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Field Raman spectrograph for environmental analysis

Description: The enormous cost for chemical analysis at DOE facilities predicates that cost-saving measures be implemented. Many approaches, ranging from increasing laboratory sample throughput by reducing preparation time to the development of field instrumentation, are being explored to meet this need. Because of the presence of radioactive materials at many DOE sites, there is also a need for methods that are safer for site personnel and analysts. This project entails the development of a compact Raman spectrograph for field screening and monitoring of a wide variety of wastes, pollutants, and corrosion products in storage tanks, soils, and ground and surface waters. Analytical advantages of the Raman technique include its ability to produce a unique, spectral fingerprint for each contaminant and its ability to analyze both solids and liquids directly, without the need for isolation or cleanup.
Date: December 1, 1995
Creator: Haas, J.W. III; Forney, R.W.; Carrabba, M.M. & Rauh, R.D.
Partner: UNT Libraries Government Documents Department

Field Raman Spectrograph for Environmental Analysis

Description: The widespread contamination found across the US Department of Energy (DOE) complex has received considerable attention from the government and public alike. A massive site characterization and cleanup effort has been underway for several years and is expected to continue for several decades more. The scope of the cleanup effort ranges from soil excavation and treatment to complete dismantling and decontamination of whole buildings. To its credit, DOE has supported research and development of new technologies to speed up and reduce the cost of this effort. One area in particular has been the development of portable instrumentation that can be used to perform analytical measurements in the field. This approach provides timely data to decision makers and eliminates the expense, delays, and uncertainties of sample preservation, transport, storage, and laboratory analysis. In this program, we have developed and demonstrated in the field a transportable, high performance Raman spectrograph that can be used to detect and identify contaminants in a variety of scenarios. With no moving parts, the spectrograph is rugged and can perform many Raman measurements in situ with flexible fiber optic sampling probes. The instrument operates under computer control and a software package has been developed to collect and process spectral data. A collection of Raman spectra for 200 contaminants of DOE importance has been compiled in a searchable format to assist in the identification of unknown contaminants in the field.
Date: July 1, 1998
Creator: Sylvia, J.M.; Haas, J.W.; Spencer, K.M.; Carrabba, M.M.; Rauh, R.D.; Forney, R.W. et al.
Partner: UNT Libraries Government Documents Department