A Precise Potentiometric Titration Method for the Determination of Uranium

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Description

Abstract: "A precise potentiometric method for the determination of uranium in essentially pure uranium oxides is described. Ten gram samples of oxides are reduced in a Jones reductor and titrated potentiometrically to U+4, using platinum and tungsten electrodes. A weighed amount of solid Bureau of Standards potassium dichromate is then used to oxidize at least 99 percent of the uranous ion, and the oxidation is completed by titration with 0.01 N potassium dichromate using calomel and platinum electrodes. This method, which is based on a primary chemical standard, has a precision of +/- 0.015% on a single determination at the … continued below

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8 p. : tables. ; 28 cm.

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Voss, F. S. & Greene, R. E. August 25, 1953.

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  • Main Title: A Precise Potentiometric Titration Method for the Determination of Uranium
  • Series Title: Atomic Energy Commission Reports
  • Added Title: Atomic Energy Commission Report AECD-4030

Description

Abstract: "A precise potentiometric method for the determination of uranium in essentially pure uranium oxides is described. Ten gram samples of oxides are reduced in a Jones reductor and titrated potentiometrically to U+4, using platinum and tungsten electrodes. A weighed amount of solid Bureau of Standards potassium dichromate is then used to oxidize at least 99 percent of the uranous ion, and the oxidation is completed by titration with 0.01 N potassium dichromate using calomel and platinum electrodes. This method, which is based on a primary chemical standard, has a precision of +/- 0.015% on a single determination at the 95 percent confidence interval."

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8 p. : tables. ; 28 cm.

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  • OCLC: 911662094
  • SuDoc Number: Y 3.AT 7:22/AECD-4030
  • Report No.: AECD-4030
  • Archival Resource Key: ark:/67531/metadc173075

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Technical Report Archive and Image Library

The Technical Report Archive & Image Library (TRAIL) identifies, acquires, catalogs, digitizes and provides unrestricted access to U.S. government agency technical reports. The mission of TRAIL is to ensure preservation, discoverability, and persistent open access to government technical publications regardless of form or format.

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  • August 25, 1953

Added to The UNT Digital Library

  • Feb. 12, 2018, 7:42 a.m.

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  • April 23, 2019, 7:53 p.m.

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Voss, F. S. & Greene, R. E. A Precise Potentiometric Titration Method for the Determination of Uranium, report, August 25, 1953; [Oak Ridge, Tennessee]. (https://digital.library.unt.edu/ark:/67531/metadc173075/: accessed November 9, 2025), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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