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Process Development of 2,2-Dinitropropyl Acrylate

Description: Abstract: Developmental production of approximately 500 pounds of 2,2-dinitropropanol and 250 pounds of 2,2-dinitropropyl acrylate was carried out in a 50-gallon capacity stainless-steel reactor system. The intermediate alcohol was produced in a yield of 73%. The ester was made with a yield of 78%. Cost studies show that the manufacturing cost for DNPA monomer should approximate $2.70 per pound on a production basis of 30,000 pounds, with an indicated plant cost of $4.60 per pound for the polym… more
Date: October 1955
Creator: Benziger, T. M.; Rohwer, R. K. & Stein, W. H.
Partner: UNT Libraries Government Documents Department
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Determination of Hydrogen in Lithium Hydride

Description: Abstract: "A method for determining hydrogen in lithium hydride by heating samples with lead at 600 C, was developed. The hydrogen evolved during thermal decomposition of the hydride is purified and oxidized to water with cupric oxide at 400 C. The analysis is completed by collecting and weighing this water. Success in development of the analytical procedure has depended upon a careful design and assembly of equipment for handling samples in a dry, inert atmosphere. For seven pure hydride sampl… more
Date: May 1954
Creator: Bergstresser, K. S. & Waterbury, Glenn R.
Partner: UNT Libraries Government Documents Department
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Preliminary Report on Thermal and Electrical Conductivities of Some Plutonium-Aluminum Alloys

Description: Abstract: "The thermal and electrical conductivities of a series of Pu-Al alloys have been determined in the range 0.12 atomic percent Pu. The conductivities are approximately proportional to the volume of free aluminum."
Date: March 15, 1950
Creator: Gibney, Robert B. & Sandenaw, Thomas A.
Partner: UNT Libraries Government Documents Department
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A Method for Rolling Uranium Foil

Description: "This report gives briefly a rather simple method for fabricating foils from uranium buttons. Two log sheets one of a U-238 run and one of a U-255 run are given."
Date: October 21, 1947
Creator: Bernard, George L., (Jr.)
Partner: UNT Libraries Government Documents Department
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Fall-Out Studies with a Laboratory Controlled Model

Description: From abstract: "To seek information for a better understanding of the phenomena involved in fall-out, a fireball effect was simulated in a small closed room by subjecting various materials to a high-current (~360 amp.) are produced between graphite electrodes, and anode being impregnated with radioactive materials. The time duration of the arc, power dissipated, and distance from the samples were controlled. The radioactivity which remained airborne, that which settled out onto the floor and it… more
Date: August 1955
Creator: Kalil, Ford
Partner: UNT Libraries Government Documents Department
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Consolidation and shaping of boron ; summary of previous work

Description: From abstract: "The deposit on the rods is in the form of a brittle uneven tube which is cracked off and subsequently pulverized to a 200-mesh powder. This report is chiefly concerned with methods of consolidating this powder and shaping it into forms required, though it also discusses to some extent other methods of shaping boron or born-rich materials."
Date: October 8, 1945
Creator: Kamm, Robert L.
Partner: UNT Libraries Government Documents Department
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Notes on Evaporation of Target Materials

Description: Abstract: "The general utility of vacuum evaporated films is discussed. The characteristics that makes this technique most useful are the uniformity of the films, the easy control of their thickness over a large range, and the adaptability of the system to different metals and compounds. The design of a vacuum evaporator should provide adequate pumping speed, cooling of components, filament heater supply, and general flexibility and adaptability of the components to different materials. The des… more
Date: March 1953
Creator: Northrop, J. A. & Stokes, R. H.
Partner: UNT Libraries Government Documents Department
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Survey of Los Alamos and Pueblo Canyon for Radioactive Contamination and Radio Assay Tests Run on Sewer-Water Samples and Water and Soil Samples Taken From Los Alamos and Pueblo Canyons

Description: "Report of the Survey of Los Alamos and Pueblo Canyon for radioactive contamination and radioassay tests run on sewer water samples and water and soil samples taken from Los Alamos and Pueblo Canyons." The objective of this report was to determine the extent and sources of radioactive contamination in the areas studied.
Date: February 20, 1947
Creator: Kingsley, William H.; Fox, Alvin; Tribby, J. F. & Doner, Elmer
Partner: UNT Libraries Government Documents Department
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Fraunhofer Diffraction Pattern Produced by a Slit of Varying Width and its Application to High Speed Cameras

Description: Abstract: "A theoretical and experimental investigation is made of the diffraction pattern produced by a slit, whose aperture varies uniformly from a constant value A to zero. The results of this investigation are applied to a proposed high speed camera. It is shown that diffraction effects are very serious and cannot be neglected. It seems, unless the suggested design of this high speed camera is changed, the camera will be of little use for accurate measurements, and photographs will show too… more
Date: November 11, 1947
Creator: Geiger, F. E. & Brixner, Berlyn
Partner: UNT Libraries Government Documents Department
open access

An Optical Fallout Analogue

Description: This report describes the optical analogue that contains an optical filtering system which controls the intensity of light according to the assumed initial distribution of activity over height and particle size and according to the assumed decay rate, a size control system which depends on the lateral dimensions of the cloud of debris and adjusts the size of the light beam accordingly, and a position control system which moves the beam to the correct position on the plate as determined by the w… more
Date: October 1955
Creator: Felt, Gaelen L.
Partner: UNT Libraries Government Documents Department
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Heat Treatment and Machinability of Beryllium Rod

Description: Purpose: "The purpose of this investigation was to determine whether or not the machinability of extruded beryllium rod could be improved by appropriate heat treatment. It was thought that this could be accomplished in the extruded Be rod by recrystallization without further growth of these grains. This should impart a certain degree of ductility to the metal. The investigations was divided into two parts: Part I - Heat Treatment of Beryllium Rod; Part II - Machinability of Beryllium Rod."
Date: February 19, 1946
Creator: Norhaft, P. C.
Partner: UNT Libraries Government Documents Department
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A Survey of Some Los Alamos County Canyons for Radioactive Contamination, Spring 1953 to Spring 1955

Description: Abstract: This document is a survey analysis of soil samples from Los Alamos, Pueblo, Bayo, and Mortandad canyons to determine the presence and activities of radioactive contaminants. Also included are the results of analyses of a few samples of grass and of surface water. This survey covers the period from spring 1953 to spring 1955.
Date: April 1956
Creator: Dodd, Aubrey O.
Partner: UNT Libraries Government Documents Department
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The Wind Variability of Fall-Out Patterns

Description: The following report investigates part of the variability of the computed fall-out intensity patterns due to the variability of the winds, on the basis of winds from four Pacific shot days. An extreme case from Operation Sandstone is also considered.
Date: March 1956
Creator: Sherman, Leon
Partner: UNT Libraries Government Documents Department
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Spontaneous Fission of 48

Description: Report discussing an experiment to reinvestigate the spontaneous fission of 48 (Pu-238) in an effort to determine a more accurate value for the spontaneous fission constant that was found in a previous experiment.
Date: December 19, 1949
Creator: Jungerman, John A.
Partner: UNT Libraries Government Documents Department
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Separation of Small Amounts of Scandium From Uranium

Description: Abstract: A method for separating small amounts of scandium (1 to 10 mg.) from a gram of uranium depends upon formation of insoluble uranium peroxide while the scandium in solution is complexed with ethylenediamine-tetraacetic acid. The precipitated peroxide carries down less than 30 p.p.m. of scandium. Uranium left in solution, less than one milligram in amount, does not interfere when the scandium is precipitated as ammonium scandium tartrate and determined gravimetrically by ignition of the … more
Date: May 1954
Creator: Bergstresser, Karl S.
Partner: UNT Libraries Government Documents Department
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Safety Tests on Hand Stacking of U-235 Cubes

Description: From abstract: "Critical assembly tests have been made on the Pajarito Universal Machine to determine the safety limits of handstacking cubes of 95% U-235 in spherical geometries preparatory to making critical assemblies of U-235 in an "infinite" tuballoy tamper. The U-235 cubes were stacked as pseudospheres in a cavity at the top of a tuballoy block 12" high and 8" on a side, and the assembly tamped by locating it inside a doughnut shaped water tank whose tamping effect is equivalent to the ta… more
Date: October 11, 1948
Creator: Josephson, V.; Young, D. S. & Dike, R. S.
Partner: UNT Libraries Government Documents Department
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Influence of Gamma Irradiation on RG 8/U Cable

Description: Abstract: "Static measurements have been made of the currents produced by Co-60 gamma irradiation of solid dielectric RG 8/U cable. Sensitivity curves are presented as a function of the magnitude and polarity of the collection voltage to 90 volts. It is shown that the current is due to a polarity- and voltage-sensitive ionization component and to a polarity- and voltage-insensitive component attributed to the Compton process. The total cable sensitivity at -90 volts, with saturation not achieve… more
Date: November 1955
Creator: Kloepper, Robert M.
Partner: UNT Libraries Government Documents Department
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