Hydrogen Peroxide Analysis and Decomposition in Chromate Solutions

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Description

Abstract: "A novel procedure employing ion exchange resins was developed to separate chromate ions from hydrogen peroxide, permitting, permitting the subsequent analysis of peroxide to determine its decomposition in sodium chromate solutions. At high pH's, peroxide was absorbed anionically on the ion exchange resins along with chromate. By selecting a resin which would be effective at nearly neutral conditions, chromate was satisfactorily separated from peroxide. It was found that the rate of peroxide decomposition in slightly alkaline sodium chromate solutions was dependent on temperature, pH, aeration, and chromate concentration. No significant effect on decomposition was caused by visible light."

Physical Description

[24] p. : ill., tables ; 28 cm.

Creation Information

Rynasiewicz, Joseph & Ryan, J. W. March 17, 1952.

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  • Main Title: Hydrogen Peroxide Analysis and Decomposition in Chromate Solutions
  • Series Title: Atomic Energy Commission Reports
  • Added Title: Atomic Energy Commission Report AECD-3790

Description

Abstract: "A novel procedure employing ion exchange resins was developed to separate chromate ions from hydrogen peroxide, permitting, permitting the subsequent analysis of peroxide to determine its decomposition in sodium chromate solutions. At high pH's, peroxide was absorbed anionically on the ion exchange resins along with chromate. By selecting a resin which would be effective at nearly neutral conditions, chromate was satisfactorily separated from peroxide. It was found that the rate of peroxide decomposition in slightly alkaline sodium chromate solutions was dependent on temperature, pH, aeration, and chromate concentration. No significant effect on decomposition was caused by visible light."

Physical Description

[24] p. : ill., tables ; 28 cm.

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Digitized from microopaque cards (1).

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  • OCLC: 911187996
  • SuDoc Number: Y 3.AT 7:22/AECD-3790
  • Report No.: AECD-3790
  • Government Documents No.: W-31-109-Eng-52
  • Archival Resource Key: ark:/67531/metadc172892

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Technical Report Archive and Image Library

The Technical Report Archive & Image Library (TRAIL) identifies, acquires, catalogs, digitizes and provides unrestricted access to U.S. government agency technical reports. The mission of TRAIL is to ensure preservation, discoverability, and persistent open access to government technical publications regardless of form or format.

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Imaged from microcard, these technical reports describe research performed for U.S. government agencies from the 1930s to the 1960s. The reports were provided by the Technical Report Archive and Image Library (TRAIL).

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Creation Date

  • March 17, 1952

Added to The UNT Digital Library

  • Feb. 12, 2018, 7:42 a.m.

Description Last Updated

  • April 23, 2019, 4:17 p.m.

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Rynasiewicz, Joseph & Ryan, J. W. Hydrogen Peroxide Analysis and Decomposition in Chromate Solutions, report, March 17, 1952; [Oak Ridge, Tennessee]. (https://digital.library.unt.edu/ark:/67531/metadc172892/: accessed May 22, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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