Structural Diversity in Lithium Aryloxides, Part 1. Structurally Characterized [Li(OAr)(THF){sub x}]{sub n} where OAr = OC{sub 6}H{sub 5}, OC{sub 6}H{sub 4}(2-Me), OC{sub 6}H{sub 3}(2,6-Me){sub 2}, OC{sub 6}H{sub 4}(2-Pr{sup i}), OC{sub 6}H{sub 3}(2,6-Pr{sup i}){sub 2}, OC{sub 6}H{sub 4}(2-Bu{sup t}), OC{sub 6}H{sub 3}(2,6-Bu{sup t}){sub 2} Page: 50 of 120
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S7
Table S1.4. Anisotropic displacement parameters (A^2 x 10^3) for 1.
The anisotropic displacement factor exponent takes the form:
-2 pi^2 ( h^2 a*^2 Ull + ... + 2 h k a* b* U12 ]
Ull U22 U33 U23 U13 U12
Li(1) 40(2) 64(3) 43(2) 0(2) 21(2) -3(2)
Li(2) 42(2) 58(3) 37(2) 1(2) 18(2) 5(2)
C(1) 45(1) 39(1) 37(1) 0(1) 22(1) 0(1)
C(2) 42(1) 43(1) 44(1) -3(1) 19(1) -2(1)
C(3) 56(2) 45(2) 47(2) 1(1) 7(1) -1(1)
C(4) 98(3) 59(2) 42(2) -6(1) 29(2) 4(2)
C(5) 97(2) 82(2) 55(2) -2(2) 52(2) 12(2)
C(6) 57(2) 73(2) 50(2) -3(1) 33(1) 5(1)
C(7) 38(1) 37(1) 38 (1) -1(1) 22(1) -2(1)
C(8) 48(2) 61(2) 40(1) -7(1) 25(1) -2(1)
C(9) 60(2) 66(2) 64(2) -12(1) 45(2) -4(1)
C(10) 48(2) 61(2) 77(2) -2(1) 39(2) 6(1)
C(11) 39(2) 64(2) 50(2) 5(1) 18(1) 5(1)
C(12) 45(1) 48(2) 36(1) 0(1) 21(1) 2(1)
C(13) 94(2) 66(2) 43(2) 8(1) 38(2) 18(2)
C(14) 79(2) 81(2) 60(2) 13(2) 30(2) 18(2)
C(15) 127(3) 60(2) 82(2) 18 (2) 56(2) 36(2)
C(16) 98(2) 49(2) 64(2) -7(1) 48(2) -5(2)
C(17) 64(2) 66(2) 101(2) -16(2) 57(2) -10(2)
C(18) 65(2) 78(2) 132(3) -24(2) 36(2) -16(2)
C(19) 165 (4) 79(3) 137 (3) -50 (2) 113 (3) -48 (3)
C(20) 116(3) 48(2) 169(4) 2(2) 109(3) 4(2)
0(1) 42(1) 62(1) 34(1) -7(1) 19(1) -2(1)
O(2) 38(1) 61(1) 39(1) -1(1) 20(1) 5(1)
0(3) 69(1) 55(1) 39(1) 5(1) 28(1) 13(1)
0(4) 48(1) 60(1) 78(1) -9(1) 37(1) -6(1)
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Boyle,Timothy J.; Pedrotty, Dawn M.; Alam,Todd M.; Vick,Sara C. & Rodriguez, Mark A. Structural Diversity in Lithium Aryloxides, Part 1. Structurally Characterized [Li(OAr)(THF){sub x}]{sub n} where OAr = OC{sub 6}H{sub 5}, OC{sub 6}H{sub 4}(2-Me), OC{sub 6}H{sub 3}(2,6-Me){sub 2}, OC{sub 6}H{sub 4}(2-Pr{sup i}), OC{sub 6}H{sub 3}(2,6-Pr{sup i}){sub 2}, OC{sub 6}H{sub 4}(2-Bu{sup t}), OC{sub 6}H{sub 3}(2,6-Bu{sup t}){sub 2}, article, June 12, 2000; Albuquerque, New Mexico. (https://digital.library.unt.edu/ark:/67531/metadc711673/m1/50/: accessed April 24, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.