The Synthesis of Butylsilanes by a Large-Scale Reduction with Lithium Aluminum Hydride

One of 5,165 reports in the series: NACA Research Memorandums available on this site.

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Description

"Eighty pounds of butylsilanes required for test purposes was synthesized by reducing butyltrichlorosilane with lithium aluminum hydride in dioxane solution. This was safely and successfully accomplished by operating in steel equipment under an atmosphere of oil-pumped nitrogen to minimize the hazards involved in conducting this operation on a large scale. The apparatus and procedure used to carry out the necessary manipulations are described in this report" (p. 1).

Physical Description

12 p. : ill.

Creation Information

Kaye, Samuel; Tannenbaum, Stanley & Hipsher, Harold F. July 22, 1953.

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This report is part of the collection entitled: National Advisory Committee for Aeronautics Collection and one other and was provided by UNT Libraries Government Documents Department to Digital Library, a digital repository hosted by the UNT Libraries. It has been viewed 38 times . More information about this report can be viewed below.

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  • Main Title: The Synthesis of Butylsilanes by a Large-Scale Reduction with Lithium Aluminum Hydride
  • Series Title: NACA Research Memorandums

Description

"Eighty pounds of butylsilanes required for test purposes was synthesized by reducing butyltrichlorosilane with lithium aluminum hydride in dioxane solution. This was safely and successfully accomplished by operating in steel equipment under an atmosphere of oil-pumped nitrogen to minimize the hazards involved in conducting this operation on a large scale. The apparatus and procedure used to carry out the necessary manipulations are described in this report" (p. 1).

Physical Description

12 p. : ill.

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  • Accession or Local Control No: 93R16993
  • URL: http://hdl.handle.net/2060/19930087703 External Link
  • Report No.: NACA-RM-E53F03
  • Center for AeroSpace Information Number: 19930087703
  • Archival Resource Key: ark:/67531/metadc59702

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National Advisory Committee for Aeronautics Collection

The National Advisory Committee for Aeronautics (NACA) was a U.S. federal agency founded on March 3, 1915 to undertake, promote, and institutionalize aeronautical research. On October 1, 1958 the agency was dissolved, and its assets and personnel transferred to the newly created National Aeronautics and Space Administration (NASA).

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This selection of materials from the Technical Report Archive and Image Library (TRAIL) includes hard-to-find reports published by various government agencies. The technical publications contain reports, images, and technical descriptions of research performed for U.S. government agencies. Topics range from mining, desalination, and radiation to broader physics, biology, and chemistry studies. Some reports include maps, foldouts, blueprints, and other oversize materials.

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Creation Date

  • July 22, 1953

Added to The UNT Digital Library

  • Nov. 17, 2011, 10:13 p.m.

Description Last Updated

  • Dec. 4, 2018, 5:12 p.m.

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Kaye, Samuel; Tannenbaum, Stanley & Hipsher, Harold F. The Synthesis of Butylsilanes by a Large-Scale Reduction with Lithium Aluminum Hydride, report, July 22, 1953; (digital.library.unt.edu/ark:/67531/metadc59702/: accessed December 18, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; crediting UNT Libraries Government Documents Department.