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PREPARATION AND CHARACTERIZATION OF NANOSTRUCTURED GRANULAR SUPPORT PARTICLES AND CATALYTIC MATERIALS

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We have set up successfully two experimental systems during the past time of the project. The first system is sol-gel chemical method for preparing {gamma}-Al{sub 2}O{sub 3}, SiO{sub 2}, Cr{sub 2}O{sub 3} granular support particles. The second system is the laser-induced solution deposition (LISD) technique for nanoparticle catalysts containing Fe/Cu, and Co/Cu on the granular support. We have successfully deposited {gamma}-Al{sub 2}O{sub 3}, SiO{sub 2}, Cr{sub 2}O{sub 3} granular support particles by sol-gel method and Co and CoO nanoparticles by LISD novel fabrication technique. The characterization methods we have used include scanning electron microscope (SEM), high-resolution transmission electron microscope (HRTEM) … continued below

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19 pages

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Zhong, Zhenchen January 15, 2002.

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This report is part of the collection entitled: Office of Scientific & Technical Information Technical Reports and was provided by the UNT Libraries Government Documents Department to the UNT Digital Library, a digital repository hosted by the UNT Libraries. It has been viewed 13 times. More information about this report can be viewed below.

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Description

We have set up successfully two experimental systems during the past time of the project. The first system is sol-gel chemical method for preparing {gamma}-Al{sub 2}O{sub 3}, SiO{sub 2}, Cr{sub 2}O{sub 3} granular support particles. The second system is the laser-induced solution deposition (LISD) technique for nanoparticle catalysts containing Fe/Cu, and Co/Cu on the granular support. We have successfully deposited {gamma}-Al{sub 2}O{sub 3}, SiO{sub 2}, Cr{sub 2}O{sub 3} granular support particles by sol-gel method and Co and CoO nanoparticles by LISD novel fabrication technique. The characterization methods we have used include scanning electron microscope (SEM), high-resolution transmission electron microscope (HRTEM) and X-Ray diffraction (XRD). The research toward to the proposed direction is in good progress. We have given three presentations in national and local materials meetings and have submitted another two papers in another two key national meetings in nanotechnology and American Physical Annual March Meeting 2002. A couple of papers are in preparation.

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19 pages

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OSTI as DE00792321

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  • Other Information: PBD: 15 Jan 2002

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  • January 15, 2002

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  • Oct. 19, 2015, 7:39 p.m.

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  • March 25, 2016, 2:21 p.m.

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Zhong, Zhenchen. PREPARATION AND CHARACTERIZATION OF NANOSTRUCTURED GRANULAR SUPPORT PARTICLES AND CATALYTIC MATERIALS, report, January 15, 2002; Pittsburgh, Pennsylvania. (https://digital.library.unt.edu/ark:/67531/metadc742648/: accessed April 18, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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