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Method of solubilizing phthalocyanines and metallophthalocyanines

Description: A one-step method of manufacturing soluble phthalocyanines and metallophthalocyanines, like zinc phthalocyanine, by converting a phthalocyanine or a metallophthalocyanine to a trialkylsilyl-substituted derivative is disclosed. The phthalocyanine or metallophthalocyanine is converted to a soluble trialkylsilyl-substituted derivative by interacting the phthalocyanine or metallophthalocyanine with an active metal amide, like lithium 2,2,6, 6-tetra-methylpiperidide, and a halotrialkylsilane, like chlorotrimethylsilane, to provide a phthalocyanine compound, like phthalocyanine monomers, dimers or polymers, metalated or unmetalated, that are soluble in organic media.
Date: June 1, 1990
Creator: Rathke, Jerome W.; Chen, Michael J. & Fendrick, Carol M.
Partner: UNT Libraries Government Documents Department

Method and apparatus for transporting liquid slurries

Description: An improved method and device to prevent erosion of slurry transport devices is disclosed which uses liquid injection to prevent contact by the slurry composition with the inner surface of the walls of the transport system. A non-abrasive liquid is injected into the slurry transport system and maintains intimate contact with the entire inner surface of the transport system, thereby creating a fluid barrier between the nonabrasive liquid and the inner surface of the transport system which thereby prevents erosion.
Date: January 1, 1991
Creator: Berry, Gregory F.; Lyczkowski, Robert W. & Wang, Chi-Sheng
Partner: UNT Libraries Government Documents Department

Process of making cryogenically cooled high thermal performance crystal optics

Description: A method for constructing a cooled optic wherein one or more cavities are milled, drilled or formed using casting or ultrasound laser machining techniques in a single crystal base and filled with porous material having high thermal conductivity at cryogenic temperatures. A non-machined strain-free single crystal can be bonded to the base to produce superior optics. During operation of the cooled optic, N{sub 2} is pumped through the porous material at a sub-cooled cryogenic inlet temperature and with sufficient system pressure to prevent the fluid bulk temperature from reaching saturation.
Date: June 29, 1990
Creator: Kuzay, Tuncer M.
Partner: UNT Libraries Government Documents Department

Cesium iodide alloys

Description: This invention relates to a CsI composition with improved mechanical strength and outstanding multispectral infrared transmittance, for window use. The additive is a monovalent iodide, other than CsI, added in amounts sufficient to maximize fracture strength from 16 to 40 MPa, while maintaining at least 10% transparency in the 4 to 50 micrometer wavelength range. The preferred additive is AgI, although RbI or CuI can be used. 6 figs. (DLC)
Date: January 1, 1991
Creator: Kim, Hyoun-Ee & Moorhead, A. J.
Partner: UNT Libraries Government Documents Department

Locking mechanism for indexing device

Description: Disclosed is a locking mechanism for an indexing spindle. A conventional spur gear having outwardly extending teeth is affixed to the spindle. Also included is a rotatably mounted camshaft whose axis is arranged in skewed relationship with the axis of the spindle. A disk-like wedge having opposing camming surfaces is eccentrically mounted on the camshaft. As the camshaft is rotated, the camming surfaces of the disk are interposed between adjacent gear teeth with a wiping action that wedges the disk between the gear teeth. A zero backlash engagement between disk and gear results, with the engagement having a high mechanical advantage so as to effectively lock the spindle against bi-directional rotation.
Date: January 25, 1982
Creator: Lindenmeyer, C. W.
Partner: UNT Libraries Government Documents Department

Method of preparing high-temperature-stable thin-film resistors

Description: A chemical vapor deposition method for manufacturing tungsten-silicide thin-film resistors of predetermined bulk resistivity and temperature coefficient of resistance (TCR) is disclosed. Gaseous compounds of tungsten and silicon are decomposed on a hot substrate to deposit a thin-film of tungsten-silicide. The TCR of the film is determined by the crystallinity of the grain structure, which is controlled by the temperature of deposition and the tungsten to silicon ratio. The bulk resistivity is determined by the tungsten to silicon ratio. Manipulation of the fabrication parameters allows for sensitive control of the properties of the resistor.
Date: November 12, 1980
Creator: Raymond, L. S.
Partner: UNT Libraries Government Documents Department

Secure communication of static information by electronic means

Description: This invention is comprised of a method and apparatus for the secure transmission of static data from a tag to a remote reader. Each time the static data is to be transmitted to the reader, the 10 bits of static data are combined with 54 bits of binary data, which constantly change from one transmission to the next, into a 64-bit number. This number is then encrypted and transmitted to the remote reader where it is decrypted to produce the same 64 bit number that was encrypted in the tag. With a continual change in the value of the 64 bit number in the tag, the encrypted numbers transmitted to the reader will appear to be dynamic in character rather than being static.
Date: December 31, 1991
Creator: Gritton, D. G.
Partner: UNT Libraries Government Documents Department

Vanadium-pumped titanium x-ray laser

Description: A resonantly photo-pumped x-ray laser is formed of a vanadium and titanium foil combination that is driven by two beams of intense line focused optical laser radiation. Ground state neon-like titanium ions are resonantly photo-pumped by line emission from fluorine-like vanadium ions.
Date: February 13, 1991
Creator: Nilsen, J.
Partner: UNT Libraries Government Documents Department

Amorphous silicon/polycrystalline thin film solar cells

Description: An improved photovoltaic solar cell is described including a p-type amorphous silicon layer, intrinsic amorphous silicon, and an n-type polycrystalline semiconductor such as cadmium sulfide, cadmium zinc sulfide, zinc selenide, gallium phosphide, and gallium nitride. The polycrystalline semiconductor has an energy bandgap greater than that of the amorphous silicon. The solar cell can be provided as a single-junction device or a multijunction device.
Date: March 13, 1991
Creator: Ullal, H. S.
Partner: UNT Libraries Government Documents Department

Process for strengthening silicon based ceramics

Description: A process for strengthening silicon based ceramic monolithic materials and composite materials that contain silicon based ceramic reinforcing phases that requires that the ceramic be exposed to a wet hydrogen atmosphere at about 1400{degrees}C. The process results in a dense, tightly adherent silicon containing oxide layer that heals, blunts, or otherwise negates the detrimental effect of strength limiting flaws on the surface of the ceramic body.
Date: March 7, 1991
Creator: Kim, Hyoun-Ee & Moorhead, A. J.
Partner: UNT Libraries Government Documents Department

Magnetron sputtered boron films and Ti/B multilayer structures

Description: A method is described for the production of thin boron and titanium/boron films by magnetron sputter deposition. The amorphous boron films contain no morphological growth features, unlike those found when thin films are prepared by various physical vapor 5 deposition processes. Magnetron sputter deposition method requires the use of a high density crystalline boron sputter target which is prepared by hot isostatic pressing. Thin boron films prepared by this method are useful for ultra-thin band pass filters as well as the low Z element in low Z/high Z mirrors which enhance reflectivity 10 from grazing to normal incidence.
Date: March 11, 1991
Creator: Makowiecki, D. M. & Jankowski, A. F.
Partner: UNT Libraries Government Documents Department

Precision surface machining

Description: Precision finishing apparatus utilizing line contact polishing to produce optical quality parts. A rotatable cylinder is horizontally disposed above a workpiece which is mounted on a rotatable, and horizontally and vertically adjustable chuck. Predetermined surfaces can be cut into the surface of the cylinder to produce figures of revolution, such as aspheres,, when the workpiece is being rotated.
Date: March 6, 1991
Creator: Lazazzera, Vito J. & Schmell, Rodney A.
Partner: UNT Libraries Government Documents Department

Optical transcutaneous bilirubin detector

Description: This invention consists of a transcutaneous bilirubin detector comprising a source of light having spectral components absorbable and not absorbable by bilirubin, a handle assembly, electronic circuitry and a fiber optic bundle connecting the assembly to the light source and circuitry. Inside the assembly is a prism that receives the light from one end of the fiber optic bundle and directs it onto the skin and directs the reflected light back into the bundle. The other end of the bundle is trifucated, with one end going to the light source and the other two ends going to circuitry that determines how much light of each kind has been reflected. A relatively greater amount absorbed by the skin from the portion of the spectrum absorbable by bilirubin may indicate the presence of the illness. Preferably, two measurements are made, one on the kneecap and one on the forehead, and compared to determine the presence of bilirubin. To reduce the impact of light absorption by hemoglobin in the blood carried by the skin, pressure is applied with a plunger and spring in the handle assembly, the pressure limited by points of a button slidably carried in the assembly that are perceived by touch when the pressure applied is sufficient.
Date: March 4, 1991
Creator: Kronberg, J. W.
Partner: UNT Libraries Government Documents Department

Chemotactic selection of pollutant degrading soil bacteria

Description: A method is described for identifying soil microbial strains which may be bacterial degraders of pollutants. This method includes: Placing a concentration of a pollutant in a substantially closed container; placing the container in a sample of soil for a period of time ranging from one minute to several hours; retrieving the container and collecting its contents; microscopically determining the identity of the bacteria present. Different concentrations of the pollutant can be used to determine which bacteria respond to each concentration. The method can be used for characterizing a polluted site or for looking for naturally occurring biological degraders of the pollutant. Then bacteria identified as degraders of the pollutant and as chemotactically attracted to the pollutant are used to innoculate contaminated soil. To enhance the effect of the bacteria on the pollutant, nutrients are cyclicly provided to the bacteria then withheld to alternately build up the size of the bacterial colony or community and then allow it to degrade the pollutant.
Date: March 4, 1991
Creator: Hazen, T. C.
Partner: UNT Libraries Government Documents Department

Method to synthesize dense crystallized sodalite pellet for immobilizing halide salt radioactive waste

Description: This report describes a method for immobilizing waste chloride salts containing radionuclides such as cesium and strontium and hazardous materials such as barium. A sodalite intermediate is prepared by mixing appropriate amounts of silica, alumina and sodium hydroxide with respect to sodalite and heating the mixture to form the sodalite intermediate and water. Heating is continued to drive off the water to form a water-free intermediate. The water-free intermediate is mixed with either waste salt or waste salt which has been contacted with zeolite to concentrate the radionuclides and hazardous material. The waste salt-intermediate mixture is then compacted and heated under conditions of heat and pressure to form sodalite with the waste salt, radionuclides and hazardous material trapped within the sodalite cage structure. This provides a final product having excellent leach resistant capabilities.
Date: January 1, 1992
Creator: Koyama, T.
Partner: UNT Libraries Government Documents Department

Apparatus and method for critical current measurements

Description: An apparatus for the measurement of the critical current of a superconductive sample, e.g., a clad superconductive sample, the apparatus including a conductive coil, a means for maintaining the coil in proximity to a superconductive sample, an electrical connection means for passing a low amplitude alternating current through the coil, a cooling means for maintaining the superconductive sample at a preselected temperature, a means for passing a current through the superconductive sample, and, a means for monitoring reactance of the coil. The alternating current capable of generating a magnetic field sufficient to penetrate, e.g., any cladding, and to induce eddy currents in the superconductive material, passing a steadily increasing current through the superconductive material, the current characterized as having a different frequency than the alternating current, and, monitoring the reactance of the coil with a phase sensitive detector as the current passed through the superconductive material is steadily increased whereby critical current of the superconductive material can be observed as the point whereat a component of impedance deviates.
Date: March 15, 1991
Creator: Martin, J. A. & Dye, R. C.
Partner: UNT Libraries Government Documents Department

Actinide halide complexes

Description: A compound of the formula MX{sub n}L{sub m} wherein M = Th, Pu, Np,or Am thorium, X = a halide atom, n = 3 or 4, L is a coordinating ligand selected from the group consisting of aprotic Lewis bases having an oxygen-, nitrogen-, sulfur-, or phosphorus-donor, and m is 3 or 4 for monodentate ligands or is 2 for bidentate ligands, where n + m = 7 or 8 for monodentate ligands or 5 or 6 for bidentate ligands, a compound of the formula MX{sub n} wherein M, X, and n are as previously defined, and a process of preparing such actinide metal compounds including admixing the actinide metal in an aprotic Lewis base as a coordinating solvent in the presence of a halogen-containing oxidant, are provided.
Date: February 7, 1991
Creator: Avens, Larry R.; Zwick, Bill D.; Sattelberger, Alfred P.; Clark, David L. & Watkin, J. G.
Partner: UNT Libraries Government Documents Department

Integrated null-flux suspension and multiphase propulsion system for magnetically-levitated vehicles

Description: This report discusses a propulsion and stabilization system comprising a series of figure 8 coils mounted vertically on the walls of the guideway to provide suspension, lateral guidance and propulsion of a magnetically levitated vehicle. This system further allows for altering the magnetic field effects by changing the relative position of the loops comprising the figure 8 coils either longitudinally and/or vertically with resulting changes in the propulsion, the vertical stability, and the suspension.
Date: January 1, 1992
Creator: Rote, D. M.; He, Jianliang & Johnson, L. R.
Partner: UNT Libraries Government Documents Department

Improved high speed maglev design

Description: This report discusses a propulsion and stabilization system for an inductive repulsion type magnetically levitated vehicle which is propelled and suspended by a system which includes dividing the superconducting magnets into two types: a strong field magnet which is located vertically below the vehicle for propulsion and guidance and a weak field superconducting magnet located at the ends of the vehicle for levitation and added guidance. Several proposed embodiments exist for the placement of the magnetic field shielding: locating the shielding on the vehicle, locating the shielding on the guideway, and locating the shielding on the guideway and adding shielding to the vertical undercarriage. In addition, the separation between the be vehicle and the guideway can be controlled to reduce the exposure of the passenger cabin to magnetic fields.
Date: January 1, 1992
Creator: Rote, D. M.; He, Jianliang & Coffey, H. T.
Partner: UNT Libraries Government Documents Department

Oil/gas separator for installation at burning wells

Description: An oil/gas separator is disclosed that can be utilized to return the burning wells in Kuwait to production. Advantageously, a crane is used to install the separator at a safe distance from the well. The gas from the well is burned off at the site, and the oil is immediately pumped into Kuwait`s oil gathering system. Diverters inside the separator prevent the oil jet coming out of the well from reaching the top vents where the gas is burned. The oil falls back down, and is pumped from an annular oil catcher at the bottom of the separator, or from the concrete cellar surrounding the well.
Date: December 31, 1991
Creator: Alonso, C. T.; Bender, D. A. & Bowman, B. R.
Partner: UNT Libraries Government Documents Department

Phase stable rf transport system

Description: This invention is comprised of an RF transport system which delivers a phase-stable RF signal to a load, such as an RF cavity of a charged particle accelerator. A circuit generates a calibration signal at an odd multiple frequency of the RF signal where the calibration signal is superimposed with the RF signal on a common cable that connects the RF signal with the load. Signal isolating diplexers are located at both the RF signal source end and load end of the common cable to enable the calibration to be inserted and extracted from the cable signals without any affect on the RF signal. Any phase shift in the calibration signal during traverse of the common cable is then functionally related to the phase shift in the RF signal. The calibration phase shift is used to control a phase shifter for the RF signal to maintain a stable RF signal at the load.
Date: February 19, 1991
Creator: Curtin, M. T.; Natter, E. F. & Denney, P. M.
Partner: UNT Libraries Government Documents Department

Pulse combustor with controllable oscillations

Description: A pulse combustor having thermally induced pulse combustion in a continuously flowing system is described. The pulse combustor is fitted with at lease one elongated ceramic body which significantly increases the heat transfer area in the combustion chamber of the combustor. The ceramic body or bodies possess sufficient mass and heat capacity to ignite the fuel-air charge once the ceramic body or bodies are heated by conventional spark plug initiated combustion so as to provide repetitive ignition and combustion of sequentially introduced fuel-air charges without the assistance of the spark plug and the rapid quenching of the flame after each ignition in a controlled manner so as to provide a selective control over the oscillation frequency and amplitude. Additional control over the heat transfer in the combustion chamber is provided by employing heat exchange mechanisms for selectively heating or cooling the elongated ceramic body or bodies and/or the walls of the combustion chamber.
Date: December 31, 1991
Creator: Richards, G. A.; Morris, G. J. & Welter, M. J.
Partner: UNT Libraries Government Documents Department

Process for producing clad superconductive materials

Description: A process for fabricating superconducting composite wire by the steps of placing a superconductive precursor admixture capable of undergoing a self propagating combustion in stoichiometric amounts sufficient to form a superconductive product within a metal tube, sealing one end of said tube, igniting said superconductive precursor admixture whereby said superconductive precursor admixture endburns along the length of the admixture, and cross-section reducing said tube at a rate substantially equal to the rate of burning of said superconductive precursor admixture and at a point substantially planar with the burnfront of the superconductive precursor mixture, whereby a clad superconductive product is formed in situ, the product characterized as superconductive without a subsequent sintering stage, is disclosed.
Date: March 19, 1991
Creator: Cass, R. B.; Ott, K. C. & Peterson, D. E.
Partner: UNT Libraries Government Documents Department