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The Solvent-Extraction Performance of Redox IC Columns (ANL June 1948 Flowsheet) Using Raschig Ring Packing, and Unirradiated Uranium: Redox Technical Study No. 14

Description: A report which summarizes the performance data obtained from Redox solvent extraction IC Column studies made prior to January 15, 1949 in accordance with conditions of the A.N.L. June 1, 1948, Flowsheet.
Date: August 22, 1949
Creator: Hartzell, L. O.; Woodfield, F. W. & Bradley, J. G.
Partner: UNT Libraries Government Documents Department
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A Rapid Colorimeric Method for the Determination of Phosphate in Uranium Waste Solutions

Description: Report discussing tests of a new colorimetric method. From abstract: "A colorimetric method, which is a modification of the classical phosphomolybdic acid method, has been developed for the determination of phosphate in synthetic uranium waste solutions...The chief advantage of the method, over those presently included in HW Manuals, is the rapidity with which determinations may be carried out."
Date: August 22, 1949
Creator: Sege, C. A. & Ice, C. H.
Partner: UNT Libraries Government Documents Department
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Preliminary Report on Existing Active Particle Hazard-200 Areas

Description: "Recent surveys by the Health Instrument Section have disclosed the presence of many small radioactive spots on ground surfaces in the T and B plant areas. Investigation has shown that representative samples of the spots when mechanically separated invariably end in a single radioactive particle."
Date: October 22, 1947
Creator: Mickelson, M. L.
Partner: UNT Libraries Government Documents Department
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The Preparation of Thin Films of Plutonium by Electrodeposition

Description: This report discusses methods for preparing thin films of plutonium on metallic disks, which are used for alpha energy analysis, fission counting, and preparation of geometry standards in ordinary counting. Various methods of preparation were tested and analyzed, but electrodeposition was the most effective method. Deposition was then tested, but the yields were "somewhat erratic".
Date: March 22, 1950
Creator: Miller, H. W. & Brouns, R. J.
Partner: UNT Libraries Government Documents Department
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The Oxidation of Plutonium to the Plutonyl State

Description: This report follows the study of the oxidation of plutonium III and IV to the plutonyl state.
Date: March 22, 1950
Creator: Miller, H. W. & Brouns, R. J.
Partner: UNT Libraries Government Documents Department
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Preliminary Report on the Ultrasonic Properties of Uranium

Description: This report discusses preliminary results acquired from investigations made on the ultrasonic properties of uranium, such as sonic vibrations in the megacycle frequency range.
Date: October 22, 1952
Creator: Worlton, D. C. & Wood, E. C.
Partner: UNT Libraries Government Documents Department
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Corrosion of Aluminum in Alum Coagulated Process Water

Description: The following report provides the results of an accelerated corrosion test that was performed to compare the effect of two coagulants on the corrosion rates of aluminum slug jacket alloy and 72S. Additionally, some analytical data on the water from the two treatments were obtained and are presented in this report.
Date: January 22, 1952
Creator: Dalrymple, R. S.
Partner: UNT Libraries Government Documents Department
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In-Line Scintillation Gamma Monitor : Preliminary Specifications

Description: From introduction: "The following recommendations represent the best estimate, based on present knowledge, of the requirements for generally applicable or "universal" instrument for the continuous monitoring of radioactive process streams in terms of their gamma activity."
Date: January 22, 1953
Creator: Upson, U. L. & Connally, R. E.
Partner: UNT Libraries Government Documents Department
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Determination of Radiocesium with Chloroplatinic Acid

Description: The following report examines a rapid method used to eliminate the possibility of explosive perchlorate-organic mixtures in a control laboratory in order to determine radiocesium. These methods include the usage of chloroplatinic acid as a precipitate of radocesium.
Date: June 22, 1950
Creator: Erwing, R. E.
Partner: UNT Libraries Government Documents Department
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Corrosion Data for Type 347 Stainless Steel Pipe Waste Metal Recovery Process

Description: Introduction: "A limited test progress for the evaluation of type 347 stainless steel pipe which failed the Huey (?) test has been complicated. The tests reported herein were similar in scope to those reported in document number EW-20765, Corrosion Tests on Stainless Steel Plate, Waste Metal Recovery Process. Material tested was obtained on order number EWC-8553, National Tube Company Heat #3X9741. Lots 9789 and 9790."
Date: May 22, 1951
Creator: Sanborn, Kenneth L.
Partner: UNT Libraries Government Documents Department
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On the Annealing and Aging of Zircaloy-3b

Description: The object of this study was to determine the effects of several annealing treatments and aging treatments on the tensile test behavior of Zircaloy-3b.
Date: October 22, 1956
Creator: Johnson, D. E.
Partner: UNT Libraries Government Documents Department
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Hazardous Materials - Redox Plant

Description: The Redox process uses or produces only a very few materials that are hazardous for reasons other than radioactivity. The conditions under which these materials become hazardous were carefully taken into consideration in the development of the process and design of the equipment. A considerable about of information on the hazardous properties of the process materials was obtained so that the pertinent material could be incorporated into the process specifications. Providing the equipment is ope… more
Date: May 22, 1956
Creator: Underwood, J. W.
Partner: UNT Libraries Government Documents Department
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Soil Column Studies with Radiostrontium I. Effects of Temperature and of Species of Accompanying Ion

Description: Soil chemistry studies have been carried on at Hanford for a number of years in support of the disposal of low and intermediate level liquid wastes to the ground. Equilibrium type experiments were carried out to investigate the mechanisms of the reactions of Sr, Cs, and rare earth ions with soils (1, 3, 4, 5). Experiments were also conducted with simulated and actual wastes in soil columns and an empirical method was developed for prediction of radionuclide breakthrough from ground disposal fac… more
Date: September 22, 1959
Creator: Nelson, J. L.
Partner: UNT Libraries Government Documents Department
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A Tentative Anion Exchange-Precipitation Procedure for the Determination of Cs¹³⁷

Description: An anion exchange precipitation procedure was developed for the determination of Cs¹³⁷ in various aged fission product waste solutions, and other solutions containing Cs¹³⁷. The procedure is based on the ability of an anion exchange column to function simultaneously at an anion exchanger and as a precipitating agent (1).
Date: December 22, 1955
Creator: Perkins, R. W.
Partner: UNT Libraries Government Documents Department
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Description: The design criteria are written to supply information for the preparation of a project proposal covering budget item B-2265 for Fiscal Year 1956. The function of in-line instrumentation installed shall be the rapid on-the-spot analysis of process variables for quick presentation to process operators for immediate action in process control. Alarm or safety circuits may be incorporated on the equipment.
Date: February 22, 1956
Creator: Hildreth, N. T.
Partner: UNT Libraries Government Documents Department
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Wet Fluoride Studies: Calcium Plutonium (IV) Fluoride

Description: Laboratory studies have shown that the double salt, CaF2-PuF4, can be precipitated by rapid addition of hydro-fluoric acid to solutions containing 25 to 75 g Pu/1, caleium equimolar to plutonium, and 1 to 10 M HNO3. The precipitate, which is subsequently washed with water and dried to 300 degrees C in dehumidified, deoxygenated argon, can be reduced thermally by calcium to give high yields of plutonium metal.
Date: December 22, 1953
Creator: Branin, P. B.
Partner: UNT Libraries Government Documents Department
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Improved Calibration Facility

Description: Aid in redesign of the calibration facility in order to: 1. Reduce the rate of exposure for calibration personnel below 1 mr/hr; 2. Reduce the rate of exposure outside of the 3745 Building; 3. Reduce the risk of breaking radium sources; 4. Improve the efficiency of calibration procedures by: a. Allowing calibration to be done faster; b. Providing several calibration ranges which can operate simultaneously in the present space allowed; c. Allowing instrument survey work to proceed while calibrat… more
Date: August 22, 1995
Creator: Roesch, W. C.
Partner: UNT Libraries Government Documents Department
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Pyrophoricity of Uranium in Reactor Environments

Description: Report discussing information relative to the pyrophoricity of uranium for the purpose of reactor core fire safety. The report includes physical and chemical properties of uranium.
Date: January 22, 1960
Creator: Zima, G. E.
Partner: UNT Libraries Government Documents Department
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Limitations for Existing Storage Tanks for Radioactive Wastes from Separations Plants

Description: Continued process improvements in the separation plants provide an incentive for economics in waste storage costs by utilizing existing facilities to their maximum capability consistent with the radiological hazards involved. The major improvements have reduced waste volumes resulting in increased fission product concentration and energy potential. Analyses have been made to determine the effect of this change on the integrity of the existing structures.
Date: October 22, 1959
Creator: Doud, E.
Partner: UNT Libraries Government Documents Department
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The Effect of Solution and Vessel Thermal Expansion on Volume Measurements in the Chemical Processing Department

Description: The major portion of transfers and inventory in the Chemical Processing Department are dependent on volume measurement. Good volume measurements are therefore essential to good SS material control. Considerable attention has been given to the volume problem especially on primary transfer points. Document HW-57888 discusses the biasing effect pf temperature on manometer oil. HW- 57866 given the procedure for vessel calibration. Other undocumented correspondence has discussed recent calibrations … more
Date: May 22, 1959
Creator: Johnson, W. R.
Partner: UNT Libraries Government Documents Department
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Composition of Solids from Purex LWW

Description: The solids in Purex lww were first observed during flowsheet tests for recovery of fission products from plant wastes. Since the nature of this solid was not apparent from the flowsheet composition of lww, some work was performed to characterize this material. Although this work has been conducted over a period of about one year, it has been subordinate to the main one of testing flowsheets for fission product recovery. The solids have been observed in each of about six samples of plant lww tha… more
Date: January 22, 1959
Creator: Van Tuyl, H.H.
Partner: UNT Libraries Government Documents Department
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Electrical Precipitator for Aerosol Collection on Electron Microscope Screens

Description: In order to utilize the advantages of the electron microscope for the study of respirable particles, it is desirable to have an instrument capable of sampling from atmospheres having very sparse dispersions of particles at a rate sufficiently high to result in precipitation densities of approximately one particle per 10/u² of microscope screen for a 10 minute sampling period. In order to avoid qualitative or quantitative alteration of the aerosol, it was desired that the instrument collect the … more
Date: September 22, 1955
Creator: Baum, J. W.
Partner: UNT Libraries Government Documents Department
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Purification of Mercury Metal

Description: Mercury to be used in polarography as a dropping mercury electrode must be of the highest purity. The author has found that much of the commercial "triple-distilled" mercury as well as that which is repurified on site is not sufficiently pure and because of this, a study of mercury purification techniques was made and a very satisfactory procedure was tested thoroughly. This procedure is described in detail in this report.
Date: November 22, 1955
Creator: Koyama, Karl
Partner: UNT Libraries Government Documents Department
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