Characteristics of STP Pre-2004 Archived KE Basin Sludge Samples Before and After Re-Jarring in the RPL - April 2012

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This report describes results of work performed in the Shielded Analytical Laboratory (SAL) at the Pacific Northwest National Laboratory’s (PNNL) Radiochemical Processing Laboratory (RPL) with archive K East (KE) Basin sludge samples obtained before the year 2004, with some of them composited and initially characterized five years ago (Delegard et al. 2011). The previously performed testing included the physical properties determinations for selected samples (settled and particle densities, water and solids concentrations), the pH, as well as identification of crystalline phases by X-ray diffractometry (XRD) for selected samples. Another objective of the previous characterization and testing campaign was to transfer ... continued below

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Sinkov, Sergey I.; Delegard, Calvin H.; Schmidt, Andrew J. & Chenault, Jeffrey W. September 28, 2012.

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Description

This report describes results of work performed in the Shielded Analytical Laboratory (SAL) at the Pacific Northwest National Laboratory’s (PNNL) Radiochemical Processing Laboratory (RPL) with archive K East (KE) Basin sludge samples obtained before the year 2004, with some of them composited and initially characterized five years ago (Delegard et al. 2011). The previously performed testing included the physical properties determinations for selected samples (settled and particle densities, water and solids concentrations), the pH, as well as identification of crystalline phases by X-ray diffractometry (XRD) for selected samples. Another objective of the previous characterization and testing campaign was to transfer some sludge composites and individual samples into new storage containers to overcome the embrittlement effect which develops in original glass containers as a result of extended exposure to high radiation fields and which increases probability of sample loss.

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  • Report No.: PNNL-21836
  • Grant Number: AC05-76RL01830
  • DOI: 10.2172/1086422 | External Link
  • Office of Scientific & Technical Information Report Number: 1086422
  • Archival Resource Key: ark:/67531/metadc840290

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  • September 28, 2012

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  • May 19, 2016, 9:45 a.m.

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  • Nov. 22, 2016, 10:13 p.m.

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Sinkov, Sergey I.; Delegard, Calvin H.; Schmidt, Andrew J. & Chenault, Jeffrey W. Characteristics of STP Pre-2004 Archived KE Basin Sludge Samples Before and After Re-Jarring in the RPL - April 2012, report, September 28, 2012; Richland, Washington. (digital.library.unt.edu/ark:/67531/metadc840290/: accessed August 20, 2017), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.