Synthesis of model compounds for coal liquefaction research: Final report, June 21, 1990--July 30, 1993

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Description

The objectives of this project were to develop feasible synthetic routes to produce (1) 4(4{prime}-hydroxy-5{prime}6{prime},7{prime}8{prime}-tetrahydro-1{prime}-naphthylmethyl)-6-methyldibenzothiophene, and (2) a 1-hydroxynaphthalene-dibenzothiophene polymer. These compounds are thought to be representative of sulfur containing molecules in coal. The program was divided into two technical tasks. Unfortunately, the attempted syntheses of these compounds was unsuccessful due to their unusual reactivities. Attempted synthetic routes and possible future routes are described, and Appendix A lists the compounds that were synthesized during this program.

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12 p.

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Hirschon, A.S.; Asaro, M. & Bottaro, J. July 1, 1993.

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Description

The objectives of this project were to develop feasible synthetic routes to produce (1) 4(4{prime}-hydroxy-5{prime}6{prime},7{prime}8{prime}-tetrahydro-1{prime}-naphthylmethyl)-6-methyldibenzothiophene, and (2) a 1-hydroxynaphthalene-dibenzothiophene polymer. These compounds are thought to be representative of sulfur containing molecules in coal. The program was divided into two technical tasks. Unfortunately, the attempted syntheses of these compounds was unsuccessful due to their unusual reactivities. Attempted synthetic routes and possible future routes are described, and Appendix A lists the compounds that were synthesized during this program.

Physical Description

12 p.

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OSTI as DE95011469

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  • Other Information: PBD: Jul 1993

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  • Other: DE95011469
  • Report No.: DOE/PC/90036--T7
  • Grant Number: AC22-90PC90036
  • DOI: 10.2172/61099 | External Link
  • Office of Scientific & Technical Information Report Number: 61099
  • Archival Resource Key: ark:/67531/metadc691621

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  • July 1, 1993

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  • Aug. 14, 2015, 8:43 a.m.

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  • Nov. 25, 2015, 4:37 p.m.

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Hirschon, A.S.; Asaro, M. & Bottaro, J. Synthesis of model compounds for coal liquefaction research: Final report, June 21, 1990--July 30, 1993, report, July 1, 1993; United States. (digital.library.unt.edu/ark:/67531/metadc691621/: accessed September 23, 2017), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.