Sulfur Partitioning During Vitrification of INEEL Sodium Bearing Waste: Status Report

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Description

The sodium bearing tank waste (SBW) at Idaho National Engineering and Environmental Laboratory (INEEL) contains high concentrations of sulfur (roughly 5 mass% of SO3 on a nonvolatile oxide basis). The amount of sulfur that can be feed to the melter will ultimately determine the loading of SBW in glass produced by the baseline (low-temperature, joule-heated, liquid-fed, ceramic-lined) melter. The amount of sulfur which can be fed to the melter is determined by several major factors including: the tolerance of the melter for an immiscible salt layer accumulation, the solubility of sulfur in the glass melt, the fraction of sulfur removed ... continued below

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Darab, John G.; Macisaac, Brett D.; Russell, Renee L.; Smith, Harry D. & Vienna, John D. July 31, 2001.

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Description

The sodium bearing tank waste (SBW) at Idaho National Engineering and Environmental Laboratory (INEEL) contains high concentrations of sulfur (roughly 5 mass% of SO3 on a nonvolatile oxide basis). The amount of sulfur that can be feed to the melter will ultimately determine the loading of SBW in glass produced by the baseline (low-temperature, joule-heated, liquid-fed, ceramic-lined) melter. The amount of sulfur which can be fed to the melter is determined by several major factors including: the tolerance of the melter for an immiscible salt layer accumulation, the solubility of sulfur in the glass melt, the fraction of sulfur removed to the off-gas, and the incorporation of sulfur into the glass up to it?s solubility limit. This report summarizes the current status of testing aimed at determining the impacts of key chemical and physical parameters on the partitioning of sulfur between the glass, a molten salt, and the off-gas.

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  • Other Information: PBD: 31 Jul 2001

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  • Report No.: PNNL-13588
  • Report No.: EW4010000
  • Grant Number: AC06-76RLO1830
  • DOI: 10.2172/786800 | External Link
  • Office of Scientific & Technical Information Report Number: 786800
  • Archival Resource Key: ark:/67531/metadc723302

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Creation Date

  • July 31, 2001

Added to The UNT Digital Library

  • Sept. 29, 2015, 5:31 a.m.

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  • April 7, 2016, 2:13 p.m.

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Darab, John G.; Macisaac, Brett D.; Russell, Renee L.; Smith, Harry D. & Vienna, John D. Sulfur Partitioning During Vitrification of INEEL Sodium Bearing Waste: Status Report, report, July 31, 2001; Richland, Washington. (digital.library.unt.edu/ark:/67531/metadc723302/: accessed November 21, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.