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Measurement assurance program for LSC analyses of tritium samples

Description: Liquid Scintillation Counting (LSC) for Tritium is done on 600 to 800 samples daily as part of a contamination control program at the Savannah River Site`s Tritium Facilities. The tritium results from the LSCs are used: to release items as radiologically clean; to establish radiological control measures for workers; and to characterize waste. The following is a list of the sample matrices that are analyzed for tritium: filter paper smears, aqueous, oil, oily rags, ethylene glycol, ethyl alcohol, freon and mercury. Routine and special causes of variation in standards, counting equipment, environment, operators, counting times, samples, activity levels, etc. produce uncertainty in the LSC measurements. A comprehensive analytical process measurement assurance program such as JTIPMAP{trademark} has been implemented. The process measurement assurance program is being used to quantify and control many of the sources of variation and provide accurate estimates of the overall measurement uncertainty associated with the LSC measurements. The paper will describe LSC operations, process improvements, quality control and quality assurance programs along with future improvements associated with the implementation of the process measurement assurance program.
Date: May 1, 1997
Creator: Levi, G.D. Jr. & Clark, J.P.
Partner: UNT Libraries Government Documents Department

Liquid-helium scintillation detection with germanium photodiodes

Description: Special high-purity germanium photodiodes have been developed for the direct detection of vacuum ultraviolet scintillations in liquid helium. The photodiodes are immersed in the liquid helium, and scintillations are detected through one of the bare sides of the photodiodes. Test results with scintillation photons produced by 5.3-MeV ..cap alpha.. particles are presented. The use of these photodiodes as liquid-helium scintillation detectors may offer substantial improvements over the alternate detection method requiring the use of wavelength shifters and photomultiplier tubes.
Date: May 1, 1982
Creator: Luke, P.N.; Haller, E.E. & Steiner, H.M.
Partner: UNT Libraries Government Documents Department

Measurement of actinides in environmental samples by Photo-Electron Rejecting Alpha Liquid Scintillation

Description: This work describes the adaptation of extractive scintillation with a Photo-Electron Rejecting Alpha Liquid Scintillation (PERALS) (ORDELA, Inc.) spectrometer to the analysis of actinides in environmental samples from the Savannah River Site (SRS). Environmental quality assurance standards and actual water samples were treated by one of two methods; either a two step direct extraction, or for more complex samples, pretreatment by an extraction chromatographic separation prior to measurement of the alpha activity by PERALS.
Date: May 1, 1994
Creator: Cadieux, J. R.; Clark, S.; Fjeld, R. A.; Reboul, S. & Sowder, A.
Partner: UNT Libraries Government Documents Department