Abstract: "Sound, fabricable ingots of thorium were produced by triple are melting of electrolytic thorium. Consumable electrodes were fabricated by tack welding of cold-pressed and vacuum-sintered bars of the granular thorium electrodeposited from a molten-salt bath. The hydrogen content of the electrodeposited material was reduced from 80 to 4 ppm by vacuum sintering at 1250 C at pressures below 1 x 10-(-3) mm of mercury. Both sodium and chlorine content were reduced during melting; sodium from 250 to 25 ppm and chlorine from 1000 to 30 ppm. Oxygen and HCl acid-insoluble contents increased during sintering and melting. Oxygen content increased …
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Battelle Memorial Institute Report BMI-1007
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Abstract: "Sound, fabricable ingots of thorium were produced by triple are melting of electrolytic thorium. Consumable electrodes were fabricated by tack welding of cold-pressed and vacuum-sintered bars of the granular thorium electrodeposited from a molten-salt bath. The hydrogen content of the electrodeposited material was reduced from 80 to 4 ppm by vacuum sintering at 1250 C at pressures below 1 x 10-(-3) mm of mercury. Both sodium and chlorine content were reduced during melting; sodium from 250 to 25 ppm and chlorine from 1000 to 30 ppm. Oxygen and HCl acid-insoluble contents increased during sintering and melting. Oxygen content increased from 0.35 to 0.50 w/o and HCl acid-insoluble content from 0.8 to 4.0 w/o. A starlike includion revealed by metallographic examination of the as-cast thorium was identified as ThO2."
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Saller, Henry A.; Dickerson, Ronald F. & Foster, Ellis L.Evaluation and Consolidation of Electrolytic Thorium,
report,
June 15, 1955;
Columbus, Ohio.
(https://digital.library.unt.edu/ark:/67531/metadc502879/:
accessed June 10, 2023),
University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu;
crediting UNT Libraries Government Documents Department.