Analytical Method for Measuring Total Protium and Total Deuterium in a Gas Mixture Containing H2, D2, and HD Via Gas Chromatography

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A new analytical technique has been developed that measures both total protium (H) and deuterium (D) in a gas mixture containing H2, D2, and HD. This new analytical technique uses a micro gas chromatograph (GC) with two molecular sieve columns. One column uses D2 as the carrier gas and the other uses H2 as the carrier gas. Laboratory tests have shown that when used in this configuration the GC can measure both total protium and total deuterium, each with a sensitivity of less than 20 ppm. This new analytical technique was developed as a result of a request to provide ... continued below

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SESSIONS, HENRY March 24, 2004.

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A new analytical technique has been developed that measures both total protium (H) and deuterium (D) in a gas mixture containing H2, D2, and HD. This new analytical technique uses a micro gas chromatograph (GC) with two molecular sieve columns. One column uses D2 as the carrier gas and the other uses H2 as the carrier gas. Laboratory tests have shown that when used in this configuration the GC can measure both total protium and total deuterium, each with a sensitivity of less than 20 ppm. This new analytical technique was developed as a result of a request to provide instrumentation to measure the protium and deuterium concentrations at several process points during initial testing of the new hydrogen tritium thermal cycling absorption process columns.

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  • Other Information: PBD: 24 Mar 2004

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  • Report No.: WSRC-TR-2004-00084
  • Grant Number: AC09-96SR18500
  • DOI: 10.2172/822364 | External Link
  • Office of Scientific & Technical Information Report Number: 822364
  • Archival Resource Key: ark:/67531/metadc785634

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Office of Scientific & Technical Information Technical Reports

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  • March 24, 2004

Added to The UNT Digital Library

  • Dec. 3, 2015, 9:30 a.m.

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  • May 4, 2016, 9:22 p.m.

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SESSIONS, HENRY. Analytical Method for Measuring Total Protium and Total Deuterium in a Gas Mixture Containing H2, D2, and HD Via Gas Chromatography, report, March 24, 2004; South Carolina. (digital.library.unt.edu/ark:/67531/metadc785634/: accessed October 16, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.