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Structure-dependent hydrostatic deformation potentials of individual single-walled carbon nanotubes

Description: Summary: The hydrostatic pressure coefficients of interband transition energies of a number of single-walled carbon nanotubes with different chiralities were measured. Both optical absorption and photoluminescence experiments were performed on de-bundled, single-walled carbon nanotube suspensions with hydrostatic pressure applied by diamond anvil cells. The pressure coefficients of the first van Hove transition (bandgap) energies are negative and dependent on the nanotube structure, while the second van Hove transitions are much less sensitive to hydrostatic pressure. The hydrostatic deformation potentials of individual nanotubes are deduced within an elastic model. An empirical equation that relates the pressure coefficients to nanotube structure is presented and discussed.
Date: November 7, 2003
Creator: Wu, J.; Walukiewicz, W.; Shan, W.; Bourret-Courchesne, E. D.; Ager, J. W., III; Yu, K. M. et al.
Partner: UNT Libraries Government Documents Department

Hydrostatic Mooring System

Description: This report is a summary of the following topics of the first quarter of 2000: (1) Han Padron Associates (HPA) provided conceptual structural design of the mooring buoy; and (2) they completed partial review of the HPA design and designed the sealing elements.
Date: April 25, 2000
Creator: Korsgaarb, Jens
Partner: UNT Libraries Government Documents Department

The Hydrostatic Mooring System. Quarterly Report for the Period April-June 2000

Description: The following topics are summarized for the 2nd quarter of 2000: (1) We amended the structural design of the buoy, moving the horizontal bulkhead from the bottom to the top of the buoy. (2) We designed the main bearing using Hilman Rollers. We discarded a parallel design using Lubron slide bearings due to concerns about keeping dirt out of the sliding surfaces. (3) We performed a preliminary failure tree risk analysis for the system as required by ABS. (4) We made various drawings of the system and sub-components.
Date: July 15, 2000
Creator: Korsgaard, Jens
Partner: UNT Libraries Government Documents Department

Shallow Flaws Under Biaxial Loading Conditions, Part II: Application of a Weibull Stress Analysis of the Cruciform Bend Specimen Using a Hydrostatic Stress Criterion

Description: Cruciform beam fracture mechanics specimensl have been developed in the Heavy Section Steel Technology (HSST) Program at Oak Ridge National Laboratory (ORNL) to introduce a prototypic, far- field, out-of-plane biaxird bending stress component in the test section that approximates the nonlinear biaxial stresses resulting from pressurized-thernxd-shock or pressure-temperature loading of a nuclear reactor pressure vessel (RPV). Matrices of cruciform beam tests were developed to investigate and quantify the effects of temperature, biaxial loading, and specimen size on fracture initiation toughness of two-dimensional (constant depth), shtdlow, surface flaws. Tests were conducted under biaxial load ratios ranging from uniaxial to equibiaxial. These tests demonstrated that biaxial loading can have a pronounced effect on shallow-flaw fracture toughness in the lower transition temperature region for RPV materials. Two and three- parameter Weibull models have been calibrated using a new scheme (developed at the University of Illinois) that maps toughness data from test specimens with distinctly different levels of crack-tip constraint to a small scale yielding (SSY) Weibull stress space. These models, using the new hydrostatic stress criterion in place of the more commonly used maximum principal stress in the kernel of the OW integral definition, have been shown to correlate the experimentally observed biaxiaI effect in cruciform specimens, thereby providing a scaling mechanism between uniaxial and biaxial loading states.
Date: August 1999
Creator: Bass, B. R.; McAfee, W. J. & Williams, P. T.
Partner: UNT Libraries Government Documents Department

A new hydrostatic leveling system developed for the Advanced Photon Source.

Description: As a result of the calibration tests performed with the first prototype units using the new measurement principle, we believe that the described leveling method is stable and accurate to the micron level with a sufficiently large range for the expected elevation changes of the support girders used in the Advanced Photon Source (APS) storage ring. Although long-term studies with this system have not been conducted, we believe that after installation this system requires little or no servicing for long periods of time. The methods described in this paper cover only the elevation changes of individual vessels. However, changes in the tilt of a girder must also be known. Therefore, a combination of tiltmeters in conjunction with this hydrostatic level system (HLS) would be most suitable for measuring the tilt and elevation changes of the APS girders.
Date: September 18, 1998
Creator: Kivioja, L. A.
Partner: UNT Libraries Government Documents Department

Pressure dependence of donor excitation spectra in AlSb

Description: We have investigated the behavior of ground to bound excited-state electronic transitions of Se and Te donors in AlSb as a function of hydrostatic pressure. Using broadband far-infrared Fourier transform spectroscopy, we observe qualitatively different behaviors of the electronic transition energies of the two donors. While the pressure derivative of the Te transition energy is small and constant, as might be expected for a shallow donor, the pressure derivatives of the Se transition energies are quadratic and large at low pressures, indicating that Se is actually a deep donor. In addition, at pressures between 30 and 50 kbar, we observe evidence of an anti-crossing between one of the selenium electronic transitions and a two-phonon mode.
Date: January 16, 2002
Creator: Hsu, L.; McCluskey, M.D. & Haller, E.E.
Partner: UNT Libraries Government Documents Department

Hydrostatic compaction of Microtherm HT.

Description: Two samples of jacketed Microtherm{reg_sign}HT were hydrostatically pressurized to maximum pressures of 29,000 psi to evaluate both pressure-volume response and change in bulk modulus as a function of density. During testing, each of the two samples exhibited large irreversible compactive volumetric strains with only small increases in pressure; however at volumetric strains of approximately 50%, the Microtherm{reg_sign}HT stiffened noticeably at ever increasing rates. At the maximum pressure of 29,000 psi, the volumetric strains for both samples were approximately 70%. Bulk modulus, as determined from hydrostatic unload/reload loops, increased by more than two-orders of magnitude (from about 4500 psi to over 500,000 psi) from an initial material density of {approx}0.3 g/cc to a final density of {approx}1.1 g/cc. An empirical fit to the density vs. bulk modulus data is K = 492769{rho}{sup 4.6548}, where K is the bulk modulus in psi, and {rho} is the material density in g/cm{sup 3}. The porosity decreased from 88% to {approx}20% indicating that much higher pressures would be required to compact the material fully.
Date: September 1, 2010
Creator: Broome, Scott Thomas & Bauer, Stephen J.
Partner: UNT Libraries Government Documents Department

Hydrostatic, uniaxial, and triaxial compression tests on unpoled "Chem-prep" PZT 95/5-2Nb ceramic within temperature range of -55 to 75 degrees C.

Description: Sandia is currently developing a lead-zirconate-titanate ceramic 95/5-2Nb (or PNZT) from chemically prepared ('chem-prep') precursor powders. Previous PNZT ceramic was fabricated from the powders prepared using a 'mixed-oxide' process. The specimens of unpoled PNZT ceramic from batch HF803 were tested under hydrostatic, uniaxial, and constant stress difference loading conditions within the temperature range of -55 to 75 C and pressures to 500 MPa. The objective of this experimental study was to obtain mechanical properties and phase relationships so that the grain-scale modeling effort can develop and test its models and codes using realistic parameters. The stress-strain behavior of 'chem-prep' PNZT under different loading paths was found to be similar to that of 'mixed-oxide' PNZT. The phase transformation from ferroelectric to antiferroelectric occurs in unpoled ceramic with abrupt increase in volumetric strain of about 0.7 % when the maximum compressive stress, regardless of loading paths, equals the hydrostatic pressure at which the transformation otherwise takes place. The stress-volumetric strain relationship of the ceramic undergoing a phase transformation was analyzed quantitatively using a linear regression analysis. The pressure (P{sub T1}{sup H}) required for the onset of phase transformation with respect to temperature is represented by the best-fit line, P{sub T1}{sup H} (MPa) = 227 + 0.76 T (C). We also confirmed that increasing shear stress lowers the mean stress and the volumetric strain required to trigger phase transformation. At the lower bound (-55 C) of the tested temperature range, the phase transformation is permanent and irreversible. However, at the upper bound (75 C), the phase transformation is completely reversible as the stress causing phase transformation is removed.
Date: October 1, 2003
Creator: Zeuch, David Henry; Montgomery, Stephen Tedford; Lee, Moo Yul & Hofer, John H.
Partner: UNT Libraries Government Documents Department

Do grain boundaries in nanophase metals slide?

Description: Nanophase metallic materials show a maximum in strength as grain size decreases to the nano scale, indicating a break down of the Hall-Petch relation. Grain boundary sliding, as a possible accommodation mechanisms, is often the picture that explain computer simulations results and real experiments. In a recent paper, Bringa et al. Science 309, 1838 (2005), we report on the observation of an ultra-hard behavior in nanophase Cu under shock loading, explained in terms of a reduction of grain boundary sliding under the influence of the shock pressure. In this work we perform a detailed study of the effects of hydrostatic pressure on nanophase Cu plasticity and find that it can be understood in terms of pressure dependent grain boundary sliding controlled by a Mohr-Coulomb law.
Date: October 27, 2006
Creator: Bringa, E M; Leveugle, E & Caro, A
Partner: UNT Libraries Government Documents Department

On the Micromechanisms of Shock-Induced Martensitic Transformation in Tantalum

Description: Shock-induced twinning and martensitic transformation in tantalum, which exhibits no solid-state phase transformation under hydrostatic pressures up to 100 GPa, have been further investigated. Since the volume fraction and size of twin and phase domains are small in scale, they are considered foming by heterogeneous nucleation that is catalyzed by high density lattice dislocations. A dynamic dislocation mechanism is accordingly proposed based upon the observation of dense dislocation clustering within shock-recovered tantalum. The dense dislocation clustering can cause a significant increase of strain energy in local regions of {beta} (bcc) matrix, which renders mechanical instability and initiates the nucleation of twin and phase domains through the spontaneous reactions of dislocation dissociation within the dislocation clusters. That is, twin domains can be nucleated within the clusters through the homogeneous dissociation of 1/2<111> dislocations into 1/6<111> partial dislocations, and {omega} phase domains can be nucleated within the closters through the inhomogeneous dissociation of 1/2<111> dislocations into 1/12<111>, 1/3<111> and 1/12<111> partial dislocations.
Date: December 7, 2005
Creator: Hsiung, L L
Partner: UNT Libraries Government Documents Department


Description: This paper describes the mathematical modeling and initial testing of an oil-hydrostatic bearing that derives compensation from both a central radial slit where fluid enters and stepped clearances near each end. Bearings using either a radial slit or stepped clearances for compensation were well studied over forty years ago by Donaldson. These bearings have smooth bores uninterrupted with multiple recesses around the circumference. The present slit-step bearing achieves the best of both types with somewhat higher hydrostatic stiffness than the slit bearing and fluid shear drag lower than the step bearing. This is apparent in TABLE 1, which compares calculated values of initial (i.e., centered) hydrostatic stiffness for each type. The slit-step bearing is one of several types being studied at Lawrence Livermore National Laboratory for possible use on the Precision Optical Grinder and Lathe (POGAL).
Date: July 28, 2006
Creator: Hale, L C; Donaldson, R R; Castro, C; Chung, C A & Hopkins, D J
Partner: UNT Libraries Government Documents Department

Effect of pressure on the electrical resistivity and magnetism in UPdSn

Description: The electrical resistivity of a UPdSn single crystal exerted to various hydrostatic pressures was measured as a function of temperature and magnetic field. Clear anomalies in the temperature dependence of resistivity along the c-axis mark the magnetic phase transitions between paramagnetic and antiferromagnetic (AF) state at TN and the AF 1 -AF2 transition at T I .L arge negative magnetoresistance effects have been observed not only in the AF state as a result of the metamagnetic transition to canted structure ai B,, but also at temperatures far above TN. The latter result is attributed to the existence of AF correlations or short range AF ordering in the paramagnetic range. The value of TN increases with increasing applied pressure, whereas TI simultaneously decreases. It is also found that 13, decreases with increasing pressure. As a consequence, the stability range of the AF- 1 phase expands with applied pressure partially on account of the ground-state AF-2 phase.
Date: January 1, 2002
Creator: Honda, F.; Alsmadi, A. K. (Abdel Khaleq); Sechovsky, V. (Vladimir); Kamarad, J.; Nakotte, H. (Heinrich); Lacerda, A. H. (Alex H.) et al.
Partner: UNT Libraries Government Documents Department

Precise and Accurate Density Determination of Explosives Using Hydrostatic Weighing

Description: Precise and accurate density determination requires weight measurements in air and water using sufficiently precise analytical balances, knowledge of the densities of air and water, knowledge of thermal expansions, availability of a density standard, and a method to estimate the time to achieve thermal equilibrium with water. Density distributions in pressed explosives are inferred from the densities of elements from a central slice.
Date: July 1, 2005
Creator: Olinger, B.
Partner: UNT Libraries Government Documents Department

A High Precision Double Tubed Hydrostatic Leveling System for Accelerator Alignment Applications

Description: Since 1998 several hydrostatic leveling systems (HLS) have been installed in different locations at Fermilab. This work was in collaboration with Budker Institute and SLAC. All systems were either half-filled pipe (HF) or full-filled pipe (FF). Issues assembling HLS are covered in this article. An improved and cost-effective water system with temperature stabilized of water media is presented. This proposal is a double-tube full-filled DT-FF system. Examples of hardware configurations are included for systems located at Fermilab.
Date: September 1, 2006
Creator: Singatulin, Shavkat; Volk, J.; Shiltsev, V.; Chupyra, A.; Medvedko, A. & Kondaurov, M.
Partner: UNT Libraries Government Documents Department

The L_X-M relation of Clusters of Galaxies

Description: We present a new measurement of the scaling relation between X-ray luminosity and total mass for 17,000 galaxy clusters in the maxBCG cluster sample. Stacking sub-samples within fixed ranges of optical richness, N200, we measure the mean 0.1-2.4 keV X-ray luminosity, <L{sub X}>, from the ROSAT All-Sky Survey. The mean mass, <M{sub 200}>, is measured from weak gravitational lensing of SDSS background galaxies (Johnston et al. 2007). For 9 {le} N{sub 200} < 200, the data are well fit by a power-law, <L{sub X}>/10{sup 42} h{sup -2} ergs{sup -1} = (12.6{sub -1.3}{sup +1.4}(stat) {+-} 1.6 (sys)) (<M{sub 200}>/10{sup 14} h{sup -1} M{sub {circle_dot}}){sup 1.65{+-}0.13}. The slope agrees to within 10% with previous estimates based on X-ray selected catalogs, implying that the covariance in L{sub X} and N{sub 200} at fixed halo mass is not large. The luminosity intercept is 30%, or 2{sigma}, lower than determined from the X-ray flux-limited sample of Reiprich & Boehringer (2002), assuming hydrostatic equilibrium. This slight difference could arise from a combination of Malmquist bias and/or systematic error in hydrostatic mass estimates, both of which are expected. The intercept agrees with that derived by Stanek et al. (2006) using a model for the statistical correspondence between clusters and halos in a WMAP3 cosmology with power spectrum normalization {sigma}{sub 8} = 0.85. Similar exercises applied to future data sets will allow constraints on the covariance among optical and hot gas properties of clusters at fixed mass.
Date: May 16, 2008
Creator: Rykoff, E.S.; Evrard, A.E.; McKay, T.A.; Becker, M.R.; Johnston, D.E.; Koester, B.P. et al.
Partner: UNT Libraries Government Documents Department

Failure of a fiber composite lamina under three-dimensional stresses

Description: The efficient use of thick-section fiber composites requires a proven three-dimensional failure model. Numerous failure criteria have been proposed, but the lack of critical experimental results makes it difficult to assess the accuracy of these models. It is shown that the various predictions for failure of a lamina due to the simple state of uniaxial stress plus superposed hydrostatic pressure are disparate. These differences are sufficient to allow evaluation of failure criteria using data that has the normal scatter found for composite materials. A high-pressure test system for fiber composites is described and results for the effects of pressure on the transverse and longitudinal compression strengths of a carbon fiber/epoxy lamina are discussed. Results are compared with a few representative failure models.
Date: August 31, 1999
Creator: DeTeresa, S. J.
Partner: UNT Libraries Government Documents Department

On the quasihydrostatic flows of radiatively cooling self-gravitating gas clouds

Description: Two model problems are considered, illustrating the dynamics of quasihydrostatic flows of radiatively cooling, optically thin self-gravitating gas clouds. In the first problem, spherically symmetric flows in an unmagnetized plasma are considered. For a power-law dependence of the radiative loss function on the temperature, a one-parameter family of self-similar solutions is found. The authors concentrate on a constant-mass cloud, one of the cases, when the self-similarity indices are uniquely selected. In this case, the self-similar flow problem can be formally reduced to the classical Lane-Emden equation and therefore solved analytically. The cloud is shown to undergo radiative condensation, if the gas specific heat ratio {gamma} > 4/3. The condensation proceeds either gradually, or in the form of (quasihydrostatic) collapse. For {gamma} < 4/3, the cloud is shown to expand. The second problem addresses a magnetized plasma slab that undergoes quasihydrostatic radiative cooling and condensation. The problem is solved analytically, employing the Lagrangian mass coordinate.
Date: March 1, 1995
Creator: Meerson, B.; Megged, E. & Tajima, T.
Partner: UNT Libraries Government Documents Department

Uniaxial Compression Experiments on PZT 95/5-2Nb Ceramic: Evidence for an Orientation-Dependent, ''Maximum Compressive Stress'' Criterion for Onset of the F(R1)()A(O) Polymorphic Phase Transformation

Description: Some time ago we presented evidence that, under nonhydrostatic loading, the F{sub R1} {r_arrow} A{sub O} polymorphic phase transformation in unpoled PZT 95/5-2Nb ceramic began when the maximum compressive stress equaled the hydrostatic pressure at which the transformation otherwise took place. More recently, we showed that this simple stress criterion did not apply to nonhydrostatically compressed, poled ceramic. However, unpoled ceramic is isotropic, whereas poled ceramic has a preferred crystallographic orientation and is mechanically anisotropic. If we further assume that the transformation depends not only on the magnitude of the compressive stress, but also its orientation relative to some feature(s) of PZT 95/5-2Nb's crystallography, then these disparate results can be qualitatively resolved. In this report, we first summarize the existing results for unpoled and poled ceramic. Using our orientation-dependent hypothesis and these results, we derive simple arithmetic expressions that accurately describe our previously-observed effects of nonhydrostatic stress on the transformation of unpoled ceramic. We then go on to test new predictions based on the orientation-dependent model. It has long been known that the transformation can be triggered in uniaxial compression: the model specifically requires a steadily increasing axial stress to drive the transformation of a randomly-oriented polycrystal to completion. We show that when the stress is held constant during uniaxial compression experiments, the transformation stops, supporting our hypothesis. We close with a discussion of implications of our model, and ways to test it using poled ceramic.
Date: January 1, 1999
Creator: Carlson, L.W.; Grazier, J.M.; Holcomb, D.J.; Montgomery, S.T. & Zeuch, D.H.
Partner: UNT Libraries Government Documents Department

HFIR Vessel Probabilistic Fracture Analysis, Considering Success of Hydrostatic Proof Tests

Description: Periodic hydrostatic proof testing and probabilistic fracture mechanics analyses are performed to demonstrate the structural integrity and useful life of the High Flux Isotope Reactor (HFIR) pressure vessel. Calculations of the hydro-test conditions (pressure, temperature, and frequency) and of the probability of failure account for vessel degradation (flaw growth and radiation-induced embrittlement) that takes place between tests and of the credible worst-case-operating condition. The specified useful life of the vessel is limited by specified maximum permissible calculated probabilities of failure for hydro-test and worst-case-operating conditions. The probability of failure can be calculated with or without accounting for the success (absence of failure) of a test, but if success is accounted for, the calculated probabilities are less and thus the maximum permissible life greater. This report describes a simple method for including the success of a test.
Date: January 1, 1999
Creator: Cheverton, R.D.
Partner: UNT Libraries Government Documents Department

The Dielectric Properties and Phase Transitions of [Pb(Zn{sub 1/3}Nb{sub 2/3})O{sub 3}]{sub 0.905} (PbTiO{sub 3}){sub 0.095}: Influence of Pressure

Description: Studies of the influences of temperature, hydrostatic pressure, dc biasing field and frequency on the dielectric constant ({epsilon}{prime}) and loss (tan {delta}) of single crystal [pb (Zn{sub 1/3}Nb{sub 2/3})O{sub 3}]{sub 0.905} (PbTiO{sub 3}){sub 0.095}, or PZN-9.5PT for short, have provided a detailed view of the ferroelectric (FE) response and phase transitions of this technologically important material. While at 1 bar, the crystal exhibits on cooling a cubic-to-tetragonal FE transition followed by a second transition to a rhombohedral phase, pressure induces a FE-to-relaxer crossover, the relaxer phase becoming the ground state at pressures {ge}5 kbar. Analogy with earlier results suggests that this crossover is a common feature of compositionally-disordered soft mode ferroelectrics and can be understood in terms of a decrease in the correlation length among polar domains with increasing pressure. Application of a dc biasing electric field at 1 bar strengthens FE correlations, and can at high pressure re-stabilize the FE response. The pressure-temperature-electric field phase diagram was established. In the absence of dc bias the tetragonal phase vanishes at high pressure, the crystal exhibiting classic relaxor behavior. The dynamics of dipolar motion and the strong deviation from Curie-Weiss behavior of the susceptibility in the high temperature cubic phase are discussed.
Date: August 1, 2000
Partner: UNT Libraries Government Documents Department

Forward-in-Time Differencing for Fluids: Nonhydrostatic Modeling of Rotating Stratified Flow on a Mountainous Sphere

Description: Traditionally, numerical models for simulating planetary scale weather and climate employ the hydrostatic primitive equations-an abbreviated form of Navier-Stokes equations that neglect vertical accelerations and use simplified inertial forces. 1 Although there is no evidence so far that including nonhydrostatic effects in global models has any physical significance for large scale solutions, there is an apparent trend in the community toward restoring Navier-Stokes equations (or at least their less constrained forms) in global models of atmospheres and oceans. The primary motivation for this is that the state-of-the-art computers already admit resolutions where local nonhydrostatic effects become noticeable. Other advantages include: the convenience of local mesh refinement; better overall accuracy; insubstantial computational overhead relative to hydrostatic models; universality and therefore convenience of maintaining a single large code; as well as conceptual simplicity and mathematical elegancy--features important for education. The few existing nonhydrostatic global models differ in analytic formulation and numerical design, reflecting their different purposes and origins. Much of our present research improves the design of a high-performance numerical model for simulating the flows of moist (and precipitating), rotating, stratified fluids past a specified time-dependent irregular lower boundary. This model is representative of a class of nonhydrostatic atmospheric codes employing the an elastic equations of motion in a terrain-following curvilinear framework, and contains parallel implementations of semi-Lagrangian and Eulerian approximations selectable by the user. The model has been employed in a variety of applications; the quality of results suggest that modern nonoscillatory forward-in-time (NFT) methods are superior to the more traditional centered-in-time-and-space schemes, in terms of accuracy, computational efficiency, flexibility and robustness.
Date: March 31, 1999
Creator: Smolarkiewicz, P.K.; Grubisic, V. & Margolin, L.G.
Partner: UNT Libraries Government Documents Department