A Microdetermination of Uranium by Ferric Sulfate Titration

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Description

Abstract: "Following nitrate removal by means of a three-stage hydrochloric acid digestion, uranium was reduced with chromous sulfate reagent. In an inert atmosphere, the quadrivalent uranium was titrated at 80-95[degrees] with standard ferric sulfate solution. The end point was obtained with a potentiometric cell including a platinum in-titrant reference electrode and a platinum indicator electrode. Application was made to various low leverl uranium solutions. For samples containing 1 - 12 milligrams or uranium, less than one percent error may be expected. Iron and chromium do not interfere."

Physical Description

[14] p. ; ill., tables ; 28 cm.

Creation Information

Christopherson, E. W. February 16, 1949.

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This report is part of the collection entitled: Technical Report Archive and Image Library and was provided by the UNT Libraries Government Documents Department to the UNT Digital Library, a digital repository hosted by the UNT Libraries. It has been viewed 19 times. More information about this report can be viewed below.

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Titles

  • Main Title: A Microdetermination of Uranium by Ferric Sulfate Titration
  • Series Title: HW (Series)
  • Added Title: Hanford Works (Richland, Washington) Report 12450
  • Series Title: Hanford Works Reports
  • Added Title: Hanford Works Report HW-12450

Description

Abstract: "Following nitrate removal by means of a three-stage hydrochloric acid digestion, uranium was reduced with chromous sulfate reagent. In an inert atmosphere, the quadrivalent uranium was titrated at 80-95[degrees] with standard ferric sulfate solution. The end point was obtained with a potentiometric cell including a platinum in-titrant reference electrode and a platinum indicator electrode. Application was made to various low leverl uranium solutions. For samples containing 1 - 12 milligrams or uranium, less than one percent error may be expected. Iron and chromium do not interfere."

Physical Description

[14] p. ; ill., tables ; 28 cm.

Notes

Digitized from microopaque cards (1).

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  • OCLC: 921184726
  • SuDoc Number: Y 3.AT 7:22/HW-12450
  • Report No.: HW-12450
  • Archival Resource Key: ark:/67531/metadc502804

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Technical Report Archive and Image Library

The Technical Report Archive & Image Library (TRAIL) identifies, acquires, catalogs, digitizes and provides unrestricted access to U.S. government agency technical reports. The mission of TRAIL is to ensure preservation, discoverability, and persistent open access to government technical publications regardless of form or format.

TRAIL Microcard Collection

Imaged from microcard, these technical reports describe research performed for U.S. government agencies from the 1930s to the 1960s. The reports were provided by the Technical Report Archive and Image Library (TRAIL).

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Creation Date

  • February 16, 1949

Added to The UNT Digital Library

  • Feb. 12, 2018, 7:42 a.m.

Description Last Updated

  • April 23, 2019, 6:20 p.m.

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Christopherson, E. W. A Microdetermination of Uranium by Ferric Sulfate Titration, report, February 16, 1949; Richland, Washington. (https://digital.library.unt.edu/ark:/67531/metadc502804/: accessed October 3, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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