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Biology Seminar : methods of assaying for plutonium in biological materials

Description: From introduction: "Since plutonium is manufactured at the Hanford Works, a study of its effect on biological materials is important. To determine the amount of plutonium deposited in a biological sample, it is necessary to have an accurate method for extracting plutonium from these samples. Some of the different methods for plutonium assay are reviewed and given in this paper."
Date: November 1948
Creator: Case, A. C.
Partner: UNT Libraries Government Documents Department

Correlation of chemical analyses on graphite bars and test pile results

Description: From abstract: "The chemical analyses of graphite test bars obtained from National Carbon Company and the analyses performed by the Hanford Works Laboratories Division do not correlate significantly with the test pile results, nor do the chemical analyses obtained from National Carbon Company agree with those done in the Handford Works Laboratories. Chemical results obtained at Hanford on samples taken lengthwise from individual bars correlated significantly with the individual test pile results."
Date: unknown
Creator: Lane, J.J.
Partner: UNT Libraries Government Documents Department

Investigation of Waikele Well No. 2401-01, Oahu, Hawaii: Pumping Test, Well Logs and Water Quality

Description: Introduction: A dependable water supply is required for Naval Magazine Lualualei, Waikele Branch. The water supply for Naval Magazine Lualualei, Waikele Branch, Oahu, Hawaii has been dependent on Oahu Sugar Co.'s water for many years. Because the supply of water from Oahu Sugar Co. is not always dependable, in March 1982, the Pacific Division of the Naval Facilities Engineering Command entered into a cooperative agreement with the U.S. Geological Survey to determine the productivity and water quality of an abandonment Navy well. The well, No. 2401-01, is located in Waikele Gulch near the confluence of Waikele and Kipapa Streams (fig. 1.0-1)
Date: November 1983
Creator: Eyre, Paul
Partner: UNT Libraries Government Documents Department

Geohydrology of the Anza-Terwilliger Area, Riverside County, California

Description: The Anza-Terwilliger area consists of about 96 square miles (24-9 square kilometers) in the upper parts of the Santa Margarita River and Coyote Creek drainage basins in Riverside County, Calif., about 90 miles (145 kilometers) southeast of Los Angeles. This report deals with geology, steady state and transient state of ground water, net depletion of ground water, surface-water flow, precipitation, chemistry of water, land and water use, and gravity data for the Anza-Terwilliger area. The data indicate that the rate of ground-water depletion ha's accelerated since 1950. Pumping depressions adjacent to the Cahuilla Indian Reservation have increased the hydraulic gradient and are.causing water beneath the reservation to flow toward these depressions. Total depletion of ground water since 1950 is about 14,000 acre-feet (17.3 cubic hectometers). Chemical analyses indicate that the ground water in local areas contains concentrations of nitrate above that recommended by the Environmental Protection Agency for human consumption.
Date: March 1976
Creator: Moyle, W. R., Jr.
Partner: UNT Libraries Government Documents Department

Chemical and Physical Character of Ground Water in the National Reactor Testing Station, Idaho

Description: Report documenting "the chemical and physical properties of the ground water beneath the National Reactor Testing Stations (NRTS), Idaho. The chemical properties described are chiefly the concentration and proportions of the dissolved constituents" (p. 1).
Date: May 1962
Creator: Olmsted, F. H.
Partner: UNT Libraries Government Documents Department

Aircraft Reactor Test Removal and Disassembly

Description: Report documenting the dissection of a reactor called the Aircraft Reactor Test (ART). Includes the removal of the reactor from its test cell, component removal, and plans for a for a disassembly building facility.
Date: 1960?
Creator: Abbatiello, A. A. & McQuilkin, F. R.
Partner: UNT Libraries Government Documents Department

B Plant, TK-21-1, analytical results for the final report

Description: This document is the final laboratory report for B Plant Tk-21-1. A Resource Conservation and Recovery Act (RCRA) sample was taken from Tk-21 -1 September 26, 1996. This sample was received at 222-S Analytical Laboratory on September 27, 1996. Analyses were performed in accordance with the accompanying Request for Sample Analysis (RSA) and Letter of Instruction B PLANT RCRA SAMPLES TO 222S LABORATORY, LETTER OF INSTRUCTION (LOI) 2B-96-LOI-012-01 (LOI) (Westra, 1996). LOI was issued subsequent to RSA and replaces Letter of Instruction 2C-96-LOI-004-01 referenced in RSA.
Date: December 9, 1996
Creator: Fritts, L.L., Westinghouse Hanford
Partner: UNT Libraries Government Documents Department

Miniature chemical measurement systems

Description: Prospect of microfabricated monolithic devices that accomplish complete chemical assays is enticing. Early work with microfabricated chemical analysis devices focused on separations methods. More recently reagent manipulation has been integrated with separation devices to create more powerful capabilities. Examples of procedures, other than separations, that have been demonstrated on micromachined structures include reagent mixing, dilution, and reaction, preconcentration through sample stacking and biopolymer tagging for detection. Developments in liquid phase microfabricated chemical analysis devices are reviewed.
Date: December 31, 1996
Creator: Ramsey, J.M.
Partner: UNT Libraries Government Documents Department

Geochemistry of Background Sediment Samples at Technical Area 39, Los Alamos National Laboratory

Description: This report presents results of chemical analyses of 24 analytes in 16 background sediment samples collected from Ancho Canyon and Indio Canyon at Technical Area (TA) 39, Los Alamos National Laboratory. Preliminary upper tolerance limits (UTLS) for sediments are calculated from this data set but, because of the small sample size, these UTLs exceed the maximum values in the data set by up to 50'ZO and will require revision as more background sediment data are obtained.
Date: November 1, 1998
Creator: McDonald, Eric V.; Campbell, Katherine; Longmire, Patrick A. & Reneau, Steven L.
Partner: UNT Libraries Government Documents Department

Determination of Iron Contamination of Used Lubricating Oil for Use in Measuring Rates of Wear in Aircraft Engines

Description: Report discusses methods of determining the iron contamination of used lubricating oil in order to study wear rates of piston rings and cylinder barrels of aircraft engines. Two methods of separating iron from used lubricating oil are presented. The results of the analyses of the oil are presented and the methods are evaluated.
Date: March 1944
Creator: Tischler, Adelbert O.
Partner: UNT Libraries Government Documents Department

Continued studies of calorimeter performance at the Lawrence Livermore Laboratory

Description: Calibrations of two calorimeters used for tritium and plutonium assays were made. Data from three new standards of about 0.5, 1, and 5 W were added to the results of a previous report and analyzed together. The accuracies of both calorimeters appear to fall within the specified 0.5 percent, although the data now available for the large calorimeter is insufficient to permit a more definite conclusion. An expression of the bias correction for each calorimeter with respect to the sample power cannot be determined. The bias of the medium thermopile-type calorimeter tends to be positive, however, and that of the large resistance-bridge design appears to be negative. (auth)
Date: November 17, 1975
Creator: Steward, S.A. & Tsugawa, R.T.
Partner: UNT Libraries Government Documents Department

Genome Project Standards in a New Era of Sequencing

Description: For over a decade, genome 43 sequences have adhered to only two standards that are relied on for purposes of sequence analysis by interested third parties (1, 2). However, ongoing developments in revolutionary sequencing technologies have resulted in a redefinition of traditional whole genome sequencing that requires a careful reevaluation of such standards. With commercially available 454 pyrosequencing (followed by Illumina, SOLiD, and now Helicos), there has been an explosion of genomes sequenced under the moniker 'draft', however these can be very poor quality genomes (due to inherent errors in the sequencing technologies, and the inability of assembly programs to fully address these errors). Further, one can only infer that such draft genomes may be of poor quality by navigating through the databases to find the number and type of reads deposited in sequence trace repositories (and not all genomes have this available), or to identify the number of contigs or genome fragments deposited to the database. The difficulty in assessing the quality of such deposited genomes has created some havoc for genome analysis pipelines and contributed to many wasted hours of (mis)interpretation. These same novel sequencing technologies have also brought an exponential leap in raw sequencing capability, and at greatly reduced prices that have further skewed the time- and cost-ratios of draft data generation versus the painstaking process of improving and finishing a genome. The resulting effect is an ever-widening gap between drafted and finished genomes that only promises to continue (Figure 1), hence there is an urgent need to distinguish good and poor datasets. The sequencing institutes in the authorship, along with the NIH's Human Microbiome Project Jumpstart Consortium (3), strongly believe that a new set of standards is required for genome sequences. The following represents a set of six community-defined categories of genome sequence standards that better ...
Date: June 1, 2009
Creator: Consortia, GSC; Consortia, HMP Jumpstart; Chain, P. S. G.; Grafham, D. V.; Fulton, R. S.; FitzGerald, M. G. et al.
Partner: UNT Libraries Government Documents Department

Prevention of iron-sulfide deposition in petroleum processing. Final CRADA report.

Description: The purpose of this CRADA extension which effectively ended in 2003 was to quantify the effect of iron-sulfide formation on the fouling propensity of crude oil. The specific objectives are focused on fouling of the Crude Distillation Unit (CDU-1) at the Shell Refinery in Mobile, Alabama. The technical approach consists of analyzing the plant data, chemical analysis of crude oil to detect key precursors, performing refinery tests using the Argonne Field Fouling Unit, and verifying the effectiveness of a physical device of tube insert and enhanced tubes to change threshold conditions and thereby reducing fouling.
Date: March 25, 2010
Creator: Doctor, R. D.; Panchal, C. B. & Systems, Energy
Partner: UNT Libraries Government Documents Department

Conformational Diversity in (Octaethylporphinato) (trichloroacetato)iron(III) Derivatives

Description: Treatment of [Fe(OEP)]20 with trichloroacetic acid results in ruffled formation of (octaethylporphinato trichloroacetato)iron(HI). Various crystalline solvates can be isolated, depending on the crystallization solvent. Initial crystallization with CHC13/hexanes resulted in the isolation of an unsolvated form. [Fe(OEP)(02C2C13 )]. This form contains distinct porphyrin core conformations at the same site: one is domed and the other is ruffled. Crystal data for [Fe(OEP)(02C2C13 )]: Q = 14.734(4) .4. b = 13.674(1) .\. c = 17..541 [,.5] .~. 3 = 90.67(1)0, V = 35-!5.8(14) .\3. monoclinic. space group R1/ n. Z = 4. Subsequent crystallization with CHC13/hexanes resulted in a new crystalline form, [Fe(OEP)(OzC2C13 )~.- CHC13; the porphyrin core is slightly ruffled. Crystal data for [Fe(OEP)(OoC2C13 )]. CHC13: a =12.323(1) .~, 6 = 13.062(3) .\. C = 14.327(2) .$, Q = 89.32(1)", .3 = 113.36(2)0. :~ = 105.26(1)'. V = `2031.3(6) .\3. triclinic. space group Pi. Z = 2. Crystallization with CH2C12/hexanes resulted in the isolation of yet another form, [Fe(OEP) (02 C2C13)]. H02C2C13. which contains two independent molecules in the unit cell: molecule is slightly saddled and molecule B is modestly ruffled. Crystal data for [Fe(OEP)(02ClC13 )]. H02C2C13: a = 13.148(3) .\, b = 13.45.5(3) A, c = Q3.761(5) -& ~ = 90.72(3)", ~ = 91. ~4(3)". -y = 92.36(3)0, V = 4198.5(15) .\3, triclinic.space group PI, Z = 4. .+11 conformations form dimers in the solid state. Temperature-dependent manometic susceptibility measurements showed that [Fe(OEP)(02C2C13)] .CHC13 contains a high-spin iron(III) center; the data for {Fe(OEP)(02C2C13 )l.H02C2C13 are understood in terms of an admixed intermediate-spin state (S = 3/2, 5/2) and are readily fit to a faltempo model with a ground state multiplet containing about 78% S = 5/2 character and 22% S = 3/2 character. The structural data for [Fe(OEP)(02C2C13 )]. CHC13 are consistent with the observed high-spin state, while data for ...
Date: October 19, 1998
Creator: Cheng, B.; Ma, J.; Neal, T.J.; Scheidt, W.R.; Schulz, C.E. & Shelnutt, J.A.
Partner: UNT Libraries Government Documents Department