclear Reactors: An Evaluation of Current Development Programs

Description: Organic reactor technology is critically evaluated and areas of research and development work now lacking or inadequate for the successful development of this reactor concept are indicated. The development programs for present organic and heavy water moderated concepts appear generally adequate to reach specific goals. However, the narrow scope of the organic reactor program should be broadened to assure coverage of areas where the application of novel principles might result in marked economic… more
Date: May 1, 1961
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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