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Annual Report 1961: This seventh Annual Report is a summary of some of the progress in scientific and engineering research and development carried on at Argonne National Laboratory during 1961. As is customary in this series, only those portions of the total program that have reached such a stage that they may be of general interest are recorded. Thus, a comparison with the Annual Reports for 1959 (ANL-6125) and for 1960 (ANL-6275) will reveal the description of a generally different set of scientific activities. A more detailed presentation of any work covered in this report or of the many ANL projects not mentioned may be obtained by perusing the various progress and topical reports issued by the Laboratory during 1961. A list of the publications in the scientific journals during 1961 by Argonne personnel has been given as an Appendix.
Operating Manual for the Argonaut Reactor: The design of the Argonaut (Argonne Nuclear Assembly for University Training) was initiated by the Reactor Engineering Division of Argonne National Laboratory to satisfy needs for a low-power reactor facility within the Laboratory, and for training uses within the international School of Nuclear Science and Engineering (ISNSE). It was intended primarily for instruction and research in reactor physics. It was also considered as a possibility that it would fulfill the requirements of universities engaged in a program of nuclear science. The cost of the facility was to be kept to a minimum consistent with the high degree of inherent safety and a great amount of flexibility in the system. The basic design stemmed from the Knolls Atomic Power Laboratory Thermal Test Reactor* (TTR), now called Nuclear Test Reactor (NTR). Modification during the course of the work justified the new name "Argonaut".
Chemical Engineering Division Summary Report for January, February, and March 1958: Development work was continued on the fused fluoride process for the recovery of enriched uranium from zirconium-matrix fuel alloys. The alloy is dissolved by immersing it in molten sodium fluoride-zirconium fluoride at 600°C and passing hydrogen fluoride vapor through the system.The dissolved uranium tetrafluoride in the melt is then volatilized as uranium hexafluoride by sparging with fluorine. The uranium hexafluoride product is purified and decontaminated by fractional distillation. Additional corrosion tests were made on a variety of metals in an effort to find a material of construction suitable for the fluorination step. All the metals tested, with the exception of Hastelloy B, were attacked rapidly in the fluorinated melt. The attack was particularly severe at the melt-gas interface when tests were made with partially submerged specimens of the metals.
The Fabrication of a Plutonium Helix for a Doppler Experiment: A helix constructed of plutonium was made to test the Doppler temperature effect in ZPR-III. The helix, 1 inch in diameter and 6-1/4 inches long, contained 240 grams of delta-phase plutonium alloy encapsulated in titanium tubing. Four plutonium rods were extruded, joined together, and pushed into a titanium tube. This tube was swaged tightly over the plutonium rod, and the assembly was wound into a coil. Electrical leads to the coil were made by swaging copper tubing over the ends of the coil. The helix was tested by cycling about 500 times between 50°C and 190°C. The coil was heated with a current of 130 amperes and cooled with a blast of chilled helium. (1) Several helices of uranium(2) were cycled during the same tests. Despite the severity of the thermal cycles, the helices were undamaged.
A laboratory Ivestigation of the Fluorination of Crude Uranium Tertrafluoride: Ore concentrates have been converted directly to crude uranium tetrafluoride by hydrogen reduction and hydrofluorination in fluidized-bed reactors. Small-scale laboratory experiments demonstrated that this process can be extended to the production of crude uranium hexafluoride through fluorination of the uranium tetrafluoride in a fluidized bed. The satisfactory temperature range for the reaction lies between 300°C and 600°C. At 450°C the fluorine utilization is between 50 and 80 per cent. With excess fluorine, over 99 per cent of the uranium is volatilized from the solid material. The fluidization characteristics of certain materials are improved by the addition of an inert solid diluent to the bed.
Chemical Engineering Division Summary Report July, August, and September, 1957: Development work continued on a fused salt process for the recovery of uranium from zirconium-matrix fuel alloys. The fuel is dissolved in a sodium fluoride-zirconium fluoride melt at 600°C by hydrogen fluoride sparging. The melt is then sparged with fluorine gas which volatilizes the dissolved uranium as the hexafluoride. The final decontamination and purification of the uranium hexafluoride are accomplished by fractional distillation. The testing of graphite as a container material for the hydrofluorination step was continued. Additional thermal cycling experiments were performed, using a helium sparge in equimolar sodium fluoride-zirconium fluoride melt at 600°C. The extent of penetration of the fused salt into the graphite was determined. No mechanical degradation was present. Dimensional change data were also obtained for graphite vessels in which the fused salt was sparged with hydrogen fluoride.
Chemical Engineering Division Summary Report for January, February, and March 1957: A fused fluoride process for dissolution of zirconium-uranium fuel alloys is being developed. The alloy is dissolved in an equimolar sodium fluoride-zirconium fluoride melt at 600°C by sparging the system with hydrogen fluoride. The uranium is volatilized from the melt as the hexafluoride by a sparging operation with fluorine or bromine pentafluoride vapor. This product is then decontaminated and purified by fractional distillation.
Quarterly Report October, November and December, 1956: Methods of producing extremely clean surfaces on rolled Zircaloy-2 strip have been investigated. It has been found that the finer abrasives, 400 mesh or finer, are more effective than coarse types because of their ability to penetrate pits and crevices more readily. Two such cleanings, with an intermediate 35 v/o HNO3-5 v/o HF pickle, resulted in a microscopically clean surface. Ultrasonic inspection of the EBWR fuel plates has been completed during this quarter. Approximately 95% of the plates were found acceptable. All subassemblies manufactured from the EBWR plates met dimensional specifications and passed 9-day corrosion tests at 290°C (550°F). All thoria-urania pellets for the loading of Borax-IV have been pressed, loaded into tube plates, and fabricated into subassemblies. The total number of subassemblies made was 82, of which 72 were fuel plates and 10 were blanket plates, more than sufficient for the loading. The reactor has gone critical using this loading.
A Coated Cast Iron Crucible for use with Eutectic Al-Si Alloy in the Temperature Range 595°-650°C: The feasibility of the coated metal crucible as a container for eutectic Al-Si alloy has been proven by test. Small, enamel-coated cast iron pots has been proven by test. Small, enamel-coated cast iron pots have successfully withstood the chemically aggressive Al-Si alloy and the adverse influence of an oxidizing atmosphere for a period of 3 months at 725°C. A similarly coated castiron crucible containing 450 pounds of eutectic Al-Si alloy was successfully tested for 144 days in a jacketing operation conducted at 595°-650°C. Under the same conditions, the normal service life of clay-bonded graphite and silicon carbide crucibles rarely exceeds 45 days. The coating material is a commercially available enamel capable of withstanding temperatures up to 790°C (1450°F). It is readily applied to the surface of a variety of ferrous metals and alloys; however, best results are obtained with alloys low in chromium and nickel which also have a low thermal expansion coefficient.
Chemical Engineering Division Summary Report October, November, and December, 1956: A final series of runs was made in a four-inch continuous-flow mixing chamber to study the transfer of isobutanol into water and nitrobenzene into ethylene glycol. Satisfactory techniques were developed to provide for the rapid analysis of these systems. In addition, a light-scattering correlation was prepared to provide a measure of the interfacial area of the yellow-colored nitrobenzene-ethylene glycol mixtures.
Metallurgy Division Quarterly Report [for] October, November, and December 1955: A total of nine clad plates, containing uranium -5 w/o zirconium 1.5 w/o niobium alloy cores and clad with Zircaloy-II, were rolled in plain carbon steel jackets, heat treated, physically evaluated, and corrosion tested. All these plates were found to be within predetermined dimensional tolerance in width, thickness, length, cladding thickness, and core distribution. Improved control of wielding variables and of the length of the seal pin projecting above the end plugs resulted in the elimination of frequently observed segmented inclusions at the seal pin interfaces.
Chemical Engineering Division Summary Report: Measurement of radioactive carry-over was made on borax III operating at 300 psig and at power levels ranging from 4 to 14 mv. Decontamination factors of from 1.5 x 104 (at 14 mv) were obtained. These data are in essential agreement with those predicted by previous laboratory experimental work.
Quarterly Report January, February and March, 1956: The EBWR loading requires a total of 888 plates. It is anticipated that approximately 1000 plates will have to be produced to obtain the number of acceptable plates required for the loading. To the end of this quarter, 568 cladding billet cores acceptable with respect to chemical composition and physical soundness had been cast; this number represents 78% of the total number of cores cast. Approximately 75% of the Zircaloy-II stock required has been rolled, and about 55% of the cladding components required have been finished. The anticipated number of 495 cladding billets required for the thin (0.210") natural and enriched plates have been assembled, welded, sealed, and jacketed in steel. A total of 310 cladding billets have been rolled to fuel plates; of this number, 142 have been completely finished, and the remaining 168 are in the finish processing stages. The stability of the equipment for measuring the clad thickness of EBWR fuel plates has been improved by placing the phototube and the anthracene scintillator crystals in an insulated box with a temperature regulation of the order of 0.1°F.
The Fabrication of Prototype Fuel Elements for the Experimental Boiling Water Reactor and the Experimental Breeder Reactor: The purpose of this program was to develop techniques and methods for producing fuel elements for the Experimental Boiling Water and Experimental Breeder Reactors. Methods for fabricating large tubes, flat plates, and small pins were investigated. The tube and plates contained U-5 w/o Zr-1.5 w/o Nb alloy and were designed for the EBWR. The pins contained U-2 w/o Zr alloy and were designed for the EBR. Cladding and end seal material of Zircaloy-2 was required for the water-cooled EBWR elements. Unalloyed zirconium was specified for cladding on the sodium-cooled EBR elements.
Quarterly Progress Report on Reactor Development 400 Program: Physics calculations have been made for various combinations of the four types of fuel assemblies to be used in the EBWR core. Two thicknesses of plates, 0.205 in. and 0.274 in., including the two 0.020-in. cladding layers, are to be made of both natural U and U containing 1.44% U235. A total of 148 assemblies, 74 natural and 74 enriched, are to be fabricated with six identical plates each. Various configurations of these fuel assemblies will be used to (1) change the critical size of the core, (2) change the power distribution in the core, and (3) change the amount of reactivity corresponding to a given stream volume in the core. The physics calculations show that uncertainties in critical mass are adequately covered by the number and variety of fuel assemblies and that the possible changes in core characteristics with the different fuel assemblies should provide valuable information about the factors affecting maximum power density and stability in a boiling water reactor.
Chemical Engineering Division Summary Report July, August, and September, 1956: Additional runs have been made in the six-inch, continuous-flow mixing chamber to study the rate of mass transfer between isobutanol and water. These runs were inconclusive because the effluents were mutually saturated. A new four-inch cell has been designed and is being fabricated; this will permit a reduction in the time available for mass transfer. Consideration has been given to other liquid pairs which may transfer more slowly than isobutanol-water. The system nitrobenzene-ethylene glycol appears attractive.
Reactor Engineering Division Quarterly Report Section I January, February, March. 1956: Physical calculations have been performed for various combinations of the four types of fuel assemblies to be used in the EBWR core. Two thicknesses of plates (0.205 in. and 0.274 in., including two 0.020-in. cladding layers) are to be made of both natural uranium and uranium containing 1.44% U235. Any given fuel assembly contains six identical plates. A total of 148 assemblies, 74 natural and 74 enriched, are to be fabricated. Various configurations of these fuel assemblies can be used to (1) change the critical size of the core, (2) change the power distribution in the core or (3) change the amount of reactivity corresponding to a given steam volume in the core. Physics calculations show that any uncertainties in the required critical mass are adequately covered by the number and variety of fuel assemblies, and that the changes in core characteristics possible with the different fuel assemblies should provide valuable information about the factors affecting maximum power density and stability in a boiling reactor.
The Manufacture of Enriched ZPR-III Fuel Plates: This report is essentially a procedural account of the fabrication of certain enriched ZPR-III fuel plates for use in the ANL fast critical experiments at Arco, Idaho. A total of 208.92 kilograms of fully enrich, unalloyed uranium was processed. Of this amount 202.74 kilograms was received in the form of Oak Ridge type reduction buttons and 6.18 kilograms as pressed-powder plates. The completed fabrication consisted of 720 rectangular fuel plates having the nominal dimensions 3in. x 2in. x 1/8in. Their combined weight of 159.21 kilograms represents 76.22% of the weight of enriched material processed. The final distribution of the enriched material was as follows: [figure not transcribed].
Table of Sin θ and Sin2 θ for Values of θ from 2° to 87°: The table of sin θ and sin2 θ, to five decimal places for every hundreth of a degree from 2°-87°, has been prepared for the use of Professor W. H. Zachariasen in his X-ray diffraction studies. [Tables not transcribed]
Summary Report of the Hazards of the Internal Exponential Experiment (ZPR-V): The Internal exponential Exponential Experiment (ZPR-V) will be constructed by loading up to 49 of the fuel cans, containing up to 155 kg of U235, of the present Fast Exponential Experiment in a 22-in. square iron tank, surrounded by an annular thermal region of fully enriched light water lattice 10 to 15 cm thick. This assembly will be placed in a 5-ft diameter tank which will, in turn, be located in the 10-ft diameter ZPR-II tank, the annular space between the outer tanks containing water for shielding. The new experiment will be a well-shielded, strongly coupled fast-thermal system. It will be possible to make measurements that cannot be made on the present Fast Exponential Experiment. One category of such determinations is the study of reactivity effects produced in the fast core, including control scheme studies and danger coefficient and oscillator measurements of such effects as Doppler coefficients and effect of lumping and streaming. The higher flux and excellent shielding will make beam studies of energy spectrum practical. Additional foil activations will be possible. Characteristics of mixed fast-thermal systems, which are of potential importance as power breeders, can be studied.
Reactor Engineering Division Quarterly Report [for] October, November, December 1955. Section I: The gastight steel building (400,000 cu ft) in which all radioactive components are to be housed has been completed by the Graver Tank Company. This structure was tested for strength at 18.75 psig (20% above design pressure) and then tested for leaks. No leaks were found in soap bubble testing of all welded seams. Continuous measurements of temperature and pressure over a ten-day period showed the leakage, if any, to be less than the 500 cu/ ft/day at 15 psig specified. The gastight cylinder was, therefore, accepted. General construction work by the Sumner Sollitt Company on the remainder of the plant has begun.
ALPR Preliminary Design Study (Argonne Low Power Reactor) Phase 1: A preliminary design study, Phase I of the ALPR project, has been made in accordance with the Army Reactors Branch specifications for a nuclear "package" power plant with a 200-260-kw electric and 400 kw heating capacity. The plant is to be installed at the Idaho Reactor Testing Station as a prototype for remote arctic installations. The "conventional" power plant as well as the exterior reactor components are described in the accompanying report and cost estimate by Pioneer Service and Engineering Company, Architect-Engineers for the project."Nuclear" components of the reactor are designed by Argonne National Laboratory as described in the present report.
The Regeneration Factor as a Function of Time in a Th232 - U235 Thermal Reactor: This technical report is concerned with a theoretical investigation of the variation of the regeneration factor [gamma] in a Th232 - U235 thermal reactor. The abundances of the significant isotopes in the thorium-uranium cycle have been derived as a function of irradiation time at constant reactor power. The change in [gamma] as a function of irradiation time at constant power was calculated for combinations of enrichment and resonance escape probability considered likely to exist in a thermal reactor. The effect upon [gamma] of the the absorption cross section of 91Pa233 and of the fission products has been shown.
Testing of Fuel Element Parts and Assemblies by the Radiographic Method: Concurrently with the production of canned uranium slugs for pile operation there arises the problem of nondestructive testing so that no slug which may fail structurally during operation be placed in the pile. The ultimate goal of any such testing program is to devise nondestructive testing methods which will eliminate defective slugs. A secondary goal of the testing program is to learn as much as possible about the construction of the canned slug so that the mechanisms of failure can be understood. Radiography, an increasingly useful nondestructive test method, offered one possible way of investigating this area.
Preliminary Hazard Summary Report on the Boiling Experiment Reactor (BER): Experiments performed by the Laboratory with the Borax Reactor at the National Reactor Testing Station have demonstrated that a boiling reactor possesses inherent safety characteristics which have not previously been included in the estimation of reactor hazards. Other operating characteristics of Borax were also sufficiently attractive to justify the development of boiling reactors for package power and central station power plant applications. Accordingly, a proposal was made to the Atomic Energy Commission that Argonne design, construct and operate a pilot-scale boiling reactor (BER) as part of the Commission's five year program for development of power reactors. Tentative approval for this project has been granted. The primary objective of the BER is to establish the feasibility of operating a boiling reactor in conjunction with a turbine generator on a scale which can be extrapolated to large sizes. A preliminary evaluation of hazards is hereby submitted for the purpose of determining site requirements for a 20 mw reactor of this type. Because the construction of the reactor would be expedited and its usefulness as an operating experiment greatly enhanced, it is suggested that the reactor should be constructed at the DuPage site of the Laboratory. If the inherent features of safety of the boiling reactor are shown to provide a sufficient reduction in exclusion area to permit construction in a metropolitan areas, a sizeable improvement in the possibility of industrial power will have been made. It is in this sprit that this preliminary evaluation is presented.
Metallurgy Division Quarterly Report January, February, and March 1954: This quarterly report discusses ongoing research and experiments at Oak Ridge National Laboratory in the Metallurgy Division. This report discusses water cooled reactors, liquid metal cooled reactors, reactor development metallurgy, basic metallurgy, applied metallurgy, and aqueous corrosion.
Chemical Engineering Division Summary Report January, February, and March, 1954: Progress is reported on (1) direct cycle boiling reactor studies, (2) solvent extraction, (3) fluoride volatilization separation process, (4) elevated temperature separations, (5) fluidization studies, (6) development of analytical techniques, (7) processing and utilization of radioactive wastes.
Differential Thermal Analysis of Irradiated Diamond and Silicon Carbide: It was demonstrated by differential thermal analysis (DTA) that: 1. Catastrophic amounts of energy can be stored in diamond. 2. Even at low irradiations, the release takes place over serval hundred degrees, indicating a spectrum of activation energies. 3. At higher irradiations, the stored energy release is considerably less than the increased energy contents and seems not to have been completely released even at the highest temperatures reached. 4. There is some indication of an increased heat capacity below the temperature of stored energy release. It was shown by DTA that large amounts of energy can be stored in silicon carbide on irradiation. The release was found to be spread out over a greater range of temperatures than in diamond and indicated a larger and higher group of activation energies. Catastrophic release was not achieved. The amount of stored energy released over the range of temperatures used was 140 cal/g in a sample irradiated in a water-cooled test hole at HEW for an exposure of 265 Mwd/aT.
Soluble Poisons in Reactor Control: Theoretical and experimental investigations of the use of soluble poisons (neutron absorbers) to supplement mechanical control rods are summarized. Experimental evaluation of poisons of interest includes in-pile and out-of-pile tests simulating anticipated reactor operating conditions. Other phases of the investigation included methods of poison injection, removal, and cleanup of poison-diluted reactor systems, as well as studies to evaluate possible application of soluble poison control in existing and proposed reactors.
Metallurgy Division Quarterly Report October, November, and December 1953: This quarterly report discusses ongoing research and experiments at Oak Ridge National Laboratory in the Metallurgy Division. This report discusses water cooled reactors, liquid metal cooled reactors, reactor development metallurgy, basic metallurgy, applied metallurgy, and aqueous corrosion.
Dimensional Stability of Uranium Powder Compacts Upon Thermal Cycling: Thermal cycling tests on uranium have shown that the dimensional changes that occur on cycling in the alpha range are directly related to both the texture of the material and its grain size: cold rolled rods generally elongate in the direction of rolling, while the same rods, after a beta-treatment, grow at rates several orders of magnitude lower. This considerable improvement by beta-treatment has been attributed to the texture randomization accompanying the heat-treatment. In the course of this heat-treatment, however, considerable grain growth occurs, which ahs the effect of causing surface roughening on cycling (also referred to as "bumping"); fine grained material generally retains a smooth surface. These observations led to the speculation that the most desirable structure in uranium, from standpoint of dimensional stability, is one that combines both a random texture and a fine grain size. Heat treatment of rolled rod offered no easy method to obtain such a product; powder metallurgical techniques, however, appeared ideally suited for the purpose. To this end, early in 1949, the Sylvania Electric Products Company initiated a program to develop suitable techniques for producing uranium powder compacts having the above-mentioned desired characteristics. Because of the availability of thermal cycling equipment at Argonne, the Metallurgy Division of the Laboratory has undertaken to evaluate the stability of the various experimental compacts produced in the developmental phases of the program. This report contains the results of these evaluations. The data in this report indicate that compacts of nearly theoretical density and fine grain size can be obtained by hot pressing uranium or uranium hydride powders in the high alpha temperature range.
Chemical Engineering Division Summary Report October, November, and December, 1953: Progress is reported on (1) experimental breeder reactor program, (2) solvent extraction, (3) fluoride volatilization separation process, (4) elevated temperature separations, (5) denitration of uranyl nitrate in a fluidized bed, (6) development of analytical techniques, (7) processing and utilization of radioactive wastes.
Fabrication and Properties of Extruded Silver-Cadmium Control Rods: The production of cross-type control rods having a span of 4-7/8 in., and an arm thickness of 1/8 in., was studied. Extrusion techniques were developed for producing cross-type control rods from each of two alloys; one containing 75% silver-25% cadmium, and the other containing 67% silver-30% cadmium-3% copper. Fabrication of the extruded crosses into clad control rods for the Mark I naval reactor was attempted. A set of unclad control rods for the Zero Power Reactor was produced. The effect of copper, nickel, aluminum, palladium, and indium, singly and in various combinations, on the physical and mechanical properties of silver cadmium was studied. Data are given on the work hardening and annealing of binary silver-cadmium alloys, and on the precipitation hardening of certain complex silver cadmium alloys. A materials specification and suggested fabrication procedure were established for nickel-clad extruded silver-cadmium control rods.
Reactor Engineering Division Quarterly Report September 1, 1953 through November 30, 1953: Report issued by the Argonne National Laboratory covering the quarterly report from the Reactor Engineering Division. A summary of reactor programs, designs, development, and experiments are presented. This report includes tables, illustrations, and photographs.
Preliminary Report on Corrosion of Low-Uranium, Zirconium-Base Alloys: Tests were made to determine the effects of heat treatment and composition on the corrosion resistance of low-uranium, zirconium-base alloys to water at 600F. A total of 57 compositions were tested. The zirconium alloys contained up to 9% natural uranium plus small amounts of tin, antimony, lead, bismuth, yttrium, beryllium, germanium, niobium, nickel, and aluminum in various combinations. Data are presented in both tabular and graphical form. The effect of heat treatment on corrosion resistance of zirconium-uranium-tin alloys is partially masked by impurities in alloys made from sponge or bomb-reduced zirconium. In ternary alloys made from crystal bar zirconium, the effect of heat treatment on corrosion resistance is definite, and varies with the composition of the alloy. The range of ternary compositions from approximately % to 6 weight-per cent uranium and from 2 to4 per cent time, are the most attractive fuel element core alloys.
Factors Which Affect Formation and Deposition of Transport Corrosion Products in High-Temperature Recirculating Water Loops: Deposits of corrosion products form on heat transfer surfaces and in radiation flux zones at temperatures around 500F in stainless steel systems operating with circulating water. The report considers the possible harmful effects of such deposits on heat transfer and fluid flow, as well as factors involved in the origin of these corrosion products and in the mechanisms of deposition. The prevention of deposition by chemical, mechanical, and electrostatic methods is discussed.
Reactivity as a Function of Irradiation Time in Thermal Reactors: Equations governing the variation of U235. U238, Pu239, Pu240, and Pu241 have been derived and their solutions plotted as a function of irradiation time. The initial U235 content of the uranium was varied from 0.5% to 2.0%. The range of conversion ratios was from 0.5 to 1.2. The irradiation was from 0 to 20,000 mwd/ton of fuel. Since a range of initial conversion ratios is associated with each value of enrichment, a solution results in a family of curves for each isotope, and, since the range of enrichments is large, the number of curves is quite large. Translation of the isotope curves to reactivity variation necessitates a calculation requiring a modest amount of time for a particular case but a prohibitive amount of time to cover the entire range of possible combinations of enrichment and initial conversion ratios. Reactivity variation as a function of irradiation time has been computed for a natural uranium reactor with an initial conversion ratio ranging from 0.7 to 1.2 and for 3 types of reactors in which there is a considerable current interest. Similar calculations for other reactors can be made by making use of the isotope curves and the calculation technique set forth in this report.
Roll Cladding of Uranium-Niobium Alloys for Plate Type Fuel Elements: The feasibility of cladding plate type, corrosion resistant uranium-niobium fuel elements with Zircaloy-II by roll bonding has been demonstrated. Plates with cores of uranium alloyed with 3 w/o and 6 w/o Nb intended for irradiation testing in a high temperature water test loop in the MTR have been finished withing specified tolerances. The preparation of cladding billet core and clad components and the assembly of billets by enclosing cores in welded Zircaloy-II jackets can be readily accomplished with conventional fabrication equipment. Some machining operations and billet evacuations, as used in the preparation of most picture frame billet assemblies have been eliminated. Roll bonds were obtained with reductions of 75% to 80% in thickness. Reductions in excess of 90% in thickness, although not necessary for bonding , can be used for economical productions of long plates. Plates can be made with clad to core bond strengths from 30,000 psi to 60,000 psi. Properly heat treated plates have sufficient ductility to allow cold finishing by rolling, forming, bending, or twisting, with reductions of 20% to 30%. Edge bonds of Zircaloy to Zircaloy have been obtained which were corrosion resistant to 260 C water. End seals which were also corrosion resistant to water at this temperature have been made by shielded arc welding inserts to the clad.
Atomic Energy Commission Division of Reactor Development Reactor Information Meeting. Part VI, Processing; October 7, 8, 9, 1953: On October 7, 8, and 9, 1953, the Atomic Energy Commission Division of Reactor Development held a reactor information meeting at the Argonne National Laboratory. The objective of the meeting was exchange of information among people actively concerned with the design of reactors for power to the end that the power reactor program would move more speedily and more economically to another milestone of success. In this volume all the papers presented at the meeting are listed. Copies are given of those papers which are available, and references to published reports are indicated where know for those papers not included in this collections. In order to facilitate handling, this volume is being issued in six parts: Part I Power Reactors; Part II Reactor Physics. Critical and Exponential Experiments Measurements; Part III Reactor Components. Reactor Economics Considerations. Reactor Safeguard and Control; Part IV Fuel Element Design and Problems. Corrosion and Chemistry; Part V Heat Transfer; Part VI Processing. The Author Index is being bound and distributed with Part I of this volume.
Physics Division Supplement to Quarterly Report September, October, and November, 1953: This technical report describes experimental nuclear physics, mass spectroscopy, crystallography, experimental reactor physics, theoretical physics (general), reactor theory and electronic digital computers.
Eddy Current and Ultrasonic Testing of CP-6 Fuel Elements: The fuel element to be used in the Savannah River reactors is a natural uranium slug 1.00 in. in diameter and 8 in. long, encased in a 2S aluminum can 1.080 in. O.D. having a wall thickness of 0.035 in. The slug is bonded to the can with an aluminum silicon alloy, using the Hanford Al-Si process.
Metallurgy Division Quarterly Report July, August, and September 1953: This quarterly report discusses ongoing research and experiments at Oak Ridge National Laboratory in the Metallurgy Division. This report discusses water cooled reactors, liquid metal cooled reactors, reactor development metallurgy, basic metallurgy, applied metallurgy, and aqueous corrosion,
Corrosion and Stability Tests on Chemical Poisons in Higher-Temperature Water: Corrosion-stability tests have been made in static autoclaves at 500 and 600F on solutions of compounds having high neutron cross sections to evaluate their usefulness for shutdown purposes. The only compound tested which appeared to be completely stable in 600F water was boric acid. Limited corrosion data did not show it to cause excessive corrosion of zirconium or stainless steel.
Physics Division Supplement to Quarterly Report June, July, and August, 1953: This technical report describes experimental nuclear physics, mass spectroscopy, crystallography, experimental reactor physics, theoretical physics (general), reactor theory, electronic digital computers, and applied mathematics and computations (general).
Reactor Engineering Division Quarterly Report June 1, 1953 through August 31, 1953: Report issued by the Argonne National Laboratory covering the quarterly report from the Reactor Engineering Division. A summary of reactor programs (including the Power Breeder Reactor (PBR) and the Central Station Water Reactor (CSWR)), designs, development, and experiments are presented. This report includes tables, illustrations, and photographs.
Comparative Analysis of ANL High Purity Uranium: In the course of the development at Argonne of high purity uranium metal in ingot form, some questions arose as to the validity of the chemical analyses of some of the impurities (particularly those for carbon, boron, and silicon), with one analytical laboratory reporting concentrations in some instances of an order of magnitude greater than another laboratory. Since the low concentrations of impurities in this material involved, in some cases, the development of modified analytical procedures and standards, it was decided to check these discrepancies by having identically prepared samples analyzed by several AEC and associated laboratories. This report is a compilation of the results obtained.
The Manufacture of Internal Blanket and Fuel Blanket Slugs for the Experimental Breeder Reactor: Surrounding the core of the Experimental Breeder Reactor (EBR) is located the Internal Blanket (see Figure 2 of Reference 1). This blanket is compromised of natural uranium rods jacketed in stainless steel. The active portion of each rod is made up of five natural uranium slugs 0.873" diameter x 4.050" long. The slugs, stacked one of top of another, are held together and protected by a drawn-on stainless steel tube with welded and closures. These internal blanket rods are located inside the external blanket the manufacture of which has been described previously.
The Development of Equipment and Methods for Centrifugally Casting Reactor Fuel Slugs: This technical report describes the design and construction of equipment and the development of methods for multiple mold, centrifugal casting of reactor fuel slugs. Advantages of the centrifugal casting method over the conventional fabrication methods were found to be (1) fewer operations, (2) fewer and more easily recovered residues, (3) less expensive equipment, and (4) the production of fuel slugs in shapes and in alloys not well adapted to other methods of manufacture. The method consisted of vacuum melting the alloy in stoppered crucibles and bottom pouring into a spinning rotor carrying 16 radially arranged copper molds. The castings so produced were used without further processing, except for cropping the sprue end to obtain the specified length.
Development of a Process to Produce Zirconium Hanford Type Process Tubing by Roll Forming And Inert Arc Welding: The development of methods which were successful in producing zirconium Hanford type process tubing by roll forming and inert are welding (He) flat strip to which appropriate rails had ben previously attached by resistance welding is described in this report. Grade 2 drip arc melted crystal bar material was used.
Preferred Orientation in 300 C Rolled and in Recrystallized Uranium Sheet: The rolling and recrystallization textures in 300 C rolled uranium sheet were investigated using a Geiger counter diffractometer with the modified Schulz reflection technique. Seven sections of sheet material were used in order to obtain sufficient data for quantitative pole figures by the reflection technique. A special integrating specimen table was used for obtaining and recording the data atomically.

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