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Zirconium Pilot Plant Research and Development Progress Report

Description: The following progress report was compiled by the research and development division of the zirconium pilot plant. This report discusses two iodination and deposition runs that were completed as of August 20, 1951, as well as the third iodination run that uses a vaporizer condenser that condenses approximately 40 pounds of zirconium iodide.
Date: September 20, 1951
Creator: Accountius, O. E.; Black, D. G.; Dryden, C. E.; Finney, B. C.; Gruber, B. A.; Jurevic, W. G. et al.
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Electroplates on Thorium

Description: Abstract: "The protection of thorium in hot water was studied. Copper electrocladding on thorium offers promising protection against hot water. The corrosion of thorium in 95 C water was reduced appreciably by a thorium phosphate film. The results of this abbreviated investigation offer a basis for the development of a method of protecting thorium at elevated temperatures in corrosive media."
Date: January 9, 1953
Creator: Beach, John G.; Schickner, W. C.; Vaaler, L. E. & Faust, Charles L.
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Dissolution of Aluminum-Canned Thorium

Description: The following report studies the dissolution of aluminum-canned thorium, providing results that suggest a dissolution cycle that permits the separation of the canned-slug components.
Date: July 26, 1955
Creator: Beach, John G.; Schickner, William C. & Faust, Charles L.
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Electrodeposition of Aluminum on Uranium

Description: Abstract: "Aluminum electroplating was studied in a search for new methods of cladding uranium fuel elements. Uranium electroclad with 12 mils of aluminum over a 0.5-mil (or nickel plus copper) electroplate resisted corrosion for more than 100 hr in boiling water. This quality of protection was effected by hot pressing the electroclad uranium with 5.1 tons per sq in. for 5 min at 950 F. The electroclad uranium with hot-pressed samples paralleled those of later experiments with hot-pressed wroug… more
Date: March 30, 1955
Creator: Beach, John G.; Schickner, William C.; Hopkinson, Dolores. & Faust, Charles L.
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Electroplated Metals on Uranium for Aluminum Cladding

Description: Abstract: "Aluminum-clad nickel-plated uranium is corrosion resistant in boiling water. Samples with intentional defects in the aluminum-nickel clodding layers, after testing for more than 300 hr. showed no sign of rapid failure. The study of electroplated metals on uranium for aluminum cladding has defined the effects of several processing variables on the corrosion resistance. The quality of the uranium and the quality of the aluminum-nickel bond were important. Heat treatment and vacuum outg… more
Date: May 4, 1955
Creator: Beach, John G.; Schickner, William C.; Hopkinson, Dolores. & Faust, Charles L.
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Carbide Coatings on Graphite

Description: From abstract: "A Method has been developed for the uniform coating of graphite tubes with carbides of niobium, tantalum, and zirconium by thermal composition of their respective halide vapors."
Date: 1957
Creator: Blocher, John M., Jr.; Ish, Carl J.; Leiter, Don P.; Plock, Layne F. & Campbell, Ivor E.
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Zirconium Research and Development : Progress Report

Description: From introduction: "This is the ninth monthly report, BMI-514, under Contract No. AT(30-1)-771 on "Zirconium Research and Development". The report covers the work period from September 15, 1950, to October 15, 1950. Work is continuing on the preparation of large-diameter zirconium crystal bars in the 16-inch-diameter de Boer unit. Crystal bars up to 1-5/16 inches in diameter and 8 feet long have been prepared in this unit."
Date: October 15, 1950
Creator: Bulkowski, H. H.; Sebenick, J. J.; Campbell, Ivor E. & Gonser, B. W.
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Final Report on Purification of Thorium Nitrate by Solvent Extraction With Tributyl Phosphate: 2. Mixer-Settler Pilot Plant Investigations

Description: From abstract: "This report describes the construction and operation of a mixer-settler pilot plant for the purification of mantle-grade thorium nitrate. The liquid-liquid extraction process utilized 30% tributyl phosphate - 70% 'Solvesso-100' as the organic solvent and nitric acid as the salting agent. Continuous steady-state operation of the equipment was demonstrated, with very good recovery of thorium."
Date: July 31, 1952
Creator: Burkhart, C. A.; Foley, D. D.; Retzke, F. A.; Filbert, Robert B., Jr. & Clegg, John W.
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Estimated Manufacturing Costs for the Recovery of Thorium and Uranium from Monazite Sand

Description: Abstract: "Costs have been estimated for the production of uranium and pure thorium from monasite concentrates by a process involving (1) reaction of monasite with caustic soda, (2) dissolution of the hydrous oxides in hydrochloric acid, (3) separation from the bulk of the rare earths by hydroxide precipitation of thorium and uranium, and (4) purification by solvent extraction."
Date: September 15, 1950
Creator: Calkins, G. D. & Filbert, R. B., Jr.
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Final Report on Recovery of Thorium and Uranium From Monazite Sand : Volume 1

Description: Report describing a method for recovery of high yields of thorium and uranium from monazite sand concentrates. Monazite is decomposed into hydrous metal oxides, which are dissolved in an acid. The solution is then separated into a precipitate, which seperates from thorium and uranium. An alternate separation method is evaluated.
Date: September 15, 1950
Creator: Calkins, G. D.; Filbert, R. B., Jr.; Bearse, A. E. & Clegg, J. W.
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Corrosion in 650 F Degassed Water of Uranium-Molybdenum Alloys Containing Impurity Additions

Description: From introduction: "At the request of WAPD, a study has been made of the effect of minor compositional variables on the corrosion behavior of uranium-molybdenum alloys in 650 F degassed water."
Date: October 6, 1955
Creator: Cawthorne, Edward W.; Berry, Warren E., 1922-; Reynolds, James E.; Jaffee, Robert Isaac, 1917- & Peoples, Robert S.
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The Determination of Rare Earths in Thorium

Description: Abstract: "A quantitative method for the determination of individual rare earths in thorium down to a level of 0.05 ppm, is described. The procedure consists of a chromatographic cellulose-columns separation followed by a solution-type spectrographic determination. Values are given for the recovery of a number of rare earths using this combined procedure."
Date: May 15, 1952
Creator: Center, E. J.; Henry, W. M. & Householder, R. D.
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