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Recovery of deformed and hydrogen-charge palladium

Description: Positron lifetime and Doppler-broadening studies made at 300 K have been used to investigate the interaction between interstitial hydrogen and lattice defects in deformed Pd. Specimens were charged with hydrogen at 300 K to levels up to 0.1%. The presence of hydrogen was found to have no effect on the recovery curves of Pd upon annealing to 400/sup 0/C. By 400/sup 0/C the values for both lifetime and Doppler-broadening for both cold worked and cold worked plus hydrogen were below the values obt… more
Date: January 1, 1982
Creator: Snead, C. L. Jr.; Lynn, K. G. & Lynch, J. F.
Partner: UNT Libraries Government Documents Department
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Discussion: ''toughness variations during the tempering of a plain carbon martensitic steel'' by J. E. King, R. F. Smith and J. F. Knott. Retained austenite and transgranular tempered martensite embrittlement

Description: Discussion is presented to substantiate, clarify and reinterpret some of the results of the above authors for the existence and origin of tempered martensite embrittlement (TME) in relation to retained austenite, with reference to the experimental steels worked at LBL for the past several years.
Date: June 1, 1977
Creator: Rao, B.V.N. & Thomas, G.
Partner: UNT Libraries Government Documents Department
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High temperature ceramic membrane reactors for coal liquid upgrading

Description: In this project we intend to study a novel process concept, i.e, the use of ceramic membranes reactors in upgrading of coal derived liquids. Membrane reactors have been used in a number of catalytic reaction processes in order to overcome the limitations on conversion imposed by thermodynamic equilibrium. They have, furthermore, the inherent capability for combining reaction and separation in a single step. Thus they offer promise for improving and optimizing yield, selectivity and performance … more
Date: January 1, 1992
Creator: Tsotsis, T.T.
Partner: UNT Libraries Government Documents Department
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High-energy proton radiation damage of high-purity germanium detectors

Description: Motivated by their applicability to gamma-ray spectroscopy experiments in space, quantitative studies of radiation damage effects in high-purity germanium detectors due to high-energy charged particles have been initiated with the irradiation by 6 GeV/c protons of two 1.0 cm thick planar detectors maintained at 88/sup 0/K. The threshold for resolution degradation and the annealing characteristics differs markedly from those previously observed for detectors irradiated by fast neutrons. Under pr… more
Date: October 1, 1977
Creator: Pehl, R.H.; Varnell, L.S. & Metzger, A.E.
Partner: UNT Libraries Government Documents Department
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Interaction of noble-metal fission products with pyrolytic silicon carbide

Description: Fuel particles for the High-Temperature Gas-Cooled Reactor (HTGR) contain layers of pyrolytic carbon and silicon carbide, which act as a miniature pressure vessel and form the primary fission product barrier. Of the many fission products formed during irradiation, the noble metals are of particular interest because they interact significantly with the SiC layer and their concentrations are somewhat higher in the low-enriched uranium fuels currently under consideration. To study fission product-… more
Date: January 1, 1982
Creator: Lauf, R. J. & Braski, D. N.
Partner: UNT Libraries Government Documents Department
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Laser annealing of ion implanted CZ silicon for solar cell junction formation. Quarterly report No. 2

Description: Results on a contract to evaluate the merits of large spot size pulsed laser annealing of ion implanted silicon wafers for junction formation in solar cells are reported. Investigations on homogenization of the laser beam were continued. In addition to the 30 mm diameter fused silica rod with a 90/sup 0/ bend configuration, quartz tubes were obtained and briefly tried. Best results were obtained with the rod homogenizer. Laser annealing experimentation resulted in complete recrystallization of … more
Date: October 1, 1980
Creator: Katzeff, J. S.
Partner: UNT Libraries Government Documents Department
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Energy dependence of metallic-encapsulated thermoluminescent dosimeters. Annual report

Description: The gamma-ray energy responses of encapsulated /sup 7/LiF and CaF/sub 2/:Mn thermoluminescent dosimeters were measured and compred to calculated values. This study was performed in order to improve the accuracy of gamma-ray heating measurements made in polyenergetic gamma-ray fields such as Argonne National Laboratory's Zero Power Reactors. Equations used in the development of the TERC/III computer code and code input parameters are specified. A section on TLD precision is also included. Compar… more
Date: June 1980
Creator: Simons, G. G.
Partner: UNT Libraries Government Documents Department
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Coal Technology Program. Progress report for November 1977

Description: A block of Pittsburgh seam bituminous coal and a block of Wyodak subbituminous coal were pyrolyzed under reducing gas in support of in situ gasification. Information from previously completed block pyrolysis of bituminous coal under an argon atmosphere show that differences in evolved gas result from differences in heating rates. Compared to block pyrolysis at 0.3 C/sup 0//min, block pyrolysis at 3 C/sup 0//min produces less gas but gas with a higher heating value, yielding a higher overall pyr… more
Date: January 1, 1978
Partner: UNT Libraries Government Documents Department
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Catalytic steam gasification of bagasse for the production of methanol

Description: Pacific Northwest Laboratory (PNL) tested the catalytic gasification of bagasse for the production of methanol synthesis gas. The process uses steam, indirect heat, and a catalyst to produce synthesis gas in one step in fluidized bed gasifier. Both laboratory and process development scale (nominal 1 ton/day) gasifiers were used to test two different catalyst systems: (1) supported nickel catalysts and (2) alkali carbonates doped on the bagasse. This paper presents the results of laboratory and … more
Date: December 1, 1983
Creator: Baker, E.G. & Brown, M.D.
Partner: UNT Libraries Government Documents Department
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Investigations of CuInSe sub 2 Thin Films and Contacts

Description: This report describes research into electrical contacts for copper indium diselenide (CuInSe{sub 2}) polycrystalline thin films used for solar cell applications. Molybdenum contacts have historically been the most promising for heterojunction solar cells. This program studied contact stability by investigating thermally induced bilayer reactions between molybdenum and copper, indium, and selenium. Because selenization is widely used to fabricate CuInSe{sub 2} thin films for photovoltaic cells, … more
Date: October 1, 1991
Creator: Nicolet, M. A.
Partner: UNT Libraries Government Documents Department
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Optimization of steam explosion pretreatment. Final report

Description: Different operating conditions are required to optimize the yield from each of the various fractions in the substrate. Xylose recovery is maximized at short cooking times whereas maximum lignin recovery requires much longer cooking times. Peak glucose yield and rumen digestibility occur at intermediate times. If process conditions are set for maximum glucose yield we have achieved a yield of 68% of the theoretical, based on an average of a dozen substrates tested. Individual results ranged from… more
Date: April 1, 1980
Creator: Foody, P.
Partner: UNT Libraries Government Documents Department
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Silicon ingot casting: Heat Exchanger Method (HEM)/multi-wire slicing: Fixed Abrasive Slicing Technique (FAST), Phase IV. Quarterly progress report No. 2, April 1, 1980-June 30, 1980

Description: Silicon ingot size cast by HEM has been extended to 34 cm x 34 cm x 10 cm. A 20 kg ingot has been solidified at 3 kg/hr with no crucible attachment or ingot cracking problems. Another ingot of 26 kg weight has also been solidified. The heat treatment used to develop a graded structure caused cracking on the inside surface of the first large crucibles. The thermal conditions were altered to minimize high gradients and the cracking was eliminated. A high degree of single crystallinity has been ma… more
Date: August 1, 1980
Creator: Schmid, F.; Khattak, C.P. & Basaran, M.
Partner: UNT Libraries Government Documents Department
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Cadmium sulfide/copper ternary heterojunction cell research. Final report, January 8, 1979-June 7, 1980

Description: Dual source, Se and CuInSe/sub 2/, coevaporation and flash evaporation of stoichiometric CuInSe/sub 2/ powder were investigated to develop a process of fabricating large area CdS/CuInSe/sub 2/ heterojunction solar cells. CuInSe/sub 2/ was seen to decompose upon evaporation, producing layered films in the dual source system. Annealing of these films and alternative dual sources have been considered. Single phase p type films have been produced but no devices have been made from such films. Flash… more
Date: January 1, 1980
Creator: Fleming, D. L.
Partner: UNT Libraries Government Documents Department
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Improved tunnel resistance of silvered-polymer mirrors

Description: This report documents the research performed at the Solar Energy Research Institute during fiscal year (FY) 1991 to develop ways to prevent delamination failure (known as tunneling) of silvered-polymer reflector materials. Several promising approaches have been identified and demonstrated that substantially reduce such failures. These approaches include (1) use of Tedlar edge tape rather than the manufacturer-recommended ECP-244 tape, (2) thermal treatment of laminated reflector/substrate const… more
Date: October 1, 1991
Creator: Jorgensen, G.; Schissel, P.; Kennedy, C.; Shinton, Y.; Powell, D. & Siebarth, J.
Partner: UNT Libraries Government Documents Department
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Effect of cation exchange on the subsequent reactivity of lignite chars to steam. [108 references]

Description: The purpose of this investigation is to determine the role which cations in coal play in the subsequent reactivity of chars. It is hoped that this investigation will aid in an understanding of the catalytic nature of inorganic constituents in coal during its gasification. It was found that increased heat treatment temperature decreased reactivity. The decrease in reactivity was shown to be due, at least in part, to the changes in the nature of the cation with increased heat treatment temperatur… more
Date: March 1, 1977
Creator: Hippo, E. J. & Walker, Jr., P. L.
Partner: UNT Libraries Government Documents Department
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Experimental investigation of the chemistry of excited states of rare gases. First quarterly progress report, October 15, 1977--January 15, 1978

Description: The quenching of XeF(B) was studied using the steady-state photolysis of XeF/sub 2/ as the source of XeF(B). The product states from the sensitized reaction of Xe(/sup 3/P/sub 1/) with Cl/sub 2/ and COCl/sub 2/ also were studied. The new XeF(B) quenching rate constants are described. The pulsed laser induced fluorescence technique was used to measure radiative lifetimes and two-body quenching rate constant (with Ar) for the low energy Xe(6p)* states. Serious signal/noise problems for the lowest… more
Date: February 1978
Creator: Setser, D. W.
Partner: UNT Libraries Government Documents Department
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Electron-beam fusion welding of beryllium

Description: Ingot-sheet beryllium (Be) having three different chemistries and three different thicknesses was fusion-welded by the electron-beam process. Several different preheats were used to obtain 100% penetration and crack-free welds. Cracking susceptability was found to be related to aluminum (Al) content; the higher Al-content material was most susceptable. However, adequate preheat allowed full penetration and crack-free welds to be made in all materials tested. The effect of a post-weld heat treat… more
Date: January 1, 1978
Creator: Campbell, R. P.; Dixon, R. D. & Liby, A. L.
Partner: UNT Libraries Government Documents Department
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Homogenization of arc-melted uranium-6 weight percent niobium alloy ingots

Description: Microsegregation and macrosegregation in uranium-6 niobium arc-melted ingots were characterized by electron microprobe analysis. Homogenization studies determined that microsegregation can be eliminated by heat treating the alloy for six hours at 1100/sup 0/C. Extensive homogenization did not eliminate macrosegregation (banding) from the as-cast alloy, but a mathematical model describing banding and coring indicated that banding could possibly be eliminated by working prior to homogenization.
Date: January 31, 1978
Creator: Snyder, W. B., Jr.
Partner: UNT Libraries Government Documents Department
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An HVEM study of displacement cascade damage in Nb/sub 3/Sn at 13 K

Description: TEM images of the martensite structure in Nb/sub 3/Sn were recorded at various temperatures between 12 and 30/degree/K. The transition to the superconducting state was observed by a slight deflection of the electron beam due to a perturbation of the magnetic field of the objective lens at the sample. The primary interest is in irradiation effects due to fast neutrons from a fusion reactor, and therefore ion irradiation conditions that are somewhat comparable to this were selected. These consist… more
Date: February 1, 1988
Creator: Kirk, M. A.; Baker, M. C.; Kestel, B. J.; Weber, H. W. & Kampwirth, R. T.
Partner: UNT Libraries Government Documents Department
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Advanced Coal Conversion Process Demonstration (Project)

Description: This report contains a description of technical progress made on the Advanced Coal Conversion Process Demonstration Project (ACCP). The project is a US Department of Energy Innovative Clean Coal Technology Project. The cooperative agreement defining the project is between DOE and the Rosebud SynCoal Partnership RSCP. The RSCP is a partnership between Western Energy Company (WECo), a subsidiary of Entech, Montana Power's non-utility group, and NRG, a subsidiary of Northern States Power. The ACCP… more
Date: July 1, 1991
Partner: UNT Libraries Government Documents Department
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Development of low cost contacts to silicon solar cells. Final report, 15 October 1978-30 April 1980

Description: A summary of work done on the development of a copper based contact system for silicon solar cells is presented. The work has proceeded in three phases: (1) Development of a copper based contact system using plated Pd-Cr-Cu. Good cells were made but cells degraded under low temperature (300/sup 0/C) heat treatments. (2) The degradation in Phase I was identified as copper migration into the cells junction region. A paper study was conducted to find a proper barrier to the copper migration proble… more
Date: January 1, 1980
Creator: Tanner, D. P. & Iles, P. A.
Partner: UNT Libraries Government Documents Department
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Marketing research for EE G Mound Applied Technologies' heat treatment process of high strength materials

Description: This report summarizes research conducted by ITI to evaluate the commercialization potential of EG G Mound Applied Technologies' heat treatment process of high strength materials. The remainder of the report describes the nature of demand for maraging steel, extent of demand, competitors, environmental trends, technology life cycle, industry structure, and conclusion. (JL)
Date: October 9, 1991
Creator: Shackson, R.H.
Partner: UNT Libraries Government Documents Department
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