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Corrosion resistance and magnetic susceptibility

Description: From summary: "On the basis of the tests described herein, the corrosion characteristics of T-347 welded stainless steel are found not to be affected by the magnetic properties of the welds even though these properties are likely the result of the presence of the ferritic structure."
Date: March 7, 1949
Creator: Koenig, W. W. & Heckman, R. L.
open access

The Solvent-Extraction Performance of Redox IC Columns (ANL June 1948 Flowsheet) Using Raschig Ring Packing, and Unirradiated Uranium: Redox Technical Study No. 14

Description: A report which summarizes the performance data obtained from Redox solvent extraction IC Column studies made prior to January 15, 1949 in accordance with conditions of the A.N.L. June 1, 1948, Flowsheet.
Date: August 22, 1949
Creator: Hartzell, L. O.; Woodfield, F. W. & Bradley, J. G.
open access

Urine Analysis for Tritium Oxide

Description: This report analyzes a procedure based on the production of acetylene from the active water, with subsequent measurement of the ionization caused by the tritium beta particle. This eliminates the troublesome absorption on the chamber walls when hydrogen is used, and provides a rapid method for the preparation of the urine samples.
Date: July 27, 1949
Creator: Healy, J. W.
open access

A Rapid Colorimeric Method for the Determination of Phosphate in Uranium Waste Solutions

Description: Report discussing tests of a new colorimetric method. From abstract: "A colorimetric method, which is a modification of the classical phosphomolybdic acid method, has been developed for the determination of phosphate in synthetic uranium waste solutions...The chief advantage of the method, over those presently included in HW Manuals, is the rapidity with which determinations may be carried out."
Date: August 22, 1949
Creator: Sege, C. A. & Ice, C. H.
open access

The Identification and Determination of Trace Amounts of Rare Earth Elements in Graphite by Neutron Activation

Description: Abstract: "A method is described for the identification and quantitative determination of trace amounts of rare earths in graphite by measurement of the energies and decays of the activities induced by neutron irradiation. The specific rare earth elements identified are europium and samarium. During the development of this method, the half-lives of Eu-152 and Sm-153 were determined. These are reported as 9.32 +/- 0.04 hours and 46.34 +/- 0.23 respectively."
Date: September 1, 1949
Creator: Ross, A. M.
open access

Stepwise Calculation for the Determination of the Number of Transfer Units in Countercurrent Extraction Columns

Description: Report discussing a method for the stepwise calculation of the number of transfer units utilized in a given solvent extraction operation. "Use of the method results in a very appreciable saving in time of calculation with an error of 1.5% for the runs tested. The error tends to become smaller with increasing total numbers of transfer units involved."
Date: September 12, 1949
Creator: Burns, W. A. & Eschbach, E. A.
open access

Effect of Temperature on Beta-Ray Measurements

Description: Summary: "This report investigates photographic methods of measuring beta radiation and includes a study of temperature effects on these measurements. Experimental data are submitted to show that an increase in film temperature before and during beta irradiation causes a definite increase in density for the same dosage. Recommendations drawn from experience gained in the experimental works are offered."
Date: November 23, 1949
Creator: Stevens, A. J.
open access

Diameter Measurements of Slugs Before and After Prolonged Heat Treatment

Description: Abstract: "Diameter measurements of 25 slugs taken before and after a prolonged heat treatment showed no evidence of differences that would indicate blistering. The average effects of the treatment was different for the various slugs. Large differences in diameter measurements between slugs. Large differences in diameter between slugs and significant differences between indices and positions were found."
Date: February 16, 1948
Creator: Bennett, Carl A. & Lane, J. J.
open access

General Engineering and Consulting Laboratory "Hot Service" Turbine Pump Progress Report: May 1 to June 15, 1948

Description: Introduction: "This report covers progress on the testing of the General Engineering and Consulting Laboratories Turbine Pump No. 1 from May 1, 1948 to Jun 15, 1948. All testing prior to April 30, 1948 has been described in Redox Experiment Testing Report No. 1 (Document HW-9474) and No. 2 (Document HW-9694)."
Date: June 21, 1948
Creator: Stringer, J. T. & Allen, A. W.
open access

Zirconium Pheylarsonate Tracer Scale Method for the Differentiation of Pu(III) and Pu(IV) in Redox Solutions

Description: The following report studies an estimation of the amount of Pu(III) and Pu(IV) present in the IBP Stream, with the purpose of establishing an analytical, method suitable for routine control analysis. A method is discussed that is based on carrying Pu(IV) upon a zirconium phanylarsonate precipitate.
Date: June 30, 1948
Creator: Ice, C. H.
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