The Isolation and Purification of Americium

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Gram amounts of americium were separated quantitatively from kilogram quantities of lanthanum to yield an americium product approaching 90% purity. The remaining impurity was chiefly yttrium. Elution of americium from 25% loaded Dowex 50 resin column with 0.15 M citric acid— 0.10 M diammonium citrate — 0.3 M ammonium nitrate, pH 3.3 gave a product containing 99% of the americium with a La/Am ratio of 1/100 or less in one fourth of a column volume, in this case about 1 100-fold volume reduction. Approximately 9 g of americium was purified by this method. Elution with 12.8 M hydrochloric acid from … continued below

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Campbell, D. O. April 17, 1956.

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Gram amounts of americium were separated quantitatively from kilogram quantities of lanthanum to yield an americium product approaching 90% purity. The remaining impurity was chiefly yttrium. Elution of americium from 25% loaded Dowex 50 resin column with 0.15 M citric acid— 0.10 M diammonium citrate — 0.3 M ammonium nitrate, pH 3.3 gave a product containing 99% of the americium with a La/Am ratio of 1/100 or less in one fourth of a column volume, in this case about 1 100-fold volume reduction. Approximately 9 g of americium was purified by this method. Elution with 12.8 M hydrochloric acid from a 20 to 30% loaded column gave 90% of the americium in two column volumes of product with a La/Am ratio of about 1/4. About 1 g of americium was purified by this method.

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Digitized from microopaque cards (1).

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  • April 17, 1956

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  • Feb. 6, 2022, 9:31 a.m.

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  • May 27, 2022, 2:40 a.m.

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Campbell, D. O. The Isolation and Purification of Americium, report, April 17, 1956; Washington D.C.. (https://digital.library.unt.edu/ark:/67531/metadc1956980/: accessed December 1, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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