A characterization and evaluation of coal liquefaction process streams. Quarterly technical progress report, October 1--December 31, 1994

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The objectives of this project are to support the DOE direct coal liquefaction process development program and to improve the useful application of analytical chemistry to direct coal liquefaction process development. Independent analyses by well-established methods will be obtained of samples produced in direct coal liquefaction processes under evaluation by DOE. Additionally, analytical instruments and techniques which are currently underutilized for the purpose of examining coal-derived samples will be evaluated. The data obtained from this study will be used to help guide current process development and to develop an improved data base on coal and coal liquids properties. A sample ... continued below

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94 p.

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Robbins, G.A.; Brandes, S.D.; Winschel, R.A. & Burke, F.P. May 1, 1995.

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Description

The objectives of this project are to support the DOE direct coal liquefaction process development program and to improve the useful application of analytical chemistry to direct coal liquefaction process development. Independent analyses by well-established methods will be obtained of samples produced in direct coal liquefaction processes under evaluation by DOE. Additionally, analytical instruments and techniques which are currently underutilized for the purpose of examining coal-derived samples will be evaluated. The data obtained from this study will be used to help guide current process development and to develop an improved data base on coal and coal liquids properties. A sample bank will be established and maintained for use in this project and will be available for use by other researchers. The reactivity of the non-distillable resids toward hydrocracking at liquefaction conditions (i.e., resid reactivity) will be examined. From the literature and data experimentally obtained, a mathematical kinetic model of resid conversion will be constructed. It is anticipated that such a model will provide insights useful for improving process performance and thus the economics of direct coal liquefaction. During this quarter, analyses were completed on 65 process samples from representative periods of HRI Run POC-2 in which coal, coal/plastics, and coal/rubber were the feedstocks. A sample of the oil phase of the oil/water separator from HRI Run POC-1 was analyzed to determine the types and concentrations of phenolic compounds. Chemical analyses and microautoclave tests were performed to monitor the oxidation and measure the reactivity of the standard coal (Old Ben Mine No. 1) which has been used for the last six years to determine solvent quality of process oils analyzed in this and previous DOE contracts.

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94 p.

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OSTI as DE95016266

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  • Other Information: PBD: May 1995

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  • Other: DE95016266
  • Report No.: DOE/PC/93054--10
  • Grant Number: AC22-94PC93054
  • DOI: 10.2172/102462 | External Link
  • Office of Scientific & Technical Information Report Number: 102462
  • Archival Resource Key: ark:/67531/metadc622328

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  • May 1, 1995

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  • June 16, 2015, 7:43 a.m.

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  • Dec. 4, 2015, 10:36 p.m.

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Thumbnail image of item number 1 in: 'A characterization and evaluation of coal liquefaction process streams. Quarterly technical progress report, October 1--December 31, 1994'.
Thumbnail image of item number 2 in: 'A characterization and evaluation of coal liquefaction process streams. Quarterly technical progress report, October 1--December 31, 1994'.
Thumbnail image of item number 3 in: 'A characterization and evaluation of coal liquefaction process streams. Quarterly technical progress report, October 1--December 31, 1994'.
Thumbnail image of item number 4 in: 'A characterization and evaluation of coal liquefaction process streams. Quarterly technical progress report, October 1--December 31, 1994'.

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Robbins, G.A.; Brandes, S.D.; Winschel, R.A. & Burke, F.P. A characterization and evaluation of coal liquefaction process streams. Quarterly technical progress report, October 1--December 31, 1994, report, May 1, 1995; United States. (digital.library.unt.edu/ark:/67531/metadc622328/: accessed November 12, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.