The Determination of Adsorbed Moisture on Uranium and Uranium Oxide: A New Method for Moisture Determinations

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Description

Abstract: "A method is described for determining moisture on uranium and uranium oxides. This method should also be applicable to solid samples which, when heated, do not decompose to form water or liberate a substance which will react with Fischer's reagent. The method should be especially applicable to samples which are insoluble in alcohol or Karl Fischer reagent under normal titration conditions, or which will themselves react with the reagent. The amount of moisture on uranium and uranium oxide was found to be 0.02% except when the oxide was found to be 0.02% except when the oxide source was uranyl … continued below

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[16] p. : ill., tables ; 28 cm.

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Hibbits, James O. & Zucker, Donald April 22, 1953.

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  • Main Title: The Determination of Adsorbed Moisture on Uranium and Uranium Oxide: A New Method for Moisture Determinations
  • Series Title: Atomic Energy Commission Reports
  • Added Title: Atomic Energy Commission Report AECD-3535

Description

Abstract: "A method is described for determining moisture on uranium and uranium oxides. This method should also be applicable to solid samples which, when heated, do not decompose to form water or liberate a substance which will react with Fischer's reagent. The method should be especially applicable to samples which are insoluble in alcohol or Karl Fischer reagent under normal titration conditions, or which will themselves react with the reagent. The amount of moisture on uranium and uranium oxide was found to be 0.02% except when the oxide was found to be 0.02% except when the oxide source was uranyl sulfate. In this case, the moisture content was found to be 0.1%. Modifications of the procedure and apparatus are presented for improving the accuracy and shortening the time necessary for the determination."

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[16] p. : ill., tables ; 28 cm.

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  • OCLC: 911043567
  • SuDoc Number: Y 3.AT 7:22/AECD-3535
  • Report No.: AECD-3535
  • Government Documents No.: W-7405-eng-26
  • Archival Resource Key: ark:/67531/metadc172769

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Technical Report Archive and Image Library

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  • April 22, 1953

Added to The UNT Digital Library

  • Feb. 12, 2018, 7:42 a.m.

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  • April 23, 2019, 6:06 p.m.

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Hibbits, James O. & Zucker, Donald. The Determination of Adsorbed Moisture on Uranium and Uranium Oxide: A New Method for Moisture Determinations, report, April 22, 1953; [Oak Ridge, Tennessee]. (https://digital.library.unt.edu/ark:/67531/metadc172769/: accessed July 12, 2026), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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