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The evolution of ANL CMT gloveboxes

Description: This report summarizes the following topics: the design approach based upon user-friendly concepts; utilization of existing component designs; cost effectiveness; schedule; and adaptable to project process changes without losing overall effectiveness of user-friendly approach.
Date: July 6, 2000
Creator: Malecha, R. F.; Frigo, A. A. & Preuss, D. E.
Partner: UNT Libraries Government Documents Department


Description: A collimated portable gamma-ray detector will be used to quantify the plutonium content of items that can be approximated as a point, line, or area geometry with respect to the detector. These items can include ducts, piping, glove boxes, isolated equipment inside of gloveboxes, and HEPA filters. The Generalized Geometry Holdup (GGH) model is used for the reduction of counting data. This document specifies the calculations to reduce counting data into contained plutonium and the associated total measurement uncertainty.
Date: February 1, 2005
Creator: BD, KEELE
Partner: UNT Libraries Government Documents Department

ProTec Tear-Offs: A Preliminary Assessment

Description: The Savannah River National Laboratory (SRNL) has conducted a series of ''scoping'' tests (referred to as Phase 1) to assess the potential use of a Mylar{reg_sign} tear-off system as a primary or secondary protective barrier to minimize acid etching (''frosting''), accidental scratching, and/or radiation damage for shielded cells windows. Conceptually, thin, multi-layered sheets of Mylar (referred to as a ''tear-off'' system) could be directly applied to the Lexan{reg_sign} sheet or glovebox/hood sash window to serve as a secondary (or primary) barrier. Upon degradation of visual clarity due to accidental scratching, spills/splatters, and/or radiation damage, the outer layer (or sheet) of Mylar could be removed ''refreshing'' or restoring the view. Due to the multi-layer aspect, the remaining Mylar layers would provide continued protection for the window from potential reoccurrences (which could be immediate or after some extended time period). Although the concept of using a tear-off system as a protective barrier was conceptually enticing, potential technical issues were identified and addressed as part of this Phase 1 feasibility study. These included resistance to: (1) acid(s) (concentrated (28.9 M) HF, concentrated (15.9M) HNO{sub 3}, 6M HCl, and 0.6M H{sub 3}BO{sub 3}), (2) base (a simulated sludge with pH of 12.9), (3) gamma radiation (cumulative dose of {approx}200,000 rad), and (4) scratch resistance (simulating accidental scratching with the manipulators). Not only can these four factors play a significant role in determining the visual clarity of the integrated system, they can also contribute to the mechanical integrity issues which could dictate the ability to remove the outer layer when visual clarity has degraded. The results of the Phase 1 study clearly indicate that the Mylar tear-off concept (as a primary or secondary protective barrier) is a potential technical solution to prevent or retard excessive damage that would result from acid etching, base damage (as ...
Date: September 1, 2005
Creator: Peeler, D
Partner: UNT Libraries Government Documents Department

Light transmission and air used for inspection of glovebox gloves.

Description: Various materials used for manufacturing the glovebox gloves are translucent material such as hypalon, rubbers, and neoprene. This means that visible light can be transmitted through the inside of the material. Performing this test can help to increase visualization of the integrity of the glove. Certain flaws such as pockmarks, foreign material, pinholes, and scratches could be detected with increased accuracy. An analysis was conducted of the glovebox gloves obscure polymer material using a inspection light table. The fixture is equipped with a central light supply and small air pump to inflate the glove and test for leak and stability. A glove is affixed to the fixture for 360-degree inspection. Certain inspection processes can be performed: (1) Inspection for pockmarks and thin areas within the gloves; (2) Observation of foreign material within the polymer matrix; and (3) Measurements could be taken for gloves thickness using light measurements. This process could help reduce eyestrain when examining gloves and making a judgment call on the size of material thickness in some critical areas. Critical areas are fingertips and crotch of fingers.
Date: January 1, 2002
Creator: Castro, J. M. (Julio M.); Steckle, W. P. (Warren P.), Jr. & Macdonald, J. M. (John M.)
Partner: UNT Libraries Government Documents Department


Description: As part of the characterization of various glovebox glove material from four vendors, the permeability of gas through each type as a function of temperature was determined and a discontinuity in the permeability with temperature was revealed. A series of tests to determine the viscoelastic properties of the glove materials as a function of temperature using Dynamic Mechanical Analysis (DMA) was initiated. The glass transition temperature and the elastic and viscoelastic properties as a function of temperature up to maximum use temperature were determined for each glove material. The glass transition temperatures of the gloves were -60 C for butyl, -30 C for polyurethane, -16 C Hypalon{reg_sign}, - 16 C for Viton{reg_sign}, and -24 C for polyurethane-Hypalon{reg_sign}. The glass transition was too complex for the butyl-Hypalon{reg_sign} and butyl-Viton{reg_sign} composite gloves to be characterized by a single glass transition temperature. All of the glass transition temperatures exceed the vendor projected use temperatures.
Date: February 29, 2012
Creator: Korinko, P.
Partner: UNT Libraries Government Documents Department

DAF Glovebox Project Plan

Description: This document defines how the glovebox project will be managed and executed. It provides a path forward for establishing a glovebox capability in Building 341 of the DAF in time to meet JASPER programmatic requirements as the first user. Note that some elements of the glovebox project have been under way for some time and are more mature than others; other elements are being worked concurrently. This plan serves the following purposes: Assign organizational and individual responsibilities for bringing the glovebox capability online; Coordinate activities between organizations; Facilitate communication between project members and management; and Identify the mechanisms used to manage and control the project. The scope of this plan includes all activities conducted to achieve project objectives, culminating in DOE/NV approval to operate. This plan does not address the issues associated with the steady-state operation of the glovebox.
Date: November 14, 2000
Creator: Martinez, M. W. & Higgs, R. L.
Partner: UNT Libraries Government Documents Department

Tritium stripping in a nitrogen glove box using palladium/zeolite and SAES St 198{trademark}

Description: Glove box clean-up experiments were conducted in a nitrogen glove box using palladium deposited on zeolite (Pd/z) and a SAES St 198{trademark} getter as tritium stripping materials. Protium/deuterium samples spiked with tritium were released into a 620 liter glove box to simulate tritium releases in a 10,500 liter glove box. The Pd/z and the SAES St 198{trademark} stripper beds produced a reduction in tritium activity of approximately two to three orders of magnitude and glove box clean-up was limited by a persistent background tritium activity level. Attempts to significantly reduce the glove box activity to lower levels without purging were unsuccessful.
Date: January 1, 1995
Creator: Klien, J.E. & Wermer, J.R.
Partner: UNT Libraries Government Documents Department

Modeling of RTF Glove-Box and Stripper System

Description: The glove box-stripper system for the Replacement Tritium Facility (RTF) has been modeled to determine its steady-state performance. To permit comparison, simulations of modified cases were compared with a standard or base case. This paper discusses tests conducted, results obtained and makes recommendations.
Date: March 28, 2001
Creator: Hsu, R. H.
Partner: UNT Libraries Government Documents Department

CSER 96-013: Cementation Process, glovebox HA-20MB at PFP

Description: This evaluation provides criticality safety controls for the cementation processing in Glovebox HA-2OMB at the Plutonium Finishing Plant. Slag and crucible residues from Pu button making will be blended with Portland cement in 5k-in. diam. x 7-in. tall cans, for eventual disposition in special DOT 17C drums. A maximum of 180 g Pu is allowed per liquid-bearing container (mixing bowl, filter funnel, or cement can). In this SD revision, three separate areas with 500 g Pu limits each are established; the airlock cell for input S&C cans, the reaction- and mixing-process area, and a cemented-can storage area. Number and spacing of containers within an area is not restricted, for areas spaced 6 inches apart. Acid addition in the reaction stage is allowed to the extent that plutonium dissolution will not occur.
Date: September 1, 1996
Creator: Hess, A.L.
Partner: UNT Libraries Government Documents Department

Design considerations for heated wells in gloveboxes.

Description: Heated wells in gloveboxes have been used for many years by the Argonne National Laboratory Chemical Technology Division for nuclear-technology, waste-management, chemical-technology, and analytical-chemistry research. These wells allow experiments to be isolated from the main working volume of the glovebox. In addition, wells, when sealed, allow experiments to be conducted under pressurized or vacuum conditions. Until recently, typical maximum operational temperatures were about 500 C. However, more recent research is requiring operational temperatures approaching 900 C. These new requirements pose interesting design challenges that must be resolved. Some problem areas include temperature effects on material properties, maintaining a seal, cooling selected areas, and minimizing stresses. This paper discusses issues related to these design challenges and the ways in which these issues have been resolved.
Date: July 14, 1999
Creator: Frigo, A. A. & Preuss, D. E.
Partner: UNT Libraries Government Documents Department


Description: 'Study the past--what is past is prologue'. These words appear as the motto on a pair of statues at the National Archives Building in Washington DC. They are also the opening sentence in the preface of a document written in August of 1956 entitled 'A Summary of Accidents and Incidents Involving Radiation in Atomic Energy Activities--June 1945 thru December 1955'. This document, one of several written by D.F. Hayes of the Safety and Fire Protection Branch, Division of Organization and Personnel, U.S. Atomic Energy Commission in Washington DC, and many others are often forgotten even though they contain valuable glovebox fire protection lessons for us today.
Date: April 15, 2009
Creator: Till, W
Partner: UNT Libraries Government Documents Department


Description: A research and development task was undertaken to determine the permeabilities of hydrogen and dry air through different polymeric glove materials that are used to maintain the integrity of glovebox secondary containment. Fifteen different glove samples were obtained from four different manufacturers and samples cut from these gloves were tested. The gloves included baseline butyl rubber, Viton{reg_sign}, Dupont{reg_sign} Hypalon{reg_sign}, polyurethane, as well as composite gloves. The testing indicated that all of the vendor's butyl rubber gloves and the Jung Viton{reg_sign} gloves performed comparably in both gases.
Date: February 29, 2012
Creator: Korinko, P.
Partner: UNT Libraries Government Documents Department

Preparation of a glovebox for casting enriched plutonium.

Description: Objectives: Prepare existing glovebox for casting, heat treating and storing enriched plutonium, Upgrade seismic systems to reduce dispersion hazard, Upgrade atmospheric systems to reduce oxidation of plutonium, Upgrade vacuum system to prevent oxidation, InstalI/upgrade induction heating systems to melt plutonium and heat mold
Date: January 1, 2002
Creator: Ronquillo, R. D. (Richard D.); Trujillo, C. M. (Chris M.) & Trujillo, C. C. (Claudette C.)
Partner: UNT Libraries Government Documents Department


Description: An experiment was conducted to determine the puncture resistance of 15 gloves that are used or proposed for use in the Tritium Facility at Savannah River Site (SRS). These data will serve as a baseline for characterization and may be incorporated into the glove procurement specification. The testing was conducted in agreement with ASTM D120 and all of the gloves met or exceeded the minimum requirements. Butyl gloves exhibited puncture resistance nearly 2.5 times the minimum requirements at SRS while Polyurethane was nearly 7.5x the minimum.
Date: February 29, 2012
Creator: Korinko, P. & Chapman, G.
Partner: UNT Libraries Government Documents Department


Description: A task was undertaken to determine primarily the permeation behavior of various glove compounds from four manufacturers. As part of the basic characterization task, the opportunity to obtain additional mechanical and thermal properties presented itself. Consequently, a total of fifteen gloves were characterized for permeation, Thermogravimetric Analysis, Puncture Resistance, Tensile Properties and Dynamic Mechanical Analysis. Detailed reports were written for each characterization technique used. This report contains the summary of the results.
Date: May 14, 2012
Creator: Korinko, P.
Partner: UNT Libraries Government Documents Department

19 mm ballistic range: a potpourri of techniques and recipes

Description: The expansion of ballistic gun range facilities at LLL has introduced state-of-the-art diagnostic techniques to glovebox-enclosed ballistic guns systems. These enclosed ballistic ranges are designed for the study of one- dimensional shock phenomena in extremely toxic material such as plutonium. The extension of state-of-the-art phtographic and interferometric diagnostic systems to glovebox-enclosed gun systems introduces new design boundaries and performance criteria on optical and mechanical components. A technique for experimentally evaluating design proposals is illustrated, and several specific examples (such as, target alignment, collateral shrapnel damage, and soft recovery) are discussed. (auth)
Date: September 23, 1975
Creator: Carpluk, G.T.
Partner: UNT Libraries Government Documents Department

Macro and Micro Remote Viewing of Objects in Sealed Gloveboxes

Description: The Savannah River Site uses sophisticated glovebox facilities to process and analyze material that is radiologically contaminated or that must be protected from contamination by atmospheric gases. The analysis can be visual, non destructive measurement, or destructive measurement, and allows for the gathering of information that would otherwise not be obtainable. Macro and Micro systems that cover a range of 2X to 400X magnifications with a robust system compatible with the harsh glovebox environment were installed. Remote video inspection systems were developed and deployed in Savannah River Site glovebox facilities that provide high quality or mega-pixel quality remote views, for remote inspections. The specialized video systems that are the subject of this report exhibited specialized field application of remote video/viewing techniques by expanding remote viewing to high and very high quality viewing in gloveboxes. This technological enhancement will allow the gathering of precision information that is otherwise not available.
Date: February 11, 2004
Creator: Heckendorn, F.M.
Partner: UNT Libraries Government Documents Department