Experimental issues in in-situ synchrotron x-ray diffraction at high pressure and temperature by using a laser-heated diamond-anvil cell

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An integrated technique of diamond-anvil cell, laser-heating and synchrotron x-ray diffraction technologies is capable of structural investigation of condensed matter in an extended region of high pressures and temperatures above 100 GPa and 3000 K. The feasibility of this technique to obtain reliable data, however, strongly depends on several experimental issues, including optical and x-ray setups, thermal gradients, pressure homogeneity, preferred orientation, and chemical reaction. In this paper, we discuss about these experimental issues together with future perspectives of this technique for obtaining accurate data.

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15 pages; Other: FDE: PDF

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Yoo, C.S. December 1, 1997.

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Description

An integrated technique of diamond-anvil cell, laser-heating and synchrotron x-ray diffraction technologies is capable of structural investigation of condensed matter in an extended region of high pressures and temperatures above 100 GPa and 3000 K. The feasibility of this technique to obtain reliable data, however, strongly depends on several experimental issues, including optical and x-ray setups, thermal gradients, pressure homogeneity, preferred orientation, and chemical reaction. In this paper, we discuss about these experimental issues together with future perspectives of this technique for obtaining accurate data.

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15 pages; Other: FDE: PDF

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INIS; OSTI as DE00016595

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  • Conference title not supplied, Conference location not supplied, Conference dates not supplied; Other Information: Supercedes report DE98054340; PBD: 1 Dec 1997

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  • Other: DE98054340
  • Report No.: UCRL-JC--129176
  • Report No.: CONF-971201--
  • Grant Number: W-7405-Eng-48
  • Office of Scientific & Technical Information Report Number: 16595
  • Archival Resource Key: ark:/67531/metadc627891

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Office of Scientific & Technical Information Technical Reports

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  • December 1, 1997

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  • June 16, 2015, 7:43 a.m.

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  • Feb. 16, 2016, 7:05 p.m.

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Yoo, C.S. Experimental issues in in-situ synchrotron x-ray diffraction at high pressure and temperature by using a laser-heated diamond-anvil cell, article, December 1, 1997; California. (digital.library.unt.edu/ark:/67531/metadc627891/: accessed September 18, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.