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High-resolution, high-transmission soft x-ray spectrometer for the study of biological samples

Description: We present a variable line-space grating spectrometer for soft s-rays that coverst the photon energy range between 130 and 650 eV. The optical design is based on the Hettrick-Underwood principle and tailored to synchrotron-based studies of radiation-sensitive biological samples. The spectrometer is able to record the entire spectral range in one shot, i.e., without any mechanical motion, at a resolving power of 1200 or better. Despite is slitless design, such a resolving power can be achieved for a source spot as large as (30 x 3000) micrometers squared, which is important for keeping beam damage effects in radiation-sensitive samples low. The high spectrometer efficiency allows recording of comprehensive two-dimensional resonant inelastic soft x-ray scatters (RIXS) maps with good statistics within several minutes. This is exemplarily demonstrated for a RIXS map of highly oriented pyrolytic graphite, which was taken with 10 min.
Date: June 11, 2009
Creator: Fuchs, Oliver; Weinhardt, L.; Blum, M.; Welgand, M.; Umbach, E.; Bar, M. et al.
Partner: UNT Libraries Government Documents Department

Time-Resolved Hard X-Ray Spectrometer

Description: Wired array studies are being conducted at the SNL Z accelerator to maximize the x-ray generation for inertial confinement fusion targets and high energy density physics experiments. An integral component of these studies is the characterization of the time-resolved spectral content of the x-rays. Due to potential spatial anisotropy in the emitted radiation, it is also critical to diagnose the time-evolved spectral content in a space-resolved manner. To accomplish these two measurement goals, we developed an x-ray spectrometer using a set of high-speed detectors (silicon PIN diodes) with a collimated field-of-view that converged on a 1-cm-diameter spot at the pinch axis. Spectral discrimination is achieved by placing high Z absorbers in front of these detectors. We built two spectrometers to permit simultaneous different angular views of the emitted radiation. Spectral data have been acquired from recent Z shots for the radial and polar views. UNSPEC1 has been adapted to analyze and unfold the measured data to reconstruct the x-ray spectrum. The unfold operator code, UFO2, is being adapted for a more comprehensive spectral unfolding treatment.
Date: March 1, 2007
Creator: Moya, Kenneth; McKenna, Ian; Keenan, Thomas & Cuneo, Michael
Partner: UNT Libraries Government Documents Department

A Soft X-ray Spectrometer using a Highly Dispersive Multilayer Grating

Description: There is a need for higher resolution spectrometers as a tool for inelastic x-ray scattering. Currently, resolving power around R = 10,000 is advertised. Measured RIXS spectra are often limited by this instrumental resolution and higher resolution spectrometers using conventional gratings would be prohibitively large. We are engaged in a development program to build blazed multilayer grating structures for diffracting soft x-rays in high order. This leads to spectrometers with dispersion much higher than is possible using metal coated-gratings. The higher dispersion then provides higher resolution and the multilayer gratings are capable of operating away from grazing incidence as required. A spectrometer design is presented with a total length 3.8m and capable of 10{sup 5} resolving power.
Date: January 31, 2010
Creator: Warwick, Tony; Padmore, Howard; Voronov, Dmitriy & Yashchuk, Valeriy
Partner: UNT Libraries Government Documents Department

Integrated X-ray testing of the electro-optical breadboard model for the XMM reflection grating spectrometer

Description: X-ray calibration of the Electro-Optical Breadboard Model (EOBB) of the XXM Reflection Grating Spectrometer has been carried out at the Panter test facility in Germany. The EOBB prototype optics consisted of a four-shell grazing incidence mirror module followed by an array of eight reflection gratings. The dispersed x-rays were detected by an array of three CCDs. Line profile and efficiency measurements where made at several energies, orders, and geometric configurations for individual gratings and for the grating array as a whole. The x-ray measurements verified that the grating mounting method would meet the stringent tolerances necessary for the flight instrument. Post EOBB metrology of the individual gratings and their mountings confirmed the precision of the grating boxes fabrication. Examination of the individual grating surface`s at micron resolution revealed the cause of anomalously wide line profiles to be scattering due to the crazing of the replica`s surface.
Date: July 12, 1994
Creator: Bixler, J. V.; Craig, W.; Decker, T.; Aarts, H.; Boggende, T. den; Brinkman, A. C. et al.
Partner: UNT Libraries Government Documents Department

FRONT-END ASIC FOR HIGH RESOLUTION X-RAY SPECTROMETERS.

Description: We present an application specific integrated circuit (ASIC) for high-resolution x-ray spectrometers. The ASIC is designed to read out signals from a pixelated silicon drift detector (SDD). Each hexagonal pixel has an area of 15 mmz and an anode capacitance of less than 100 fF. There is no integrated Field Effect transistor (FET) in the pixel, rather, the readout is done by wirebonding the anodes to the inputs of the ASIC. The ASIC provides 14 channels of low-noise charge amplification, high-order shaping with baseline stabilization, and peak detection with analog memory. The readout is sparse and based on low voltage differential signaling. An interposer provides all the interconnections required to bias and operate the system. The channel dissipates 1.6 mW. The complete 14-pixel unit covers an area of 210 mm{sup 2}, dissipates 12 mW cm{sup -2}, and can be tiled to cover an arbitrarily large detection area. We measured a preliminary resolution of 172 eV at -35 C on the 6 keV peak of a {sup 55}Fe source.
Date: October 27, 2007
Creator: DE GERONIMO,G.; CHEN, W.; FRIED, J.; LI, Z.; PINELLI, D.A.; REHAK, P. et al.
Partner: UNT Libraries Government Documents Department

A broadband high-resolution elliptical crystal x-ray spectrometer for high energy density physics experiments

Description: Spectroscopic investigation of high temperature laser produced plasmas in general, and x-ray opacity experiments in particular, often requires instruments with both a broad coverage of x-ray energies and high spectral, spatial, and temporal resolution. We analyze the design, model the response, and report the commissioning of a spectrometer using elliptical crystals in conjunction with a large format, gated microchannel plate detector. Measurements taken with this instrument at the JANUS laser facilities demonstrate the designed spectral range of 0.24 to 5.8 keV, and spectral resolution E/{Delta}E > 500, resulting in 2 to 3 times more spectral data than achieved by previous spectrometer designs. The observed 100 picosecond temporal resolution and 35 {micro}m spatial resolution are consistent with the requirements of high energy density opacity experiments.
Date: March 31, 2006
Creator: Anderson, S G; Heeter, R F; Booth, R; Emig, J; Fulkerson, S; McCarville, T et al.
Partner: UNT Libraries Government Documents Department

Measurement of the relaxation time of hot electrons in laser-solid interaction at relativistic laser intensities

Description: The authors have measured the relaxation time of hot electrons in short pulse laser-solid interactions using a picosecond time-resolved x-ray spectrometer and a time-integrated electron spectrometer. Employing laser intensities of 10{sup 17}, 10{sup 18}, and 10{sup 19} W/cm{sup 2}, they find increased laser coupling to hot electrons as the laser intensity becomes relativistic and thermalization of hot electrons at timescales on the order of 10 ps at all laser intensities. They propose a simple model based on collisional coupling and plasma expansion to describe the rapid relaxation of hot electrons. The agreement between the resulting K{sub {alpha}} time-history from this model with the experiments is best at highest laser intensity and less satisfactory at the two lower laser intensities.
Date: August 22, 2006
Creator: Chen, H; Shepherd, R; Chung, H K; Dyer, G; Faenov, A; Fournier, K B et al.
Partner: UNT Libraries Government Documents Department

Evaluation of field-portable X-ray fluorescence spectrometry for the determination of lead contamination on small-arms firing ranges

Description: Field analytical methods for the characterization of lead contamination in soil are being developed. In this study, the usefulness of a commercially available, field-portable energy-dispersive X-ray fluorescence spectrometer (XRF) is evaluated for determining the extent of lead contamination in soils on small-arms firing ranges at a military installation. This field screening technique provides significant time and cost savings for the study of sites with lead-contaminated soil. Data obtained with the XRF unit in the field are compared with data obtained from soil samples analyzed in an analytical laboratory by inductively coupled plasma atomic emission spectroscopy. Results indicate that the field-portable XRF unit evaluated in this study provides data that are useful in determining the extent and relative magnitude of lead contamination. For the commercial unit used in this study, improvements in the spectral resolution and in the limit of detection would be required to make the unit more than just a screening tool.
Date: February 1, 1995
Creator: Schneider, J.F.; Taylor, J.D.; Bass, D.A.; Zellmer, D. & Rieck, M.
Partner: UNT Libraries Government Documents Department

Industrial x-ray fluorescence analysis new applications and challenges for cryogenic detectors

Description: Cryogenic, high-resolution X-ray detectors have potential applications in industrial X-ray fluorescence (XRF) analysis. We discuss various XRF analysis techniques currently used in the semiconductor industry, problems encountered due to limitations of current detectors and the potential benefits of using cryogenic detectors in these applications. We give examples of demonstration experiments, compare the performance of current conventional and cryogenic X-ray spectrometers and present an outlook.
Date: August 1, 1997
Creator: Frank, M.
Partner: UNT Libraries Government Documents Department

High-resolution superconducting x-ray spectrometers with an active area of 282 um x 282 um

Description: Superconducting tunnel junctions coupled to superconducting absorbers may be used as high-resolution, high-efficiency X-ray spectrometers. We have tested devices with niobium X-ray absorbing layers coupled to aluminum layers that serve as quasiparticle traps. In this work we measured the current pulses from a large area tunnel junction using an amplifier based on an array of 100 SQUIDs. Using this amplifier and a 282 micron X 282 micron junction, we have measured an energy resolution of 19 eV FWHM for 1.5 keV X rays and 21 eV for 2.6 keV X rays. The area of this junction is eight times the area of any junction previously measured to have such high energy resolution.
Date: September 11, 1996
Creator: Mears, C.A.; Labov, S.E.; Frank, M.; Netel, H.; Hiller, L.J.; Lindeman, M.A. et al.
Partner: UNT Libraries Government Documents Department

Low-energy response of superconducting tunnel junction x-ray spectrometers

Description: Thin film structures incorporating metallic superconducting layers and tunnel junctions can be configured as low-energy X-ray spectrometers. We present results obtained when low-energy X-rays are absorbed in niobium films coupled to aluminum layers that serve as quasiparticle traps in an Nb/Al/Al{sub 2}O{sub 3}/Al/Nb tunnel junction X-ray detector. The linearity of the pulse height as a function of energy is discussed along with the energy dependence of the observed resolution and its relation to the broadening mechanisms. A resolution of 14 eV at 1 keV has been measured with our detector cooled to 0.3 K.
Date: December 31, 1994
Creator: Labov, S. E.; Hiller, L. H.; Measrs, C. A.; Frank, M.; Netel, H.; Azgui, F. et al.
Partner: UNT Libraries Government Documents Department

A 100 ps gated x-ray spectrometer

Description: Material opacities are of interest in many fields. We have developed a Bragg reflection spectrometer that is gated for imaging samples in a laser heated environment for opacity measurement. A micro-channel plate is coated with a photocathode material and a fast pulse is launched across it. Electrons are converted to photons in a phosphor and recorded on film. Optical gate pulse widths of 100 ps are achieved. Some optical pulse width and sensitivity enhancements are noted at launch and termination. Events of interest are 200 ps long. The framing window is approximately 250 ps in length. Timing jitter is a problem. The instrument timing networks have been examined, and the source of jitter is still unknown. Timing to 50 ps resolution is desired. Close in proximity to the laser-driven event leads to complications in shielding from hard x-rays, hot electrons and shock-driven damage. High Z materials provide shielding from hard x-rays. Magnets screen out hot electrons produced by laser-matter interactions Filters provide energy fiducials. PCD`s provide high resolution timing measurements. Data is recorded on film in a specially designed film pack. The instrument is designed to be used in the NOVA Laser Facility at Lawrence Livermore National Laboratory.
Date: September 1, 1995
Creator: Walsh, P.J.; Blake, R.L.; Caldwell, S.; Hockaday, M.; Chrien, R. & Smith, R.C.
Partner: UNT Libraries Government Documents Department

Science and Technology Review June 2002

Description: This Science and Technology Review has the following stories: (1) Fighting Bioterrorism, Fighting Cancer; (2) A Two-Pronged Attack on Bioterrorism--synthetic two-legged molecules will be excellent detectors of biowarfare agents and cancer cells; (3) Adaptive Optics Sharpen the View from Earth--astronomers are obtaining images with unprecedented resolution, thanks to telescopes equipped with adaptive optics developed at Livermore; (4) Experiments Re-create X Rays from Comets--Experiments using the Laboratory's electron beam ion trap and an x-ray spectrometer designed by the National Aeronautics and Space Administration are shedding light on how comets emit x rays as they pass the Sun; (5) Chemistry--50 Years of exploring the Material World--from isotopic analysis to atomic-level simulations of material behavior, Livermore's chemists and materials scientists apply their expertise to fulfill the Laboratory's mission.
Date: June 1, 2002
Creator: Budil, K.
Partner: UNT Libraries Government Documents Department

DEVELOPMENT OF A HIGH RATE HIGH RESOLUTION DETECTOR FOR EXAFS EXPERIMENTS.

Description: A new detector for EXAFS experiments is being developed. It is based on a multi-element Si sensor and dedicated readout ASICs. The sensor is composed of 384 pixels, each having 1 mm{sup 2} area, arranged in four quadrants of 12 x 8 elements, and wire-bonded to 32-channel front-end ASICs. Each channel implements low noise preamplification with self-adaptive continuous reset, high order shaper, band-gap referenced baseline stabilizer, one threshold comparator and two DAC adjustable window comparators, each followed by a 24-bit counter. Fabricated in 0.35{micro}m CMOS dissipates about 8mW per channel. First measurements show at room temperature a resolution of 14 rms electrons without the detector and of 40 rms electrons (340eV) with the detector connected and biased. Cooling at -35C a FWHM of 205eV (167eV from electronics) was measured at the Mn-K{alpha} line. A resolution of about 300eV was measured for rates approaching 100kcps/cm{sup 2} per channel, corresponding to an overall rate in excess of 10MHz/cm{sup 2}. A channel-to-channel threshold dispersion after DACs adjustment of 2.5 rms electrons was also measured.
Date: November 2002
Creator: De Geronimo, G.; O'Connor, P.; Beuttenmuller, R. H.; Li, Z.; Kuczewski, A. J. & Siddons, D. P.
Partner: UNT Libraries Government Documents Department

The First Experiments on the National Ignition Facility

Description: A first set of laser-plasma interaction, hohlraum energetics and hydrodynamic experiments have been performed using the first 4 beams of the National Ignition Facility (NIF), in support of indirect drive Inertial Confinement Fusion (ICF) and High Energy Density Physics (HEDP). In parallel, a robust set of optical and x-ray spectrometers, interferometer, calorimeters and imagers have been activated. The experiments have been undertaken with laser powers and energies of up to 8 TW and 17 kJ in flattop and shaped 1-9 ns pulses focused with various beam smoothing options.
Date: November 11, 2005
Creator: Landen, O L; Glenzer, S; Froula, D; Dewald, E; Suter, L J; Schneider, M et al.
Partner: UNT Libraries Government Documents Department

Plasma Diagnostic Calibration and Characterizations with High Energy X-rays

Description: National Security Technologies’ High Energy X-ray (HEX) Facility is unique in the U.S. Department of Energy complex. The HEX provides fluorescent X-rays of 5 keV to 100 keV with fluence of 10^5–10^6 photons/cm^2/second at the desired line energy. Low energy lines can be filtered, and both filters and fluorescers can be changed rapidly. We present results of calibrating image plates (sensitivity and modulation transfer function), a Bremsstrahlung spectrometer (stacked filters and image plates), and the National Ignition Facility’s Filter- Fluorescer Experiment (FFLEX) high energy X-ray spectrometer. We also show results of a scintillator light yield and alignment study for a neutron imaging system.
Date: June 5, 2009
Creator: Ali, Zaheer
Partner: UNT Libraries Government Documents Department

X-ray Diffraction Crystal Calibration and Characterization

Description: National Security Technologies’ X-ray Laboratory is comprised of a multi-anode Manson type source and a Henke type source that incorporates a dual goniometer and XYZ translation stage. The first goniometer is used to isolate a particular spectral band. The Manson operates up to 10 kV and the Henke up to 20 kV. The Henke rotation stages and translation stages are automated. Procedures have been developed to characterize and calibrate various NIF diagnostics and their components. The diagnostics include X-ray cameras, gated imagers, streak cameras, and other X-ray imaging systems. Components that have been analyzed include filters, filter arrays, grazing incidence mirrors, and various crystals, both flat and curved. Recent efforts on the Henke system are aimed at characterizing and calibrating imaging crystals and curved crystals used as the major component of an X-ray spectrometer. The presentation will concentrate on these results. The work has been done at energies ranging from 3 keV to 16 keV. The major goal was to evaluate the performance quality of the crystal for its intended application. For the imaging crystals we measured the laser beam reflection offset from the X-ray beam and the reflectivity curves. For the curved spectrometer crystal, which was a natural crystal, resolving power was critical. It was first necessary to find sources of crystals that had sufficiently narrow reflectivity curves. It was then necessary to determine which crystals retained their resolving power after being thinned and glued to a curved substrate.
Date: June 5, 2009
Creator: Haugh, Michael J.; Stewart, Richard & Kugland, Nathan
Partner: UNT Libraries Government Documents Department

ITER Core Imaging X-Ray Spectrometer Conceptual Design and Performance Assessment - Phase 2

Description: During Phase 2 of our study of the CIXS conceptual design we have tackled additional important issues that are unique to the ITER environment. These include the thermal control of the crystal and detector enclosures located in an environment with a 100-250 C ambient temperature, tritium containment, and the range of crystal and detector movement based on the need for spectral adjustments and the desire to make measurements of colder plasmas. In addressing these issues we have selected a ''Dewar''-type enclosure for the crystals and detectors. Applying realistic view factors for radiant heat and making allowance for conduction we have made engineering studies of this enclosure and showed that the cooling requirements can be solved and the temperature can be kept sufficiently constant without compromising the specification parameters of the CIXS. We have chosen a minimum 3 mm combined thickness of the six beryllium windows needed in a Dewar-type enclosure and showed that a single window of 0.5 mm thickness satisfies tritium containment requirements. For measuring the temperature in cooler ITER plasmas, we have chosen to use the K-shell lines of Fe24+. Iron is the preferred choice because its radiation can be analyzed with the identical CIXS settings used for analyzing the tungsten radiation, i.e., essentially no adjustments besides a simple crystal rotation need to be made. We have, however, included an xy{theta}-drive motor arrangement in our design for fine adjustments and full rotation of the crystal mounts.
Date: January 2, 2011
Creator: Beiersdorfer, P; Wen, J; Dunn, J & Morris, K
Partner: UNT Libraries Government Documents Department

Atomic data for the ITER Core Imaging X-ray Spectrometer

Description: The parameters of the ITER core plasmas will be measured using the Core Imaging X-ray Spectrometer (CIXS), a high-resolution crystal spectrometer focusing on the L-shell spectra of highly ionized tungsten atoms. In order to correctly infer the plasma properties accurate atomic data are required. Here, some aspects of the underlying physics are discussed using experimental data and theoretical predictions from modeling.
Date: June 15, 2012
Creator: Clementson, J.; Beiersdorfer, P.; Biedermann, C.; Bitter, M.; Delgado-Aparicio, L. F.; Graf, A. et al.
Partner: UNT Libraries Government Documents Department

Soft x-ray images of the Laser Entrance Hole of NIC Hohlraums (paper, HTPD2012)

Description: Hohlraums at the National Ignition Facility convert laser energy into a thermal x-radiation drive, which implodes the capsule, thus compressing the fuel. The x-radiation drive is measured with a low resolution, time-resolved x-ray spectrometer that views the hohlraum's laser entrance hole (LEH) at 37{sup o} to the hohlraum axis. This measurement has no spatial resolution. To convert this to the drive inside the hohlraum, the area and fraction of the measured x-radiation which comes from the region inside the hohlraum must be known. The size of the LEH is measured with the time integrated Static X-ray Imager (SXI) which view the LEH at 18{sup o} to the hohlraum axis. A soft x-ray image has been added to the SXI to measure the fraction of x-radiation inside the LEH's Clear Aperture in order to correct the measured radiation. A multilayer mirror plus filter selects an x-ray band centered at 870 eV, near the x-ray energy peak of a 300 eV blackbody. Results from this channel and corrections to the x-radiation drive are discussed.
Date: April 30, 2012
Creator: Schneider, M. B. & Meezan, N. B.
Partner: UNT Libraries Government Documents Department

Soft x-ray spectrometer operation at the National Ignition Facility

Description: Radiation drive diagnostics during the NIF early light campaign was supported by an 18 channel soft x-ray spectrometer (Dante). In order to achieve a measurement accuracy of 2% in radiation temperature absolute calibration of the individual channels was necessary and signal distortion through long transmission lines had to be compensated for as well. For fast signals the signal attenuation due to the long (50m) cables amounted to {approx} 20% {at} 100MHz, which was corrected by a cable compensation in the frequency domain. The varying effects of cable distortion for a variety of signals between 1ns and 9ns in length were evaluated and corrections were applied. Results of the thus calculated temperatures of the NEL campaign will be presented compared to LASNEX predictions, showing agreement in peak radiation temperature within less than 2%.
Date: April 25, 2006
Creator: Schein, J.; Dewald, E.; Campbell, K.; Turner, R.; Weber, F.; Rhodes, M. et al.
Partner: UNT Libraries Government Documents Department

Development and testing of laser-induced breakdown spectroscopy for the Mars Rover Program : elemental analysis at stand-off distances

Description: One of the most Fundamental pieces of information about any planetary body is the elemental cornposition of its surface materials. The Viking Martian landers employed XRF (x-ray fluorescence) and the MER rovers are carrying APXS (alpha-proton x-ray spectrometer) instruments upgraded from that used on the Pathfinder rover to supply elemental composition information for soils and rocks for which direct contact is possible. These in-situ analyses require that the lander or rover be in contact with the sample
Date: January 1, 2003
Creator: Cremers, D. A. (David A.); Wiens, R. C. (Roger C.); Arp, Z. A. (Zane A.); Harris, R. D. (Ronny D.) & Maurice, S. (Sylvestre)
Partner: UNT Libraries Government Documents Department