PROMOTED ZINC CHROMITE CATALYSTS FOR HIGHER ALCOHOL SYNTHESIS

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Description

Work during the report period was concentrated on developing analytical techniques. Thin-layer chromatography (TLC) was used in an attempt to define the best mobile phase to separate the components of ''spent'' tetrahydroquinoline by liquid chromatography in a silica gel column. Conditions have been defined for separating the light gases produced by the reaction of carbon monoxide (CO) and hydrogen (H{sub 2}) over promoted ''zinc chromite'' catalysts. This will be done with a temperature-programmed Carboxen-1000 column, using a thermal conductivity detector for analysis. A Petrocol DM 150 capillary column will be purchased to separate the heavier products, which will be analyzed ... continued below

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15 pages

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Sun, Ms. Xiaolei & Roberts, Professor George W. June 21, 2000.

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Description

Work during the report period was concentrated on developing analytical techniques. Thin-layer chromatography (TLC) was used in an attempt to define the best mobile phase to separate the components of ''spent'' tetrahydroquinoline by liquid chromatography in a silica gel column. Conditions have been defined for separating the light gases produced by the reaction of carbon monoxide (CO) and hydrogen (H{sub 2}) over promoted ''zinc chromite'' catalysts. This will be done with a temperature-programmed Carboxen-1000 column, using a thermal conductivity detector for analysis. A Petrocol DM 150 capillary column will be purchased to separate the heavier products, which will be analyzed using a flame ionization detector.

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15 pages

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OSTI as DE00781794

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  • Other Information: PBD: 21 Jun 2000

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  • Report No.: DE--FG26-97FT97262--03
  • Grant Number: FG26-97FT97262
  • DOI: 10.2172/781794 | External Link
  • Office of Scientific & Technical Information Report Number: 781794
  • Archival Resource Key: ark:/67531/metadc723118

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  • June 21, 2000

Added to The UNT Digital Library

  • Sept. 29, 2015, 5:31 a.m.

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  • April 15, 2016, 1:26 p.m.

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Sun, Ms. Xiaolei & Roberts, Professor George W. PROMOTED ZINC CHROMITE CATALYSTS FOR HIGHER ALCOHOL SYNTHESIS, report, June 21, 2000; Morgantown, West Virginia. (digital.library.unt.edu/ark:/67531/metadc723118/: accessed May 24, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.