Final Report - Management of High Sulfur HLW, VSL-13R2920-1, Rev. 0, dated 10/31/2013

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The present report describes results from a series of small-scale crucible tests to determine the extent of corrosion associated with sulfur containing HLW glasses and to develop a glass composition for a sulfur-rich HLW waste stream, which was then subjected to small-scale melter testing to determine the maximum acceptable sulfate loadings. In the present work, a new glass formulation was developed and tested for a projected Hanford HLW composition with sulfate concentrations high enough to limit waste loading. Testing was then performed on the DM10 melter system at successively higher waste loadings to determine the maximum waste loading without the ... continued below

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Kruger, Albert A.; Gan, H.; Pegg, I. L.; Feng, Z.; Gan, H,; Joseph, I. et al. November 13, 2013.

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  • Hanford Site (Wash.)
    Publisher Info: HNF (Hanford Site (HNF), Richland, WA (United States))
    Place of Publication: Richland, Washington

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Description

The present report describes results from a series of small-scale crucible tests to determine the extent of corrosion associated with sulfur containing HLW glasses and to develop a glass composition for a sulfur-rich HLW waste stream, which was then subjected to small-scale melter testing to determine the maximum acceptable sulfate loadings. In the present work, a new glass formulation was developed and tested for a projected Hanford HLW composition with sulfate concentrations high enough to limit waste loading. Testing was then performed on the DM10 melter system at successively higher waste loadings to determine the maximum waste loading without the formation of a separate sulfate salt phase. Small scale corrosion testing was also conducted using the glass developed in the present work, the glass developed in the initial phase of this work [26], and a high iron composition, all at maximum sulfur concentrations determined from melter testing, in order to assess the extent of Inconel 690 and MA758 corrosion at elevated sulfate contents.

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  • Report No.: ORP-56310 Rev 0
  • Grant Number: DE-AC27-08RV14800
  • DOI: 10.2172/1105983 | External Link
  • Office of Scientific & Technical Information Report Number: 1105983
  • Archival Resource Key: ark:/67531/metadc869529

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  • November 13, 2013

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  • Sept. 16, 2016, 12:32 a.m.

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  • Nov. 1, 2016, 10:54 a.m.

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Kruger, Albert A.; Gan, H.; Pegg, I. L.; Feng, Z.; Gan, H,; Joseph, I. et al. Final Report - Management of High Sulfur HLW, VSL-13R2920-1, Rev. 0, dated 10/31/2013, report, November 13, 2013; Richland, Washington. (digital.library.unt.edu/ark:/67531/metadc869529/: accessed September 23, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.