Soft Landing Ion Mobility Mass Spectrometry: History, Instrumentation and an Ambient Pressure Application

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Preparative mass spectrometry is an important method for the synthesis of new materials. Recently, soft landing mass spectrometry has been used to land ions on surfaces to coat or otherwise alter them. Commercial soft landing instruments do not yet exist, and the physical phenomenon of soft landing has not yet been fully described. For future ion mobility soft landing research, the theory of ion mobility, ion optics and soft landing is discussed, and 2 soft landing instruments have been built and described, along with proof of concept experiments for both instruments. Simulations of the process of ion mobility and ion ... continued below

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vii, 61 p.: ill.

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Birdwell, David December 2010.

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This thesis is part of the collection entitled: UNT Theses and Dissertations and was provided by UNT Libraries to Digital Library, a digital repository hosted by the UNT Libraries. It has been viewed 852 times , with 11 in the last month . More information about this thesis can be viewed below.

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  • Birdwell, David

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Description

Preparative mass spectrometry is an important method for the synthesis of new materials. Recently, soft landing mass spectrometry has been used to land ions on surfaces to coat or otherwise alter them. Commercial soft landing instruments do not yet exist, and the physical phenomenon of soft landing has not yet been fully described. For future ion mobility soft landing research, the theory of ion mobility, ion optics and soft landing is discussed, and 2 soft landing instruments have been built and described, along with proof of concept experiments for both instruments. Simulations of the process of ion mobility and ion optics for use in these instruments, as well as some preliminary results for the optics are included. Surfaces described include copper on mica and iron on silicon. Self assembly of soft landed ions is observed on the surfaces.
The instruments constructed will be useful for future soft landing research, and soft landing can be used for future materials research with special attention focused on the self-assembly of the landed ions.

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vii, 61 p.: ill.

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UNT Theses and Dissertations

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  • December 2010

Added to The UNT Digital Library

  • May 4, 2011, 1:11 p.m.

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  • Aug. 2, 2011, 3:28 p.m.

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Citations, Rights, Re-Use

Birdwell, David. Soft Landing Ion Mobility Mass Spectrometry: History, Instrumentation and an Ambient Pressure Application, thesis, December 2010; Denton, Texas. (digital.library.unt.edu/ark:/67531/metadc33136/: accessed April 23, 2018), University of North Texas Libraries, Digital Library, digital.library.unt.edu; .