222-S Analytical services final results for Tank 241-U-101, grab samples 1U-96-1 through 1U-96-4

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This document is the final, format IV, laboratory report for characterization of tank 241-U-101 (U-101) grab samples from risers 1 and 7. It transmits additional analytical data for specific gravity (Sp.G.), and all raw analytical data which were not provided in the 45-day report. The 45-day report is attached to this final report as Part II. Secondary analyses were not performed on any of the U-101 samples. This is because none of the primary analyte limits, which trigger the performance of secondary analyses, were exceeded. Grab samples were taken on May 29, 1996 and May 30, 1996 from risers 1 ... continued below

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185 p.

Creation Information

Miller, G. L. August 23, 1996.

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This report is part of the collection entitled: Office of Scientific & Technical Information Technical Reports and was provided by UNT Libraries Government Documents Department to Digital Library, a digital repository hosted by the UNT Libraries. More information about this report can be viewed below.

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  • Westinghouse Hanford Company
    Publisher Info: Westinghouse Hanford Co., Richland, WA (United States)
    Place of Publication: Richland, Washington

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Description

This document is the final, format IV, laboratory report for characterization of tank 241-U-101 (U-101) grab samples from risers 1 and 7. It transmits additional analytical data for specific gravity (Sp.G.), and all raw analytical data which were not provided in the 45-day report. The 45-day report is attached to this final report as Part II. Secondary analyses were not performed on any of the U-101 samples. This is because none of the primary analyte limits, which trigger the performance of secondary analyses, were exceeded. Grab samples were taken on May 29, 1996 and May 30, 1996 from risers 1 and 7, respectively, and were received at the 222-S Laboratory on the same days that they were collected. Analyses were performed in accordance with the Tank Sampling and Analysis Plan (TSAP) for this tank and the Safety Screening Data Quality Objective (DQO). The samples were analyzed for differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), total alpha activity (AT), visual appearance, bulk density, and specific gravity. A sample data summary table, includes sample analytical data accompanied by quality control data (for example, duplicate, spike, blank and standard results and detection limits and counting efforts). The table includes data for DSC, TGA, AT, bulk density, volume percent solids and Sp.G. analyses. Data regarding the visual appearance of samples, volume percent solids and density of the solids are provided in tabular form of the 45-day report (attached as Part II). The table of the 45-day report also associates the original customer sample number with corresponding laboratory sample numbers. The TSAP specified notification limits for only DSC and total alpha. Notification limits were not exceeded for DSC or total alpha analyses for any of the samples, consequently immediate notifications were not necessary and were not made.

Physical Description

185 p.

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OSTI as DE98058190

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  • Other Information: PBD: 23 Aug 1996

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  • Other: DE98058190
  • Report No.: WHC-SD-WM-DP--190-Rev.1
  • Grant Number: AC06-96RL13200
  • DOI: 10.2172/325632 | External Link
  • Office of Scientific & Technical Information Report Number: 325632
  • Archival Resource Key: ark:/67531/metadc674164

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Office of Scientific & Technical Information Technical Reports

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  • August 23, 1996

Added to The UNT Digital Library

  • July 25, 2015, 2:20 a.m.

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  • June 13, 2016, 6:24 p.m.

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Miller, G. L. 222-S Analytical services final results for Tank 241-U-101, grab samples 1U-96-1 through 1U-96-4, report, August 23, 1996; Richland, Washington. (digital.library.unt.edu/ark:/67531/metadc674164/: accessed April 22, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.