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D-Zero Signal Board Feed-Thru, Instrumentation and Hi-Voltage Boxes

Description: The three boxes being reviewed all operate at a pressure of less than 15 psig. Since they are relieved at 13 psig, they fall outside the scopes of the ASME Pressure Vessel Code, Fermilab Engineering Standard SD-37B, and Chapter 5031 of the Fermilab Safety Manual, therefore a Pressure Vessel Engineering Note showing compliance with SD-37B is not required. In calculating the design stresses, only the largest of the three boxes, the signal board feed-thru box, was analyzed. This box had the largest spans and areas and would experience the largest pressure-related forces. The thinnest walls of each box were found to be in the top plates and they were also the side of the box which exposed the largest amount of area to internal pressure. The signal board feed-thru box top plate had at least twice the pressure area than either the instrumentation or hi-voltage boxes' top plates. This large disparity overshadows the slight difference in top plate thicknesses between the three boxes (0.56-inch vs. 0.25-inch and 0.3125-inch, respectively). Therefore, we felt the analysis of the larger signal board feedthru box would justify the design of the smaller instrumentation and hi-voltage boxes. Appended to the end of this engineering note are the weld procedure, assembly report and the pressure test procedure & results for the signal feed-thru box. Also, included as a reference is a list of the drawing numbers for the parts and assembly of the signal board feed-thru, instrumentation and hi-voltage boxes.
Date: February 14, 1990
Creator: Luther, R.

Zinc(II) oxide solubility and phase behavior in aqueous sodium phosphate solutions at elevated temperatures

Description: A platinum-lined, flowing autoclave facility is used to investigate the solubility/phase behavior of zinc(II) oxide in aqueous sodium phosphate solutions at temperatures between 290 and 560 K. ZnO solubilities are observed to increase continuously with temperature and phosphate concentration. At higher phosphate concentrations, a solid phase transformation to NaZnPO{sub 4} is observed. NaZnPO{sub 4} solubilities are retrograde with temperature. The measured solubility behavior is examined via a Zn(II) ion hydrolysis/complexing model and thermodynamic functions for the hydrolysis/complexing reaction equilibria are obtained from a least-squares analysis of the data. The existence of two new zinc(II) ion complexes is reported for the first time: Zn(OH){sub 2}(HPO{sub 4}){sup 2{minus}} and Zn(OH){sub 3}(H{sub 2}PO{sub 4}){sup 2{minus}}. A summary of thermochemical properties for species in the systems ZnO-H{sub 2}O and ZnO-Na{sub 2}O-P{sub 2}O{sub 5}-H{sub 2}O is also provided. 21 refs., 10 figs., 7 tabs.
Date: February 1, 1990
Creator: Ziemniak, S.E.; Jones, M.E. & Combs, K.E.S.

Zr and Mo isotopes in single presolar graphite grains : a record of stellar nucleosynthesis.

Description: Thirty-two individual graphite grains from the Murchison meteorite were analyzed for their Mo and/or Zr isotopic compositions by laser ablation resonant ionization mass spectrometry. {sup 96}Zr/{sup 94}Zr ratios range from 0.074 times to 10 times the solar value. Five grains have depletions in {sup 96}Zr, suggestive of the s-process, and two grains have extraordinary enrichments in {sup 96}Zr, suggestive of the r-process. Most graphite grains have close-to-terrestrial Mo isotopic imposition, but five have s-process Mo nucleosynthesis signatures.
Date: February 10, 1998
Creator: Nicolussi, G. K.