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Applications of X-ray absorption spectroscopy and low temperature XMCD to metalloproteins

Description: The author has used the extended X-ray absorption fine structure (EXAFS) and ultra-low temperature X-ray magnetic circular dichroism (XMCD) to study the environments of the metal sites in metalloproteins. EXAFS has been used to study the Zn site in spinach carbonic anhydrase. The EXAFS, in parallel with site directed mutagenesis studies, indicate that the active site Zn is in a cys-cys-his-H{sub 2}O environment, very different from the mammalian carbonic anhydrase active site. Nitrogenase, the primary enzyme in biological nitrogen fixation, contains two complex metal clusters of unique structure. EXAFS studies at the Fe and Mo K-edges of nitrogenase solutions and crystals yielded information about the various metal-metal distances in these two clusters. The author assigned 4 Fe and 3 Mo interactions >4 {angstrom}. Single crystal Mo K-edge EXAFS then found a very long Fe-Fe distance of {approximately}5.1 {angstrom}. These distances were then used to further refine the proposed crystallographic models to their highest accuracy yet. Studies were carried further by examining nitrogenas in oxidized and reduced forms--states for which there is no crystallographic information. Small structural changes were observed and an EXAFS model was put forth that attempts to deconvolute the EXAFS distances of the two metal clusters. Nitrogenase Apo I, a genetic mutant of nitrogenase which is though to contain only one of the two different metal clusters, was also examined using EXAFS. These studies showed results consistent with current models, yet the metal clusters were very disordered. Finally, ultra-low temperature methods were used to further the development of XMCD as a technique for studying biological systems. Experiments were performed on the copper in plastocyanin. Data was collected that definitively proves that the sample surface was at 0.55 {+-} 0.05 K. This result opens the door to further study of more complex biological metal clusters.
Date: January 1996
Creator: Christiansen, J. H.
Partner: UNT Libraries Government Documents Department

You Won`t Find These Leaks with a Blower Door: The Latest in "Leaking Electricity" in Homes

Description: Leaking electricity is the energy consumed by appliances when they are switched off or not performing their principal functions. Field measurements in Florida, California, and Japan show that leaking electricity represents 50 to 100 Watts in typical homes, corresponding to about 5 GW of total electricity demand in the United States. There are three strategies to reduce leaking electricity: eliminate leakage entirely, eliminate constant leakage and replace with intermittent charge plus storage, and improve efficiency of conversion. These options are constrained by the low value of energy savings-less than $5 per saved Watt. Some technical and lifestyle solutions are proposed. 13 refs., 1 fig., 2 tabs.
Date: August 1996
Creator: Rainer, L.; Greenberg, S. & Meier, A.
Partner: UNT Libraries Government Documents Department

Guidelines for sustainable building design: Recommendations from the Presidio of San Francisco energy efficiency design charrette

Description: In 1994, the Bay Chapter of the Association of Energy Engineers{reg_sign} organized a two-day design charrette for energy-efficient redevelopment of buildings by the National Park Services (NPS) at the Presidio of San Francisco. This event brought together engineers, researchers, architects, government officials, and students in a participatory environment to apply their experience to create guidelines for the sustainable redesign of Presidio buildings. The venue for the charrette was a representative barracks building located at the Main Post of the Presidio. Examination of this building allowed for the development of design recommendations, both for the building and for the remainder of the facilities. The charrette was organized into a committee structure consisting of: steering, measurement and monitoring, modeling, building envelope and historic preservation (architectural), HVAC and controls, lighting, and presentation. Prior to the charrette itself, the modeling and measurement/monitoring committees developed substantial baseline data for the other committees during the charrette. An integrated design approach was initiated through interaction between the committees during the charrette. Later, committee reports were cross-referenced to emphasize whole building design and systems integration.
Date: May 1996
Creator: Brown, K.; Sartor, D. & Greenberg, S.
Partner: UNT Libraries Government Documents Department

Energy effectiveness of duct sealing and insulation in two multifamily buildings

Description: Energy losses from forced air distribution systems have a significant impact on the energy efficiency of buildings. Little work has been done to quantify these losses in apartment buildings. In this paper the authors will discuss field measurements made on four forced air heating systems to evaluate the duct system energy losses to unconditioned basements. The apartments were heated by natural gas furnaces located in the basements. The systems had bare sheet metal ductwork exposed to the basement conditions. The pre-retrofit measurements were made on the systems after sealing large easily visible leaks. The post-retrofit measurements were made after wrapping the ducts in foil backed glass fiber insulation and additional leak sealing. Only the sections of duct exposed to the basement were retrofitted because only these sections were accessible. This study examines the potential energy savings for this type of limited retrofit. The energy losses were separated into leakage and conduction terms. Leakage measurements were made using register flowhood techniques. Conduction losses were estimated by measuring temperatures in the plenums and at the registers. Analysis of the measurements has shown typical reduction in leakage flow due to duct sealing of about 40%. The reduction in leakage translated into a reduction in energy consumption of about 10%.
Date: August 1996
Creator: Walker, I. S.; Modera, M. P.; Tuluca, A. & Graham, I.
Partner: UNT Libraries Government Documents Department

Decision making through use of interoperable simulation software

Description: Many building simulation computer programs, originally developed on mainframe computers for research purposes, can now run on the powerful workstation and personal computers that are available to most architectural and engineering firms. Major efforts have been underway during the last decade to compile these programs on personal computers and make them available to a wider range of building professionals. However, even with the addition of user-friendly front- and back-ends, their use is still limited to a small number of specialized consultants. Considering the tremendous benefits of informed decisions that these programs can support, it is critical to address and resolve the issues that are associated with their limited acceptance. In this paper, the authors report on their research and development efforts to better understand decision-making and develop computer tools that will facilitate the use of simulation software during the building design process. They present a brief analysis of decision-making and then describe how they try to address it in building design through the development of the Building Design Advisor (BDA). Moreover, the authors elaborate on the major issues that they have encountered, discuss lessons learned, and offer recommendations for short- and long-term developments in this area.
Date: March 1997
Creator: Papamichael, K.; La Porta, J. & Chauvet, H.
Partner: UNT Libraries Government Documents Department

Bipolar pulsed reset for AC coupled charge-sensitive preamplifiers

Description: A new type of charge restoration is described for use particularly in germanium gamma-ray spectrometers for accelerator and space physics applications. A bipolar pulsed reset technique is applied to these applications for the first time. This technique overcomes the problems introduced by the need to AC couple detectors and the fact that very large energy depositions occur due to charged particles present in substantial fluxes, particularly in space. The circuit is described and experimental results are presented and discussed.
Date: July 1, 1997
Creator: Landis, D. A.; Madden, N. M. & Goulding, F. S.
Partner: UNT Libraries Government Documents Department

Electrochromic lithium nickel oxide thin film by pulsed laser deposition

Description: * Thin films of lithium nickel oxide were deposited by pulsed laser deposition (PLD) from targets of pressed LiNiO{sub 2} powder with layered structure. The composition, structure and surface air sensitivity of these films were analyzed using a variety of techniques, such as nuclear reaction analysis, Rutherford backscattering spectrometry (RBS), x-ray diffraction, infrared spectroscopy, and atomic force microscopy. Optical properties were measured using a combination of variable angle spectroscopic ellipsometry and IP spectroradiometry. Crystalline structure, surface morphology and chemical composition of Li{sub x}Ni{sub 1-x}O thin films depend strongly on deposition oxygen pressure, temperature as well as substrate target distance. The films produced at temperatures lower than 600 degrees C spontaneously absorb CO{sub 2} and H{sub 2}O at their surface once they are exposed to the air. The films deposited at 600 degrees C proved to be stable in air over a long period. Even when deposited at room temperature the PLD films are denser and more stable than sputtered films. RBS determined that the best electrochromic films had the stoichiometric composition L{sub 0.5}Ni{sub 0.5}O when deposited at 60 mTorr O{sub 2} pressure. Electrochemical tests show that the films exhibit excellent reversibility in the range 1.0 V to 3.4 V versus lithium and long cyclic life stability in a liquid electrolyte half cell. Electrochemical formatting which is used to develop electrochromism in other films and nickel oxide films is not needed for these stoichiometric films. The optical transmission range is almost 70% at 550 nm for 120 nm thick films.
Date: October 1996
Creator: Wen, S. J.; von Rottkay, K. & Rubin, M.
Partner: UNT Libraries Government Documents Department

Solar heat gain coefficient of complex fenestrations with a venetian blind for differing slat tilt angles

Description: Measured bidirectional transmittances and reflectances of a buff-colored venetian blind together with a layer calculation scheme developed in previous publications are utilized to produce directional-hemispherical properties for the venetian blind layer and solar heat gain coefficients for the blind in combination with clear double glazing. Results are presented for three blind slat tilt angles and for the blind mounted either interior to the double glazing or between the glass panes. Implications of the results for solar heat gain calculations are discussed in the context of sun positions for St. Louis, MO.
Date: August 1996
Creator: Klems, J. H. & Warner, J. L.
Partner: UNT Libraries Government Documents Department

A comparison between calculated and measured SHGC for complex fenestration systems

Description: Calorimetric measurements of dynamic net heat flow through a complex fenestration system consisting of a buff venetian blind inside clear double glazing are used to derive the direction-dependent beam SHGC (solar heat gain coefficient) of the fenestration. The data are compared with calculations according to a proposed general method for deriving complex fenestration system SHGC`s from bidirectional layer optical properties and generic calorimetric properties. Previously published optical data for the same venetian blind and generic inward-flowing fraction measurements are used in the calculation. Satisfactory agreement is found between SHGC measurements and calculation. Significant dependence on incident angle was found in the measured SHGC`s. Profile angle was not found to be a useful variable in characterizing the system performance. Predicted SHGC was found to be inherently dependent on two angles, although only the incident angle variations were observable under test conditions.
Date: September 1995
Creator: Klems, J. H.; Warner, J. L. & Kelley, G. O.
Partner: UNT Libraries Government Documents Department

A field test of permeation grouting in heterogeneous soils using a new generation of barrier liquids

Description: A field demonstration of permeation grouting was conducted at a gravel quarry near Los Banos, California, with the purpose of demonstrating the feasibility of the concept. Two grouts were used: a form of colloidal silica that gels after the addition of a gelling agent, and a polysiloxane that polymerizes after the addition of a catalyst. Both create relatively impermeable barriers in response to the large increase in viscosity during gelation or polymerization, respectively. The grouts were successfully injected at a depth between 10 and 14ft. Subsequent exhumation of the injected gravels revealed that both grouts produced relatively uniform bulbs. Laboratory measurements of the grouted material retrieved from the field showed at least a four order of magnitude reduction in permeability over the ungrouted material.
Date: August 1995
Creator: Moridis, G. J.; Persoff, P.; Apps, J. A.; Myer, L.; Pruess, K. & Yen, P.
Partner: UNT Libraries Government Documents Department

The {alpha}-induced thick-target {gamma}-ray yield from light elements

Description: The {alpha}-induced thick-target {gamma}-ray yield from light elements has been measured in the energy range 5.6 MeV {le} E{sub {alpha}} {le} 10 MeV. The {gamma}-ray yield for > 2.1 MeV from thick targets of beryllium, boron nitride, sodium fluoride, magnesium, aluminum and silicon were measured using the {alpha}-particle beam from the Lawrence Berkeley Laboratories 88 in. cyclotron. The elemental yields from this experiment were used to construct the {alpha}-induced direct production {gamma}-ray spectrum from materials in the SNO detector, a large volume ultra-low background neutrino detector located in the Creighton mine near Sudbury, Canada. This background source was an order of magnitude lower than predicted by previous calculations. These measurements are in good agreement with theoretical calculations of this spectrum based on a statistical nuclear model of the reaction, with the gross high energy spectrum structure being reproduced to within a factor of two. Detailed comparison of experimental and theoretical excitation population distribution of several residual nuclei indicate the same level of agreement within experimental uncertainties.
Date: October 1994
Creator: Heaton, R. K.
Partner: UNT Libraries Government Documents Department

Advanced instrumentation for Positron Emission Tomography

Description: This paper summarizes the physical processes and medical science goals that underly modern instrumentation design for Positron Emission Tomography. The paper discusses design factors such as detector material, crystalphototube coupling, shielding geometry, sampling motion, electronics design, time-of-flight, and the interrelationships with quantitative accuracy, spatial resolution, temporal resolution, maximum data rates, and cost. 71 refs., 3 figs., 3 tabs.
Date: April 1, 1985
Creator: Derenzo, S.E. & Budinger, T.F.
Partner: UNT Libraries Government Documents Department

Comparison of q anti qg and q anti q. gamma. events in e/sup +/e/sup -/ annihilation at PEP

Description: In comparing the particle flow in the event plane of three-jet (q anti qg) events and of radiative annihilation events (q anti q..gamma..) for similar kinematic configurations, two PEP experiments find a significant decrease in particle density in the angular region opposite to the gluon jet in q anti qg events, relative to the particle density in the region opposite to the photon in q anti q..gamma.. events. The effect is predicted both by QCD and by phenomenological string models. 5 refs., 5 figs.
Date: July 1, 1986
Creator: Hofmann, W.
Partner: UNT Libraries Government Documents Department

High-resolution PET (positron emission tomography) for medical science studies

Description: One of the unexpected fruits of basic physics research and the computer revolution is the noninvasive imaging power available to today's physician. Technologies that were strictly the province of research scientists only a decade or two ago now serve as the foundations for such standard diagnostic tools as x-ray computer tomography (CT), magnetic resonance imaging (MRI), magnetic resonance spectroscopy (MRS), ultrasound, single photon emission computed tomography (SPECT), and positron emission tomography (PET). Furthermore, prompted by the needs of both the practicing physician and the clinical researcher, efforts to improve these technologies continue. This booklet endeavors to describe the advantages of achieving high resolution in PET imaging. 6 refs., 21 figs.
Date: September 1, 1989
Creator: Budinger, T.F.; Derenzo, S.E.; Huesman, R.H.; Jagust, W.J. & Valk, P.E. (Lawrence Berkeley Lab., CA (USA))
Partner: UNT Libraries Government Documents Department

Physics of very high energy hadron-hadron colliders

Description: A review is given of the physics accessible at a very high energy hadron-hadron collider. Emphasis is placed on the reliability of the predicted rates, and upon the energy and luminosity required to explore new physics options. 38 refs., 19 figs.
Date: September 1, 1986
Creator: Hinchliffe, I.
Partner: UNT Libraries Government Documents Department

A superconducting linear motor drive for a positive displacement bellows pump for use in the g-2 cryogenics system

Description: Forced two-phase cooling of indirectly cooled magnets requires circulation of liquid helium through the magnet cooling channel. A bellows helium pump is one possible way of providing helium flow to a magnet cooling system. Since the bellows type of helium pump is immersed in liquid helium, a superconducting linear motor drive appears to be an attractive option. This report describes a linear motor drive that employs oriented permanent magnet materials such as samarium-cobalt as the stator magnet system and a superconducting loud speaker voice coil type of drive as the armature of the linear motor. This report examines drive motor requirements for a helium pump.
Date: October 1994
Creator: Green, M. A.
Partner: UNT Libraries Government Documents Department

Cryogenic tests of the g-2 superconducting solenoid magnet system

Description: The g-2 muon storage ring magnet system consists of four large superconducting solenoids that are up to 15.1 m in diameter. The g-2 superconducting solenoids and a superconducting inflector dipole will be cooled using forced two-phase helium in tubes. The forced two-phase helium cooling will be provided from the J-T circuit of a refrigerator that is capable of delivering 625 W at 4.5 K. The two-phase helium flows from the refrigerator J-T circuit through a heat exchanger in a storage dewar that acts as a phase separator for helium returning from the magnets. The use of a heat exchanger in the storage dewar reduces the pressure drop in the magnet flow circuit, eliminates most two phase flow oscillations, and it permits the magnets to operate at variable thermal loads using the liquid in the storage dewar as a buffer. The g-2 magnet cooling system will consist of three parallel two-phase helium flow circuits that provide cooling to the following components: (1) the four large superconducting solenoids, (2) the current interconnects between the solenoids and the solenoid gas cooled electrical leads, and (3) the inflector dipole and its gas cooled electrical leads. This report describes a cryogenic test of the two 15.1 meter diameter superconducting solenoids using two-phase helium from a dewar. The report describes the cool down procedure for the 3.5 ton outer solenoid magnet system using liquid nitrogen and two-phase helium. Low current operation of the outer solenoids is discussed.
Date: August 1995
Creator: Jia, L. X.; Cullen, J. R. ,Jr. & Esper, A. J.
Partner: UNT Libraries Government Documents Department

Specialty magnets

Description: A number of basic conceptual designs are explained for magnet systems that use permanent magnet materials. Included are iron free multipoles and hybrid magnets. Also appended is a discussion of the manufacturing process and magnetic properties of some permanent magnet materials. (LEW)
Date: July 1, 1986
Creator: Halbach, K.
Partner: UNT Libraries Government Documents Department

Harmonic superspace formalism and the consistent chiral anomaly

Description: The harmonic superspace formalism has been used to construct the consistent chiral anomaly in N = 1, d = 6 supersymmetric Yang-Mills thoery. The expressions of the gauge anomaly ..delta../sub s//sup phi/ and of the supersymmetric anomaly ..delta../sub SUSY//sup phi/ are given together with the consistent condition. 7 refs.
Date: August 1, 1986
Creator: Li, W.
Partner: UNT Libraries Government Documents Department

Experimental efforts and results in finding new heavy scintillators

Description: New heavy scintillators are being discovered with increasing frequency. In recent years NaI(Tl) (with its high light output and energy resolution) has been joined by BGO (with its high stopping power), BaF{sub 2} (with its excellent timing resolution), and CeF{sub 3} (with its speed and short Moliere radius). More than 10 potentially useful scintillators have been under development in the past five years, such as PbSO{sub 4} and Lu{sub 2}SiO{sub 5}(Ce). We tabulate the characteristics of these and other scintillators, including wavelength, luminous efficiency, decay time, and initial intensity. We describe a search strategy and the prospects for finding the ``ideal`` heavy scintillator, which would combine the light output of NaI(Tl) and CsI(Tl), the stopping power of BGO, and the speed of BaF{sub 2} and ZnO(Ga).
Date: September 1, 1992
Creator: Derenzo, S. E. & Moses, W. W.
Partner: UNT Libraries Government Documents Department

Recent progress in irrational conformal field theory

Description: In this talk, I will review the foundations of irrational conformal field theory (ICFT), which includes rational conformal field theory as a small subspace. Highlights of the review include the Virasoro master equation, the Ward identities for the correlators of ICFT and solutions of the Ward identities. In particular, I will discuss the solutions for the correlators of the g/h coset construction and the correlators of the affine-Sugawara nests on g {contains} h{sub 1} {contains} {hor_ellipsis} {contains} h{sub n}. Finally, I will discuss the recent global solution for the correlators of all the ICFT`s in the master equation.
Date: September 1, 1993
Creator: Halpern, M. B.
Partner: UNT Libraries Government Documents Department